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61. 发明授权

US4891451A Preparation of vinyl ethers 失效
标题翻译：乙烯基醚的制备
公开(公告)号：US4891451A
公开(公告)日：1990-01-02
申请号：US213589
申请日：1988-06-30
申请人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer
发明人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer
IPC分类号： C07C41/28
CPC分类号： C07C41/28 , C07C2101/14 , Y02P20/582
摘要： Vinyl ethers of the formula (I) ##STR1## where R.sup.1 to R.sup.3 are identical or different and are each hydrogen, a straight-chain or branched alkyl or alkenyl radical of not more than 12 carbon atoms, halogen-substituted alkyl, a cycloalkyl or cycloalkenyl radical of 5 to 8 carbon atoms, an aryl, alkylaryl, alkenylaryl, aralkyl or aralkenyl radical of 6 to 16 carbon atoms, halogen-substituted aryl or a heterocyclic radical and furthermore R.sup.1 and R.sup.2 or R.sup.1 and R.sup.3, together with the carbon atom to which they are bonded, may form a cycloalkane, cycloalkene or heterocyclic structure, and R.sup.4 is alkyl, alkylaryl or aralkyl, are prepared by a process in which an alcohol is eliminated from an acetal or ketal of the formula (II) ##STR2## where R.sup.1 to R.sup.4 have the above meanings, in the presence of borosilicate and/or iron silicate zeolites as catalysts.
摘要翻译：式（I）的乙烯基醚其中R 1至R 3相同或不同并且各自为氢，不超过12个碳原子的直链或支链烷基或烯基，卤素取代的烷基， 5至8个碳原子的环烷基或环烯基，6至16个碳原子的芳基，烷基芳基，烯基芳基，芳烷基或芳烯基，卤素取代的芳基或杂环基，此外R1和R2或R1和R3连同其键合的碳原子可以通过其中从式（II）的缩醛或缩酮中除去醇的方法制备环烷烃，环烯烃或杂环结构，并且R 4是烷基，烷基芳基或芳烷基，在有硼硅酸盐和/或铁硅酸盐沸石作为催化剂的情况下，R1至R4具有上述含义的图像（II）。

62. 发明授权

US4812593A Preparation of bifunctional compounds 失效
标题翻译：双功能化合物的制备
公开(公告)号：US4812593A
公开(公告)日：1989-03-14
申请号：US82127
申请日：1987-08-06
申请人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer
发明人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer
IPC分类号： C07C45/51 , C07C45/67 , C07C45/71 , C07C47/198 , C07C47/277 , C07C49/175 , C07C49/255 , C07C67/327 , C07C69/708 , C07C69/734 , C07C69/73
CPC分类号： C07C45/71 , C07C45/515 , C07C45/673 , C07C47/198 , C07C47/277 , C07C49/175 , C07C49/255 , C07C67/327
摘要： Bifunctional compounds of the formula ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each alkyl of 1 to 6 carbon atoms, R.sup.2 and R.sup.3 may furthermore be hydrogen, R.sup.2 is furthermore alkoxy and R.sup.4 is hydrogen, alkyl of 1 to 6 carbon atoms or alkoxy, and a double bond may be present between carbon atoms 2 and 3, are prepared by converting a tetraalkoxyalkane or a dialkoxyalkanoate of the formulae ##STR2## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 have the above meanings, in the presence of a catalyst, such as a zeolite, in particular one of the pentasil type, and/or a phosphate and/or phosphoric acid on a carrier.
摘要翻译：其中R 1，R 2和R 3各自为1至6个碳原子的烷基，R 2和R 3可以另外为氢，R 2为烷氧基，且R 4为氢，具有1-6个碳原子的烷基或烷氧基，并且碳原子2和3之间可以存在双键，通过在催化剂存在下，将式Ia，R2，R3和R4具有上述含义的四烷氧基烷烃或二烷氧基烷酸酯进行转化来制备，例如沸石，特别是pentasil类中的一种，和/或载体上的磷酸盐和/或磷酸。

63. 发明授权

US4718936A 6-(3-thienylmethylamino)-purine, its preparation and its use 失效
标题翻译： 6-（3-噻吩甲基氨基） - 嘌呤，其制备及其用途
公开(公告)号：US4718936A
公开(公告)日：1988-01-12
申请号：US711205
申请日：1985-03-13
申请人： Jens-Uwe Bliesener , Hubert Sauter , Norbert Goetz , Johann Jung , Klaus Grossmann
发明人： Jens-Uwe Bliesener , Hubert Sauter , Norbert Goetz , Johann Jung , Klaus Grossmann
IPC分类号： A01N43/90 , C07D473/34 , C07D473/26
CPC分类号： C07D473/34 , A01N43/90
摘要： 6-(3-Thienylmethylamino)-purine of the formula ##STR1## a process for its manufacture, and agents for regulating plant growth containing a compound of the formula I.
摘要翻译：式（I）的6-（3-噻吩甲基氨基） - 嘌呤（I）其制备方法以及含有式I化合物的调节植物生长的试剂。

64. 发明授权

US4532337A Preparation of 3-formyl-5,6-dihydro-2H-pyran 失效
标题翻译： 3-甲酰基-5,6-二氢-2H-吡喃的制备
公开(公告)号：US4532337A
公开(公告)日：1985-07-30
申请号：US584334
申请日：1984-02-28
申请人： Heinz Eckhardt , Klaus Halbritter , Norbert Goetz , Gerd Heilen
发明人： Heinz Eckhardt , Klaus Halbritter , Norbert Goetz , Gerd Heilen
IPC分类号： C07D309/26 , C07D309/00
CPC分类号： C07D309/26
摘要： 3-Formyl-5,6-dihydro-2H-pyran is prepared by conversion of acrolein in the presence of water, acids and halohydrocarbons of 1 to 6 carbon atoms and 1 to 6 halogen atoms as solvents at from 60.degree. to 150.degree. C. The 3-formyl-5,6-dihydro-2H-pyran obtained by the novel process is a valuable starting material for the preparation of dyes and crop protection agents.
摘要翻译： 3-甲酰基-5,6-二氢-2H-吡喃是通过在水，酸和1至6个碳原子和1至6个卤素原子的卤代烃作为溶剂在60至150℃的存在下转化丙烯醛来制备的通过新方法获得的3-甲酰基-5,6-二氢-2H-吡喃是制备染料和作物保护剂的有价值的起始原料。

65. 发明授权

US4328380A Substituted phenylpropyl halides 失效
标题翻译：取代的苯基丙基卤化物
公开(公告)号：US4328380A
公开(公告)日：1982-05-04
申请号：US176456
申请日：1980-08-08
申请人： Ernst Buschmann , Norbert Goetz , Bernd Zeeh , Juergen Varwig
发明人： Ernst Buschmann , Norbert Goetz , Bernd Zeeh , Juergen Varwig
IPC分类号： A01N29/10 , C07C17/00 , C07C17/12 , C07C17/26 , C07C17/275 , C07C17/32 , C07C22/04 , C07C22/08 , C07C25/02 , C07C25/18 , C07C41/00 , C07C41/30 , C07C43/225 , C07C45/00 , C07C45/46 , C07C49/80 , C07C67/00 , C07C201/00 , C07C205/11 , C07C21/24
CPC分类号： C07C205/11 , C07C17/12 , C07C17/269 , C07C17/275 , C07C17/278 , C07C41/30 , C07C43/225 , C07C45/46 , C07C49/80
摘要： A novel process for the preparation of phenylpropyl halides of the formula ##STR1## by reacting the corresponding phenylpropyl halides, substituted only by R.sup.2 and R.sup.1, with an alcohol, alkyl halide or olefin; and phenylpropyl halides where R.sup.3 has certain meanings.
摘要翻译：通过使相应的仅被R 2和R 1取代的苯基丙基卤化物与醇，烷基卤化物或烯烃反应制备式“苯基丙基卤化物”的新方法; 和苯基丙基卤化物，其中R3具有一定的含义。

66. 发明授权

US4298733A Preparation of cis-2,6-dimethylmorpholine 失效
标题翻译：顺式-2,6-二甲基吗啉的制备
公开(公告)号：US4298733A
公开(公告)日：1981-11-03
申请号：US184816
申请日：1980-09-08
申请人： Norbert Goetz , Walter Himmele , Leopold Hupfer
发明人： Norbert Goetz , Walter Himmele , Leopold Hupfer
IPC分类号： C07D265/30 , B01J23/60 , B01J23/656 , C07B61/00 , C07D295/023
CPC分类号： C07D295/023
摘要： A process for the preparation of cis-2,6-dimethylmorpholine by isomerizing trans-2,6-dimethylmorpholine, wherein trans-2,6-dimethylmorpholine is converted, in the presence of hydrogen and of a catalyst containing palladium as well as zinc, cadmium or manganese or a mixture of these, at from 150.degree. to 250.degree. C. under a pressure of from 1 to 200 bar.
摘要翻译：通过异构化反式-2,6-二甲基吗啉，其中反式-2,6-二甲基吗啉在氢气和含有钯的催化剂以及锌的存在下转化而制备顺式-2,6-二甲基吗啉的方法，镉或锰或它们的混合物，在150-250℃，1至200巴的压力下进行。

67. 发明授权

US4282238A Insecticidal process 失效
标题翻译：杀虫过程
公开(公告)号：US4282238A
公开(公告)日：1981-08-04
申请号：US060836
申请日：1979-07-26
申请人： Norbert Goetz , Anna Steimmig , Bernd Zeeh , Heinrich Adolphi
发明人： Norbert Goetz , Anna Steimmig , Bernd Zeeh , Heinrich Adolphi
IPC分类号： C07D233/56 , A01N43/50 , A01N49/00 , C07D233/58 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N49/00 , C07D233/56 , C07D249/08
摘要： Insecticidal agents containing, as active ingredients, imidazole derivatives or salts thereof. The imidazole derivatives have the formula ##STR1## where R.sup.1 denotes branched alkyl of 6 to 20 carbon atoms, linear alkyl of 6 to 16 carbon atoms, branched alkenyl of 10 to 20 carbon atoms, linear or branched alkynyl of 3 to 6 carbon atoms, 2-methyl-3-phenylpropyl or 2-methyl-3-phenylpropen-2-yl, phenyl being unsubstituted or mono- or polysubstituted by halogen or alkyl of 1 to 10 carbon atoms, and R.sup.2, R.sup.3 and R.sup.4 denote hydrogen or methyl.These insecticidal agents are suitable as growth regulators and ovicides for controlling insects from the Lepidoptera, Coleoptera, Diptera, Hymenoptera, Heteroptera, Homoptera and Isoptera classes.
摘要翻译：含有作为活性成分的咪唑衍生物或其盐的杀虫剂。咪唑衍生物具有式“IMAGE”，其中R 1表示6至20个碳原子的支链烷基，6至16个碳原子的直链烷基，10-20个碳原子的支链烯基，3至6个碳原子的直链或支链炔基， 2-甲基-3-苯基丙基或2-甲基-3-苯基丙-2-基，苯基是未取代的或被卤素或1-10个碳原子的烷基单取代或多取代，R2，R3和R4表示氢或甲基。这些杀虫剂适合作为生长调节剂和杀卵剂，用于控制来自鳞翅目，鞘翅目，双翅目，膜翅目，异翅目，同翅目和等翅目类的昆虫。

68. 发明授权

US4021411A Production of high molecular weight .alpha.,.beta.-unsaturated aldehydes 失效
标题翻译：生产高分子量{60，{62-不饱和醛
公开(公告)号：US4021411A
公开(公告)日：1977-05-03
申请号：US583637
申请日：1975-06-04
申请人： Norbert Goetz , Roman Fischer
发明人： Norbert Goetz , Roman Fischer
IPC分类号： C07C45/70 , C07C45/71 , C07C47/20
CPC分类号： C07C45/71 , C07C45/70
摘要： A process for the production of high molecular weight .alpha.,.beta.-unsaturated aldehydes by alkylation of the .gamma.-carbon atom of a lower molecular weight .alpha.,.beta.-unsaturated aldehyde with a substituted allyl alcohol which has a chain branching in the 4-position carbon atom or a phenyl radical in the 4-position or of a corresponding allyl alcohol carboxylic ester at elevated temperature in the liquid phase.The products are valuable intermediates for the production of natural substances and odorants.
摘要翻译：通过用较低分子量的α，β-不饱和醛的γ-碳原子烷基化制备高分子量α，β-不饱和醛的方法，该取代的烯丙醇在4-位碳上具有支链分支原子或4-位的苯基或相应的烯丙基醇羧酸酯在液相中升高的温度。

69. 发明授权

US5563114A Cyclohexenone oxime ethers, their preparation, intermediates for their preparation and their use as herbicides 失效
标题翻译：环己烯酮肟醚，它们的制备，其制备中间体及其作为除草剂的用途
公开(公告)号：US5563114A
公开(公告)日：1996-10-08
申请号：US409969
申请日：1995-03-24
申请人： Norbert Meyer , Juergen Kast , Ulf Misslitz , Albrecht Harreus , Norbert Goetz , Bruno Wuerzer , Helmut Walter , Karl-Otto Westphalen , Matthias Gerber
发明人： Norbert Meyer , Juergen Kast , Ulf Misslitz , Albrecht Harreus , Norbert Goetz , Bruno Wuerzer , Helmut Walter , Karl-Otto Westphalen , Matthias Gerber
IPC分类号： A01N35/10 , A01N43/08 , A01N43/10 , A01N43/14 , A01N43/16 , A01N43/18 , A01N43/30 , A01N43/32 , A01N43/36 , A01N43/80 , A01P13/00 , C07C239/20 , C07C251/36 , C07C251/42 , C07C251/50 , C07C251/52 , C07C251/54 , C07C251/60 , C07C255/62 , C07C323/47 , C07D207/32 , C07D207/335 , C07D261/02 , C07D261/04 , C07D261/08 , C07D275/02 , C07D307/14 , C07D309/06 , C07D317/26 , C07D319/06 , C07D333/16 , C07D333/22 , C07D333/58 , C07D335/02 , C07D339/06 , A01N43/28 , A01N43/78
CPC分类号： C07D207/335 , A01N35/10 , A01N43/14 , C07C239/20 , C07C251/42 , C07C251/52 , C07D261/08 , C07D275/02 , C07D309/06 , C07D319/06 , C07D333/22 , C07D335/02 , C07C2101/12 , C07C2101/14
摘要： Cyclohexenone oxime ethers of the general formula I ##STR1## where R.sup.1 is alkyl,A is unsubstituted or substituted C.sub.3 -, C.sub.5 - or C.sub.6 -alkylene or C.sub.3 -, C.sub.5 - or C.sub.6 -alkenylene,X is NO.sub.2, CN, halogen, alkyl, alkoxy, phenoxy, alkylthio, haloalkyl, haloalkoxy, carboxyl, alkoxycarbonyl, unsubstituted or substituted benzyloxycarbonyl and/or unsubstituted or substituted phenyl,n is 0-3 or 1-5 where X is halogen,R.sup.2 is alkoxy-alkyl or alkylthio-alkyl, unsubstituted or substituted cycloalkyl or cycloalkenyl, an unsubstituted or substituted 5-membered saturated heterocyclic structure having one or two oxygen and/or sulfur atoms as hetero atoms, an unsubstituted or substituted 6-membered or 7-membered heterocyclic structure having up to two oxygen and/or sulfur atoms and up to two double bonds, an unsubstituted or substituted 5-membered heteroaromatic having up to two nitrogen atoms and one oxygen atom or one sulfur atom, or unsubstituted or substituted phenyl or pyridyl, and their agriculturally useful salts and esters of C.sub.1 -C.sub.10 -carboxylic acids and inorganic acids, processes and intermediates for their preparation, and their use as herbicides.
摘要翻译：通式I的环己烯酮肟醚其中R 1为烷基，A为未取代或取代的C3-，C5-或C6-亚烷基或C3-，C5-或C6-亚烯基，X为NO2，CN，卤素，烷基，烷氧基，苯氧基，烷硫基，卤代烷基，卤代烷氧基，羧基，烷氧基羰基，未取代或取代的苄氧羰基和/或未取代或取代的苯基，n为0-3或1-5，其中X为卤素，R2为烷氧基 - 烷硫基 - 烷基，未取代或取代的环烷基或环烯基，具有一个或两个氧和/或硫原子作为杂原子的未取代或取代的5元饱和杂环结构，未取代或取代的6元或7元杂环结构，至多两个氧原子和/或硫原子和至多两个双键，未取代或取代的具有至多两个氮原子和一个氧原子或一个硫原子的5元杂芳族化合物，或未取代或取代的苯基或吡啶基，以及它们的农业用途 C1-C10羧酸和无机酸的富盐和酯，其制备方法和中间体，以及它们作为除草剂的用途。

70. 发明授权

US5350863A Preparation of 3-(2'-oxyethyl)dihydro-2(3H)furanones 失效
标题翻译：制备3-（2'-氧乙基）二氢-2（3H）呋喃酮
公开(公告)号：US5350863A
公开(公告)日：1994-09-27
申请号：US120439
申请日：1993-09-14
申请人： Thomas Kuekenhoehner , Norbert Goetz , Rolf Fischer , Werner Schnurr , Dirk Borchers
发明人： Thomas Kuekenhoehner , Norbert Goetz , Rolf Fischer , Werner Schnurr , Dirk Borchers
IPC分类号： C07D307/33 , C07D307/20
CPC分类号： C07D307/33
摘要： A process for preparing 3-(2'-oxyethyl)dihydro-2(3H)furanones of the general formula I ##STR1## where R.sup.1 is hydrogen or acetyl, by reacting ethylene oxide with acetoacetic acid esters of the general formula II ##STR2## where R.sup.2 is C.sub.1 -C.sub.4 -alkyl, which comprises carrying out the reaction in alcoholic solutions in the presence of alkali metal alkoxides at from 20.degree. to 100.degree. C. and from 1 to 20 bar, is described.
摘要翻译：制备通式Ⅰ的3-（2'-氧乙基）二氢-2（3H）呋喃酮的方法，其中R1是氢或乙酰基，通过使环氧乙烷与通式II的乙酰乙酸酯反应其中R 2是C 1 -C 4 - 烷基，其包括在20至100℃和1至20巴的碱金属醇盐存在下，在醇溶液中进行反应。

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