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    • 64. 发明授权
    • Pseudoboehmite powder for catalyst carrier and process for preparing the same
    • 用于催化剂载体的假勃姆石粉末及其制备方法
    • US06174511B1
    • 2001-01-16
    • US09254658
    • 1999-05-06
    • Takayuki TsukadaHiroyuki Nakamura
    • Takayuki TsukadaHiroyuki Nakamura
    • C01F702
    • C01F7/34B01J21/04B01J35/1042B01J35/1047B01J35/1061B01J35/108C01F7/141C01P2006/14C01P2006/16
    • An aluminum salt solution and an alkali aluminate solution are subjected to a neutralization reaction to precipitate and form a pseudo-boehmite powder. The neutralization reaction is performed under a condition in which the reaction temperature is within a range of 55 to 71° C., pH is within a range of 8.5 to 9.5, and the solution feed time is within a range of 7 to 25 minutes. The obtained pseudo-boehmite is as follows. That is, the pore volume concerning pores having a pore diameter ranging from 20 to 600 Å is within a range of 0.8 to 1.8 cc/g as measured by the nitrogen adsorption method, and the maximum value of variation ratio dV/dD of the pore volume with respect to the pore diameter as measured by the BJH method is not more than 0.018 cc/g•Å. When the pseudo-boehmite is used, it is possible to produce a catalyst carrier for hydrogenation refining, which has a sharp pore diameter distribution and which suffers less decrease in strength upon impregnation with a catalyst solution.
    • 将铝盐溶液和碱金属铝酸盐溶液进行中和反应以沉淀并形成假勃姆石粉末。 中和反应在反应温度为55〜71℃,pH为8.5〜9.5的范围内,溶液进料时间为7〜25分钟的条件下进行。 所得的假勃姆石如下。 也就是说,通过氮吸附法测定的孔径为20〜600的孔的孔体积在0.8〜1.8cc / g的范围内,孔的变化率dV / dD的最大值 通过BJH法测定的相对于孔径的体积不大于0.018cc / g。 当使用假勃姆石时,可以制备氢化精炼用催化剂载体,其具有尖锐的孔径分布,并且在用催化剂溶液浸渍时其强度降低较少。
    • 66. 发明授权
    • Measuring chip for optical analyzer
    • 光学分析仪测量芯片
    • US6104484A
    • 2000-08-15
    • US44847
    • 1998-03-20
    • Ryohei NagataHiroyuki Nakamura
    • Ryohei NagataHiroyuki Nakamura
    • G01N21/64G01N1/28G01N21/03G01N21/27G01N21/31G01N21/41G01N33/543G01N1/10G01N21/00
    • G01N21/553
    • A measuring chip for an optical analyzer includes a translucent or transparent substrate 1, and a sample solution chamber S formed on a sulface of the translucent or transparent substrate 1. The sample solution chamber S has an inlet S.sub.1 for introducing a sample solution to be analyzed, and an outlet S.sub.2 for discharging the analyzed sample solution. The sample solution chamber S is formed so as to be filled with the sample solution between the inlet S.sub.1 and the vicinity of the outlet S.sub.2 by the capillary phenomenon. On the translucent or transparent substrate 1, an analyzing region 10 is formed by stacking a metal thin film 2 and an immobilizing film 3 for immobilizing a physiologically active substance 4. On the analyzing region 10, the sample solution chamber S is formed to obtain a measuring chip for an optical analyzer particularly utilizing the surface plasmon resonance (SPR). Thus. it, is possible to obtain a measuring chip for an optical analyzer, which can be easily handled and which can carry out an analysis using a small quantity of sample solution.
    • 用于光学分析仪的测量芯片包括半透明或透明基板1和形成在半透明或透明基板1的表面上的样品溶液室S.样品溶液室S具有用于引入待分析样品溶液的入口S1 ,以及用于排出所分析的样品溶液的出口S2。 样品溶液室S形成为通过毛细管现象填充入口S1和出口S2附近的样品溶液。 在半透明或透明基板1上,通过堆叠用于固定生理活性物质4的金属薄膜2和固定膜3来形成分析区域10.在分析区域10上,形成样品溶液室S, 用于特别利用表面等离子体共振(SPR)的光学分析仪的测量芯片。 从而。 可以获得可以容易地处理并且可以使用少量样品溶液进行分析的光学分析仪的测量芯片。