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61. 发明授权

US4639330A Alkyl-substituted spirodecenone derivatives, organoleptic utility thereof and processes for preparing same 失效
标题翻译：烷基取代的十六烯酮衍生物，其感官效用及其制备方法
公开(公告)号：US4639330A
公开(公告)日：1987-01-27
申请号：US842207
申请日：1986-03-21
申请人： Mark A. Sprecker , Marie R. Hanna
发明人： Mark A. Sprecker , Marie R. Hanna
IPC分类号： C07C45/69 , C07C49/637 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C07C45/69 , C07C49/637
摘要： Described are alkyl-substituted spirodecenone derivatives defined according to the structure: ##STR1## wherein one of R.sub.1 or R.sub.2 is hydrogen and the other of R.sub.1 or R.sub.2 is methyl; and wherein R.sub.3 represents C.sub.3 -C.sub.4 alkyl, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including, but not limited to, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles and hair preparations; as well as processes for preparing said alkyl-substituted spirodecenone derivatives.
摘要翻译：描述了根据以下结构定义的烷基取代的螺十一酮衍生物：其中R 1或R 2中的一个是氢，R 1或R 2中的另一个是甲基; 并且其中R 3表示C 3 -C 4烷基，以及其用于增强或增强香料组合物，古龙水和香料制品的香气，包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物软化剂制品和头发制剂; 以及制备所述烷基取代的螺十一酮衍生物的方法。

62. 发明授权

US4622171A Polyhydroindan carboxaldehydes and uses thereof in augmenting or enhancing the aromas of perfume compositions, colognes and perfumed articles 失效
公开(公告)号：US4622171A
公开(公告)日：1986-11-11
申请号：US712164
申请日：1985-03-15
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is the genus of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein each of the dashed lines represent carbon-carbon single bonds or carbon-carbon double bonds with the proviso that at least one of the dashed lines represents a carbon-carbon single bond; wherein one of R.sub.1, R.sub.2 and R.sub.3 is hydrogen or methyl and each of the other of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; wherein one of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen or methyl and each of the other of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen; wherein m is 0 or 1 and n is 0 or 1 and the sum of m+n=1; wherein X' represents one of the moieties: ##STR2## wherein R.sub.7 represents C.sub.1 -C.sub.3 alkyl or acetyl; and wherein R.sub.8 represents C.sub.1 -C.sub.3 alkyl, with the proviso that when X' is methylene having the structure: ##STR3## then m is 0 and n is 1 and with the further proviso that when n is 0, one of the dashed lines is a carbon-carbon double bond; and one of R.sub.1, R.sub.2 and R.sub.3 represents methyl and one of R.sub.4, R.sub.5, and R.sub.6 represents methyl, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, perfumed polymers and cosmetic powders). Also described is a process for preparing such polyhydroindan carboxaldehydes by reacting a tricyclic compound or mixture of compounds defined according to the structure: ##STR4## with carbon monoxide and hydrogen via an "oxo" reaction; wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are defined, supra; wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein X" represents one of the moieties: with the proviso that when X' is methylene having the structure: ##STR5## then the line:+++++is a double bond and when X' is not methylene having the structure: ##STR6## then the line:+++++is a carbon-carbon single bond.

63. 发明授权

US4541949A Polyhydroindan carboxaldehydes 失效
标题翻译：聚氢化二氢甲醛
公开(公告)号：US4541949A
公开(公告)日：1985-09-17
申请号：US528568
申请日：1983-09-01
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is the composition of matter defined according to the structure: ##STR1## as well as components of such composition having the structures: ##STR2## and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles.
摘要翻译：描述了根据以下结构定义的物质的组成：以及具有以下结构的这种组合物的组分：＆lt; IMAGE＆gt; + TR＆lt; IMAGE＆gt;＆gt;及其用于增强或增强香料组合物的香气，古龙水和香水文章。

64. 发明授权

US4507225A Process for augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles with 1-phenylpenten-4-one-1 and methyl homologues thereof 失效
标题翻译：用1-苯基戊-4-酮-1及其甲基同系物增强或增强香料组合物，古龙水和香精制品香气的方法
公开(公告)号：US4507225A
公开(公告)日：1985-03-26
申请号：US487045
申请日：1983-04-21
申请人： Mark A. Sprecker , Marie R. Hanna
发明人： Mark A. Sprecker , Marie R. Hanna
IPC分类号： D06M13/12 , A61K8/00 , A61K8/35 , A61L9/01 , A61Q5/00 , A61Q13/00 , C07C45/68 , C07C45/71 , C07C49/794 , C11B9/00 , C11D3/50 , C11D9/44 , D06M13/02 , A61K7/46 , C11D9/30
CPC分类号： C11B9/0061 , C07C45/68 , C07C45/71 , C07C49/794
摘要： Described for use in augmenting or enhancing the aroma of perfume compositions, perfumed articles and colognes is the genus of compounds having the structure: ##STR1## wherein one of R.sub.1 or R.sub.2 is methyl and the other of R.sub.1 or R.sub.2 is hydrogen or wherein both R.sub.1 and R.sub.2 are hydrogen, hereinafter referred to as 1-phenylpenten-4-one-1 and methyl homologues thereof.
摘要翻译：描述用于增强或增强香料组合物，香料制品和古龙水的香气是具有以下结构的化合物的属：其中R 1或R 2中的一个为甲基，R 1或R 2中的另一个为氢或其中两个R 1 R2为氢，以下称为1-苯基戊-4-酮-1及其甲基同系物。

65. 发明授权

US5552380A Perfume uses of phenyl alkanol derivatives 失效
标题翻译：香料使用苯基链烷醇衍生物
公开(公告)号：US5552380A
公开(公告)日：1996-09-03
申请号：US356504
申请日：1994-12-15
申请人： Mark A. Sprecker , Richard A. Weiss , Marie R. Hanna
发明人： Mark A. Sprecker , Richard A. Weiss , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0061
摘要： Described are phenyl alkanol derivatives defined according to the structure: ##STR1## wherein R.sub.1 is methyl or ethyl and R.sub.2 is hydrogen or acetyl with the proviso that when R.sub.2 is hydrogen, R.sub.1 is ethyl and when R.sub.2 is acetyl, R.sub.1 is methyl and uses thereof in augmenting, enhancing or imparting an aroma in or to perfume compositions, colognes and perfumed articles including but not limited to solid or liquid, anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles and hair preparations.
摘要翻译：描述的是根据以下结构定义的苯基链烷醇衍生物：其中R1是甲基或乙基，R2是氢或乙酰基，条件是当R2是氢时，R1是乙基，当R2是乙酰基时，R1是甲基，其用途包括但不限于固体或液体，阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品和毛发制品，以增强或增强香料或香料组合物，古龙水和香料制品中的香味。

66. 发明授权

US5486502A 2-methoxy-4-formyl phenyl ester of propionic acid and use in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles 失效
标题翻译：丙酸的2-甲氧基-4-甲酰基苯基酯，用于增强或增强香水组合物，古龙水和香料的香气
公开(公告)号：US5486502A
公开(公告)日：1996-01-23
申请号：US356523
申请日：1994-12-15
申请人： Mark A. Sprecker , Richard A. Weiss , Marie R. Hanna
发明人： Mark A. Sprecker , Richard A. Weiss , Marie R. Hanna
IPC分类号： C07C69/017 , C11B9/00 , A61K7/46
CPC分类号： C07C69/017 , C11B9/0061
摘要： Described is 2-methoxy-4-formyl phenyl ester of propionic acid defined according to the structure: ##STR1## and uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles and colognes.
摘要翻译：描述了根据以下结构定义的丙酸2-甲氧基-4-甲酰基苯基酯：香料组合物，香料制品和古龙水的香味。

67. 发明授权

US4668432A Alkyl-substituted-oxo-spirodecenene derivatives, organoleptic utility thereof and processes for preparing same 失效
标题翻译：烷基取代的 - 氧代 - 十六烯烯衍生物，其感官效用及其制备方法
公开(公告)号：US4668432A
公开(公告)日：1987-05-26
申请号：US879425
申请日：1986-06-27
申请人： Mark A. Sprecker , Marie R. Hanna
发明人： Mark A. Sprecker , Marie R. Hanna
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11B9/0057 , C11D3/50
摘要： Described are alkyl-substituted-oxo-spirodecenene derivatives defined according to the structure: ##STR1## wherein X represents carbinol, carbinol C.sub.1 -C.sub.3 alkanoate or ketone; one of R.sub.1, R.sub.2, R.sub.4 and R.sub.5 represents methyl and the other of R.sub.1, R.sub.2, R.sub.4 and R.sub.5 represents hydrogen; and R.sub.3 is n-butyl or isopropyl and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles and hair preparations; as well as processes for preparing said alkyl-substituted-oxo-spirodecenene derivatives.
摘要翻译：描述了根据以下结构定义的烷基取代的氧代 - 螺十一烯衍生物：其中X表示甲醇，甲醇C1-C3链烷酸酯或酮; R1，R2，R4和R5之一表示甲基，R1，R2，R4和R5中的另一个表示氢; 并且R 3是正丁基或异丙基，并且其用于增强或增强香料组合物，古龙水和香料制品的香气，包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品和头发准备; 以及制备所述烷基取代的 - 氧代 - 十六烯烯衍生物的方法。

68. 发明授权

US4822515A Ethyl norbornyl alkyl ethers, organoleptic uses thereof and process for preparing same 失效
标题翻译：乙基降冰片基烷基醚，其感官用途及其制备方法
公开(公告)号：US4822515A
公开(公告)日：1989-04-18
申请号：US213318
申请日：1988-06-30
申请人： Mark A. Sprecker , Margo Androulakis , Marie R. Hanna
发明人： Mark A. Sprecker , Margo Androulakis , Marie R. Hanna
IPC分类号： C07C43/18 , C11B9/00 , C11D3/50 , C11D7/18
CPC分类号： C11D3/3956 , C07C43/18 , C11B9/0042 , C11B9/0046 , C11D3/50
摘要： Described are ethyl norbornyl alkyl ethers of our invention defined according to the generic structure: ##STR1## wherein R represents 1-C.sub.2, 1-C.sub.4 or 1-C.sub.6 straight chain lower alkyl and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to bleach compositions, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations. Also described is a process for preparing such ethyl norbornyl alkyl ethers of our invention by means of reaction of compounds defined according to the structure: ##STR2## and/or compounds defined according to the structure: ##STR3## in admixture with compounds having the structure: ##STR4## with hydrogen in the presence of a hydrogenation catalyst.
摘要翻译：描述了根据以下通用结构定义的本发明的乙基降冰片烷基烷基醚：其中R代表1-C2，1-C4或1-C6直链低级烷基和感官用途，用于增强或增强香料组合物的香气包括但不限于漂白组合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。还描述了通过根据以下结构定义的化合物的反应来制备本发明的这种乙基降冰片基烷基醚的方法：＆lt; IMAGE＆gt;和/或根据以下结构定义的化合物：＆lt; IMAGE＆gt;与具有结构的化合物：在氢化催化剂存在下用氢气。

69. 发明授权

US4636333A Alkoxy-substituted polyhydroindan carboxaldehydes 失效
标题翻译：烷氧基取代的多羟基茚满羧醛
公开(公告)号：US4636333A
公开(公告)日：1987-01-13
申请号：US837386
申请日：1986-03-07
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is a mixture of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein R.sub.7 represents a moiety selected from the group consisting of methyl and isopropyl prepared by means of reacting bicyclopentadiene with a lower alkanol in the presence of a Lewis acid in order to form a mixture of compounds defined according to the structure: ##STR2## and then reacting the resulting ether with carbon monoxide and hydrogen in the presence of an "oxo" reaction catalyst.
摘要翻译：描述了根据以下结构定义的多羟基茚基甲醛的混合物：其中R 7表示选自甲基和异丙基的部分，其通过在路易斯酸存在下通过双环戊二烯与低级链烷醇反应制备，以便形成根据以下结构定义的化合物的混合物：，然后在“氧代”反应催化剂存在下，使所得的醚与一氧化碳和氢气反应。

70. 发明授权

US06835699B2 Bicycle lactones, perfumery uses thereof, processes for preparing same and intermediates therefor 有权
标题翻译：自行车内酯，其香料用途，其制备方法及其中间体
公开(公告)号：US06835699B2
公开(公告)日：2004-12-28
申请号：US10401824
申请日：2003-03-28
申请人： Richard A. Weiss , Mark A. Sprecker , Marie R. Hanna , Charles E. J. Beck , Harold W. Jackson
发明人： Richard A. Weiss , Mark A. Sprecker , Marie R. Hanna , Charles E. J. Beck , Harold W. Jackson
IPC分类号： C11D350
CPC分类号： A61K8/498 , A61L9/01 , A61L9/012 , A61Q13/00 , C07D311/02 , C07D311/74 , C11B9/008 , C11D3/2096 , C11D3/50
摘要： Described are bicyclic lactones, both fused ring lactones defined according to the generic structure: and spiro lactones defined according to the generic structure: uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, perfumed articles, colognes and perfumed polymers; processes for preparing such bicyclic lactones and intermediates therefor. In the structure: Z is one of the moieties: one of R1 or R3 is methyl and the other is hydrogen; and R4, R5, R6, R7, R8 and R9 are hydrogen or nonadjacent C1-C3 alkyl. In the structure: Y represents C2-C12 substituted or unsubstituted alkylidenyl, alkenylidenyl or alkadienylidenyl having the structure: and completes a C5-C15 cycloalkyl, cycloalkadienyl or cycloalkenyl ring moiety; and wherein R12, R13, R14, R16, R17, R28, R29, R30 and R31 represent hydrogen or R1 or R3 nonadjacent alkyl; wherein s is an integer of from 0 up to 10; t is an integer of from 0 up to 10; and v is an integer of 1 or 2; with the proviso that the sum of s and t is between 0 and 10 according to the inequalities: 0≦s+t≦10; 0≦s≦10; and 0≦t≦10.
摘要翻译：描述的是双环内酯，根据通用结构定义的稠环内酯和根据通用结构定义的螺内酯：用于增强，增强或赋予香料组合物，香料制品，古龙水和加香聚合物中的香气; 制备这种双环内酯的方法及其中间体。在结构中：Z是部分之一：R 1或R 3中的一个是甲基，另一个是氢; 且R 4，R 5，R 6，R 7，R 8和R 9为氢或不相邻的C 1 -C 3烷基。在结构中：Y表示具有以下结构的C 2 -C 12取代或未取代的亚烷基，亚烯基或链二烯基;并且完成C 5 -C 15环烷基，环链二烯基或环烯基环部分; 并且其中R 12，R 13，R 14，R 16，R 17，R 28，R 29，R 30和R 31表示氢或R 1或R 3不相邻的烷基; 其中s为0至10的整数; t是0到10的整数; v为1或2的整数; 条件是根据不等式，s和t之和在0和10之间：0 <= s + t <= 10; 0 <= s <= 10; 0 <= T＆LE; 10。

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