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61. 发明授权

US08367851B2 Hydroxymethylfurfural reduction methods and methods of producing furandimethanol 有权
标题翻译：羟甲基糠醛还原方法和生产呋喃二甲醇的方法
公开(公告)号：US08367851B2
公开(公告)日：2013-02-05
申请号：US13173942
申请日：2011-06-30
申请人： Michael A. Lilga , Richard T. Hallen , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , James F. White , Michel J. Gray
IPC分类号： C07D307/02
CPC分类号： C07D307/42 , C07D307/46
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250° C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30° C. A method of producing tetrahydrofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。将H2置于反应器中，并使原料与含有至少一种选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh的金属的催化剂在小于或等于250的温度下接触氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性地氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

62. 发明申请

US20130008080A1 DEOXYGENATION OF FATTY ACIDS FOR PREPARATION OF HYDROCARBONS 有权
标题翻译：用于制备碳氢化合物的脂肪酸的去氧化
公开(公告)号：US20130008080A1
公开(公告)日：2013-01-10
申请号：US13620268
申请日：2012-09-14
申请人： Richard T. Hallen , Karl O. Albrecht , Heather M. Brown , James F. White
发明人： Richard T. Hallen , Karl O. Albrecht , Heather M. Brown , James F. White
IPC分类号： C10L1/12
CPC分类号： B01J23/6525 , B01J21/066 , B01J21/18 , B01J23/624 , B01J23/626 , B01J23/6527 , B01J37/0203 , B01J37/0205 , C10G3/44 , C10G3/47 , C10G3/48 , C10G2300/1014 , C10G2300/1018 , C10G2300/205 , C10G2300/4012 , C10G2300/4018 , C10G2300/4081 , C10G2300/44 , C10G2400/04 , C10G2400/08 , C10G2400/30 , C10L1/08 , C10L1/1208 , C10L2200/0469 , C10L2270/02 , C10L2270/04 , C11C3/00 , Y02E50/13 , Y02P30/20 , Y02T50/678
摘要： Embodiments of methods for making renewable diesel by deoxygenating (decarboxylating/decarbonylating/dehydrating) fatty acids to produce hydrocarbons are disclosed. Fatty acids are exposed to a catalyst selected from a) Pt and MO3 on ZrO2 (M is W, Mo, or a combination thereof), or b) Pt/Ge or Pt/Sn on carbon, and the catalyst decarboxylates at least 10% of the fatty acids. In particular embodiments, the catalyst consists essentially of 0.7 wt % Pt and 12 wt % WO3, relative to a mass of catalyst, or the catalyst consists essentially of a) 5 wt % Pt and b) 0.5 wt % Ge or 0.5 wt % Sn, relative to a mass of catalyst. Deoxygenation is performed without added hydrogen and at less than 100 psi. Disclosed embodiments of the catalysts deoxygenate at least 10% of fatty acids in a fatty acid feed, and remain capable of deoxygenating fatty acids for at least 200 minutes to more than 350 hours.
摘要翻译：公开了通过脱氧（脱羧/脱羰/脱水）脂肪酸制备可再生柴油以生产烃的方法的实施方案。将脂肪酸暴露于选自a）Pt和MO3的ZrO 2上的催化剂（M为W，Mo或其组合），或b）Pt / Ge或Pt / Sn在碳上，催化剂脱羧至少10％的脂肪酸。在具体实施方案中，催化剂相对于催化剂质量基本上由0.7重量％的Pt和12重量％的WO 3组成，或者催化剂基本上由a）5重量％的Pt和b）0.5重量％的Ge或0.5重量％的Sn ，相对于催化剂的质量。在不加入氢气的情况下进行脱氧，并且小于100psi。在脂肪酸进料中脱氧至少10％脂肪酸的催化剂的公开实施方案，并且能够使脂肪酸脱氧至少200分钟至超过350小时。

63. 发明申请

US20120029250A1 DEOXYGENATION OF FATTY ACIDS FOR PREPARATION OF HYDROCARBONS 有权
标题翻译：用于制备碳氢化合物的脂肪酸的去氧化
公开(公告)号：US20120029250A1
公开(公告)日：2012-02-02
申请号：US12848887
申请日：2010-08-02
申请人： Richard T. Hallen , Karl O. Albrecht , Heather M. Brown , James F. White
发明人： Richard T. Hallen , Karl O. Albrecht , Heather M. Brown , James F. White
IPC分类号： C10L1/16 , C07C27/00 , C07C1/00
CPC分类号： B01J23/6525 , B01J21/066 , B01J21/18 , B01J23/624 , B01J23/626 , B01J23/6527 , B01J37/0203 , B01J37/0205 , C10G3/44 , C10G3/47 , C10G3/48 , C10G2300/1014 , C10G2300/1018 , C10G2300/205 , C10G2300/4012 , C10G2300/4018 , C10G2300/4081 , C10G2300/44 , C10G2400/04 , C10G2400/08 , C10G2400/30 , C10L1/08 , C10L1/1208 , C10L2200/0469 , C10L2270/02 , C10L2270/04 , C11C3/00 , Y02E50/13 , Y02P30/20 , Y02T50/678
摘要： Embodiments of methods for making renewable diesel by deoxygenating (decarboxylating/decarbonylating/dehydrating) fatty acids to produce hydrocarbons are disclosed. Fatty acids are exposed to a catalyst selected from a) Pt and MO3 on ZrO2 (M is W, Mo, or a combination thereof), or b) Pt/Ge or Pt/Sn on carbon, and the catalyst decarboxylates at least 10% of the fatty acids. In particular embodiments, the catalyst consists essentially of 0.7 wt % Pt and 12 wt % WO3, relative to a mass of catalyst, or the catalyst consists essentially of a) 5 wt % Pt and b) 0.5 wt % Ge or 0.5 wt % Sn, relative to a mass of catalyst. Deoxygenation is performed without added hydrogen and at less than 100 psi. Disclosed embodiments of the catalysts deoxygenate at least 10% of fatty acids in a fatty acid feed, and remain capable of deoxygenating fatty acids for at least 200 minutes to more than 350 hours.
摘要翻译：公开了通过脱氧（脱羧/脱羰/脱水）脂肪酸制备可再生柴油以生产烃的方法的实施方案。将脂肪酸暴露于选自a）Pt和MO3的ZrO 2上的催化剂（M为W，Mo或其组合），或b）Pt / Ge或Pt / Sn在碳上，催化剂脱羧至少10％的脂肪酸。在具体实施方案中，催化剂相对于催化剂质量基本上由0.7重量％的Pt和12重量％的WO 3组成，或者催化剂基本上由a）5重量％的Pt和b）0.5重量％的Ge或0.5重量％的Sn ，相对于催化剂的质量。在不加入氢气的情况下进行脱氧，并且小于100psi。在脂肪酸进料中脱氧至少10％脂肪酸的催化剂的公开实施方案，并且能够使脂肪酸脱氧至少200分钟至超过350小时。

64. 发明授权

US07994347B2 Hydroxymethylfurfural reduction methods and methods of producing furandimethanol 有权
标题翻译：羟甲基糠醛还原方法和生产呋喃二甲醇的方法
公开(公告)号：US07994347B2
公开(公告)日：2011-08-09
申请号：US11760634
申请日：2007-06-08
申请人： Michael A. Lilga , Richard T. Hallen , Todd A. Werpy , James F. White , Johnathan E. Holladay , John G. Frye, Jr. , Alan H. Zacher
发明人： Michael A. Lilga , Richard T. Hallen , Todd A. Werpy , James F. White , Johnathan E. Holladay , John G. Frye, Jr. , Alan H. Zacher
IPC分类号： C07D307/02
CPC分类号： C07D307/42 , C07D307/46
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250° C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30° C. A method of producing tetrahydrofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。将H2置于反应器中，并使原料与含有至少一种选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh的金属的催化剂在小于或等于250的温度下接触氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性地氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

65. 发明授权

US07687661B2 Method for conversion of β-hydroxy carbonyl compounds 失效
标题翻译：转化羰基化合物的方法
公开(公告)号：US07687661B2
公开(公告)日：2010-03-30
申请号：US11377096
申请日：2006-03-15
申请人： Michael A. Lilga , James F. White , Johnathan E. Holladay , Alan H. Zacher , Danielle S. Muzatko , Rick J. Orth
发明人： Michael A. Lilga , James F. White , Johnathan E. Holladay , Alan H. Zacher , Danielle S. Muzatko , Rick J. Orth
IPC分类号： C07C67/30
CPC分类号： C07C51/377 , C07C51/41 , C07C57/04
摘要： A process is disclosed for conversion of salts of β-hydroxy carbonyl compounds forming useful conversion products including, e.g., α,β-unsaturated carbonyl compounds and/or salts of α,β-unsaturated carbonyl compounds. Conversion products find use, e.g., as feedstock and/or end-use chemicals.
摘要翻译：公开了用于转化形成有用的转化产物（例如α，b' - 不饱和羰基化合物和/或α，β-不饱和羰基化合物的盐的α-羟基羰基化合物的盐的方法。转化产物可用作例如原料和/或最终用途的化学品。

66. 发明授权

US07607275B2 Three-around cutting pattern for title roofing material 有权
标题翻译：标题屋顶材料三面切割图案
公开(公告)号：US07607275B2
公开(公告)日：2009-10-27
申请号：US11176599
申请日：2005-07-07
申请人： Bert W. Elliott , Meghan L. Howard , James F. White
发明人： Bert W. Elliott , Meghan L. Howard , James F. White
IPC分类号： E04B1/00 , E04G21/00 , E04G23/00
CPC分类号： E04D1/26 , B26D3/10 , B26D7/32 , B26D2007/322 , B65H39/10 , B65H2701/18265 , B65H2701/1922 , E04D2001/005 , Y10T156/1069 , Y10T428/24372
摘要： An apparatus and method for bundling shingles includes a sorting mechanism for separating and stacking shingles into multiple bundles of sorted shingles such that each bundle has a different repeating sequence of shingles.
摘要翻译：用于捆扎屋顶板的装置和方法包括：分拣机构，用于将带状疱for分离和堆叠成多个分类木瓦的束，使得每个束具有不同的重复序列的木瓦。

67. 发明申请

US20090186872A1 LOXAPINE ANALOGS AND METHODS OF USE THEREOF 有权
标题翻译： LOXAPINE ANALOGS及其使用方法
公开(公告)号：US20090186872A1
公开(公告)日：2009-07-23
申请号：US12411083
申请日：2009-03-25
申请人： Dale M. Edgar , David G. Hangauer , Kazumi Shiosaki , Michael Solomon , James F. White
发明人： Dale M. Edgar , David G. Hangauer , Kazumi Shiosaki , Michael Solomon , James F. White
IPC分类号： A61K31/553 , C07D413/04 , A61P25/00
CPC分类号： A61K31/553 , C07D267/20 , C07D413/12 , Y02A50/415
摘要： The invention relates to novel compounds and methods of using them for modulating sleep.
摘要翻译：本发明涉及新型化合物及其用于调节睡眠的方法。

68. 发明申请

US20090054694A1 Chemical production processes, systems, and catalyst compositions 审中-公开
标题翻译：化学生产过程，系统和催化剂组合物
公开(公告)号：US20090054694A1
公开(公告)日：2009-02-26
申请号：US11895593
申请日：2007-08-24
申请人： Thomas H. Peterson , Johnathan E. Holladay , Alan H. Zacher , Michel J. Gray , Todd A. Werpy , James F. White
发明人： Thomas H. Peterson , Johnathan E. Holladay , Alan H. Zacher , Michel J. Gray , Todd A. Werpy , James F. White
IPC分类号： C07C45/29
CPC分类号： C07C45/52 , C07C49/17 , C07C47/22
摘要： Chemical production processes are provided that include exposing a reactant composition to a catalyst composition to form a product composition, with the reactant composition including a multihydric alcohol compound and the catalyst composition being effective to dehydrate at least a portion of the multihydric alcohol compound. Embodiments of the process provide that the reactant composition is exposed to the catalyst composition for less than about 0.25 seconds and/or that the catalyst is maintained at a temperature of from about 280° C. to about 320° C. Processes utilizing a reactant composition including a multihydric alcohol compound and an inert compound are also provided.
摘要翻译：提供了化学生产方法，其包括将反应物组合物暴露于催化剂组合物以形成产物组合物，反应物组合物包含多元醇化合物，催化剂组合物有效地使至少一部分多元醇化合物脱水。该方法的实施方案提供反应物组合物暴露于催化剂组合物少于约0.25秒和/或催化剂保持在约280℃至约320℃的温度。利用反应物组合物还包括多元醇化合物和惰性化合物。

69. 发明申请

US20080152555A1 Staged alkylation in microchannels 有权
标题翻译：微通道分阶段烷基化
公开(公告)号：US20080152555A1
公开(公告)日：2008-06-26
申请号：US11973447
申请日：2007-10-09
申请人： Yong Wang , James F. White
发明人： Yong Wang , James F. White
IPC分类号： B01J8/04
CPC分类号： C10G29/205 , B01J19/0093 , B01J2219/00835 , B01J2219/00844 , B01J2219/00873 , B01J2219/00894 , C10G2300/1081 , C10G2300/1088 , C10G2300/1096 , C10G2300/4081 , C10G2400/02
摘要： The invention provides methods and systems for alkylating a paraffinic feed stream in a microchannel utilizing the staged addition of olefin.
摘要翻译：本发明提供了利用分阶段加入烯烃在微通道中烷基化链烷烃进料流的方法和系统。

70. 发明授权

US07326721B2 Doxepin analogs and methods of use thereof 失效
标题翻译：多塞平类似物及其使用方法
公开(公告)号：US07326721B2
公开(公告)日：2008-02-05
申请号：US11008891
申请日：2004-12-10
申请人： Dale M. Edgar , David G. Hangauer , James F. White , Michael Solomon
发明人： Dale M. Edgar , David G. Hangauer , James F. White , Michael Solomon
IPC分类号： A61K31/445 , C07D401/00
CPC分类号： C07D405/04 , A61K31/452 , A61K31/675
摘要： The invention relates to novel doxepin analog compounds and methods of modulating sleep by administering such compounds, or a pharmaceutically effective salt thereof.
摘要翻译：本发明涉及新的多虑平类似物化合物和通过施用这些化合物或其药学上有效的盐调节睡眠的方法。

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