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61. 发明授权

US5326877A Herbicidal substituted triazolinones 失效
标题翻译：除草取代的三唑啉酮
公开(公告)号：US5326877A
公开(公告)日：1994-07-05
申请号：US962442
申请日：1992-10-16
申请人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
发明人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
IPC分类号： A01N47/38 , C07D249/12 , C07D249/14 , C07D405/12
CPC分类号： C07D405/12 , A01N47/38 , C07D249/12
摘要： Herbicidally active substituted triazolinones of the formula ##STR1## in which R.sup.1 represents hydrogen, alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, alkoxyalkyl, cycloalkyl, cycloalkylalkyl, or represents tetrahydrofuranyl, tetrahydrofuranylalkyl, or represents in each case optionally substituted aralkyl or aryl,R.sup.2 represents hydrogen, alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, cyanoalkyl, hydroxyalkyl, alkoxyalkyl, alkoxycarbonylalkyl, alkoxycarbonylalkenyl, alkylaminoalkyl, dialkylaminoalkyl, or represents in each case optionally substituted cycloalkyl, cycloalkylalkyl, cycloalkenyl or cycloalkenylalkyl, or represents optionally substituted heterocyclylalkyl, or represents in each case optionally substituted aralkyl, aroyl, aryl, aralkyloxy or aryloxy, or represents alkoxy, alkenyloxy or alkinyloxy,X represents oxygen or sulphur andY represents oxygen or sulphur.New intermediates therefor are also shown.
摘要翻译：式（I）的除草活性取代的三唑啉酮，其中R 1表示氢，烷基，烯基，炔基，卤代烷基，卤代烯基，卤代烯基，烷氧基烷基，环烷基，环烷基烷基，或代表四氢呋喃基，四氢呋喃基烷基，或表示在各种情况下任选取代芳烷基或芳基，R 2表示氢，烷基，烯基，炔基，卤代烷基，卤代烯基，卤代烷基，氰基烷基，羟基烷基，烷氧基烷基，烷氧基羰基烷基，烷氧基羰基烯基，烷基氨基烷基，二烷基氨基烷基，或在每种情况下表示任选取代的环烷基，环烷基烷基，环烯基或环烯基烷基，或或者表示任意取代的芳烷基，芳酰基，芳基，芳烷氧基或芳氧基，或表示烷氧基，烯氧基或烷氧基，X表示氧或硫，Y表示氧或硫。还显示了其新的中间体。

62. 发明授权

US5310849A Amino and ammonium isocyanates, a process for their preparation, their use for the production of polymers containing ammonium groups and the polymers thus produced 失效
标题翻译：氨基和铵异氰酸酯，其制备方法，它们用于生产含铵基团的聚合物和由此制备的聚合物的用途
公开(公告)号：US5310849A
公开(公告)日：1994-05-10
申请号：US875622
申请日：1992-04-28
申请人： Hans-Josef Buysch , Klaus Konig , Alexander Klausener , Klaus Szablikowski , Jorn Breckwoldt
发明人： Hans-Josef Buysch , Klaus Konig , Alexander Klausener , Klaus Szablikowski , Jorn Breckwoldt
IPC分类号： C07D295/12 , C07C263/06 , C07C263/16 , C07C265/04 , C07D295/185 , C08G18/08 , C08G18/71 , C08G18/70
CPC分类号： C07D295/185 , C07C265/04 , C08G18/0814 , C08G18/714
摘要： The present invention relates to new amino and ammonium isocyanates, to a process for their preparation, e.g. by the reaction of certain ureas with isocyanates, and to the use of the new substances for the production of polymers containing ammonium groups.
摘要翻译：本发明涉及新的氨基和铵异氰酸酯，其制备方法，例如通过某些脲与异氰酸酯的反应，以及使用这些新物质来生产含铵基团的聚合物。

63. 发明授权

US5300480A Herbicidal sulphonylaminocarbonyltriazolinones having two substituents bonded via oxygen 失效
标题翻译：具有通过氧键连接的两个取代基的除草磺酰基氨基羰基三唑啉酮
公开(公告)号：US5300480A
公开(公告)日：1994-04-05
申请号：US945194
申请日：1992-09-15
申请人： Wilhelm Haas , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
发明人： Wilhelm Haas , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
IPC分类号： A01N47/38 , A01N51/00 , C07D249/12 , C07D249/14 , C07D401/12 , C07D403/12 , C07D405/12 , C07D409/12 , C07D471/04 , C07D487/04 , A01N43/653
CPC分类号： C07D401/12 , A01N47/38 , A01N51/00 , C07D249/12 , C07D249/14 , C07D403/12 , C07D405/12 , C07D409/12 , C07D471/04 , C07D487/04
摘要： Herbicidal sulphonylaminocarbonyltriazolinones having two substituents bonded via oxygen, of the formula ##STR1## in which R.sup.1 represents hydrogen or an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkenyl and aralkyl,R.sup.2 represents an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkenyl and aralkyl, andR.sup.3 represents an optionally substituted radical from the series comprising alkyl, aralkyl, aryl and heteroaryl,and their salts.
摘要翻译：具有式（*化学结构*）（I）的两个通过氧键键合的取代基的磺酰基氨基羰基三唑啉酮，其中R 1表示氢或任选取代的基团，其包含烷基，烯基，炔基，环烷基，环烯基和芳烷基，R2表示烷基，烯基，炔基，环烷基，环烯基和芳烷基的任选被取代的基团，并且R 3代表包含烷基，芳烷基，芳基和杂芳基及其盐的任选取代的基团。

64. 发明授权

US5153326A Preparation of 4-amino-1,2,4-triazol-5-ones 失效
标题翻译：制备4-氨基-1,2,4-三唑-5-酮
公开(公告)号：US5153326A
公开(公告)日：1992-10-06
申请号：US690028
申请日：1991-04-23
申请人： Klaus Konig , Klaus-Helmut Muller , Lothar Rohe
发明人： Klaus Konig , Klaus-Helmut Muller , Lothar Rohe
IPC分类号： C07D249/12
CPC分类号： C07D249/12
摘要： A process for the preparation of 4-amino-1,2,4-triazol-5-one of the formula ##STR1## in which R represents unsubstituted or substituted alkyl, alkenyl, cycloalkenyl, cycloalkyl, aralkyl, aryl or heterocyclyl,which comprises reacting a carbodihydrazide of the formula ##STR2## with a nitrile of the formulaR--C.tbd.N (III)The carbodihydrazide of the formula (II) may be produced in a preliminary stage by reacting a carbonic acid derivative with hydrazine or hydrazine hydrate.
摘要翻译：制备式（I）的4-氨基-1,2,4-三唑-5-酮的方法，其中R表示未取代或取代的烷基，烯基，环烯基，环烷基，芳烷基，芳基或杂环基，其包括使式（II）的碳二酰肼与式RC 3BOND N（III）的腈反应。式（II）的碳二酰肼可以通过使碳酸衍生物与肼反应而在预备阶段中制备或水合肼。

65. 发明授权

US5115073A Rapidly crystallizing polyurethane systems 失效
标题翻译：快速结晶聚氨酯系统
公开(公告)号：US5115073A
公开(公告)日：1992-05-19
申请号：US580717
申请日：1990-09-11
申请人： Walter Meckel , Eduard Hansel , Gu Arend , Klaus Konig
发明人： Walter Meckel , Eduard Hansel , Gu Arend , Klaus Konig
IPC分类号： C08G18/08 , C08G18/12 , C08G18/42 , C08G18/65 , C08G18/66 , C09J5/06 , C09J175/00 , C09J175/06
CPC分类号： C09J175/06 , C08G18/0804 , C08G18/12 , C08G18/4202 , C08G18/664 , C08G2170/20 , C08G2250/00
摘要： The present invention is directed to a polyurethane system containing isocyanate groups prepared by reactingA) 70 to 98 parts by weight of at least one polyester diol having a melting point of 30.degree. C. to 60.degree. C. and a molecular weight of 800 to 8,000,B) 2 to 30 parts by weight of at least one polyester diol having a melting point of 65.degree. C. to 150.degree. C. and a molecular weight of 600 to 8,000, andC) no more than 1 mole of a diol having a molecular weight of less than 600 per moles of A) plus B), with,D) at least one organic polyisocyanate, the ratio of isocyanate groups to hydroxyl groups is between 3:1 and 1.2:1.
摘要翻译：本发明涉及含有异氰酸酯基团的聚氨酯体系，其通过使A）70〜98重量份的至少一种熔点为30℃〜60℃，分子量为800〜 8,000，B）2〜30重量份的至少一种聚酯二醇，其熔点为65℃至150℃，分子量为600至8,000，C）不超过1摩尔的二醇具有小于600摩尔A）+ B）的分子量，D）至少一种有机多异氰酸酯，异氰酸酯基与羟基的比例在3:1至1.2:1之间。

66. 发明授权

US5082490A Herbicidal substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones 失效
标题翻译：除草剂取代4,5-二氨基-1,2,4-三唑-3-（THI）
公开(公告)号：US5082490A
公开(公告)日：1992-01-21
申请号：US565293
申请日：1990-08-09
申请人： Klaus-Helmut Muller , Kurt Findeisen , Michael Haug , Ulrich Heinemann , Joachim Kluth , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
发明人： Klaus-Helmut Muller , Kurt Findeisen , Michael Haug , Ulrich Heinemann , Joachim Kluth , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
IPC分类号： A01N47/38 , C07C281/06 , C07D249/12 , C07D249/14 , C07D403/12 , C07D405/12 , C07D413/12
CPC分类号： C07D405/12 , A01N47/38 , C07C281/06 , C07D249/14 , C07C2101/02
摘要： Herbicidal substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones of the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4 and R.sup.5 each independently is hydrogen or an organic radical,X is O or S, andY is O or S.
摘要翻译：式（Ⅰ）中除草取代的4,5-二氨基-1,2,4-三唑-3-（thi），其中R 1，R 2，R 3，R 4和R 5各自独立地为氢或有机基团 X是O或S，Y是O或S.

67. 发明授权

US5034538A Preparation of 4-amino-1,2,4-triazol-5-ones 失效
标题翻译：制备4-氨基-1,2,4-三唑-5-酮
公开(公告)号：US5034538A
公开(公告)日：1991-07-23
申请号：US534402
申请日：1990-06-06
申请人： Klaus Konig , Klaus-Helmut Muller , Lothar Rohe
发明人： Klaus Konig , Klaus-Helmut Muller , Lothar Rohe
IPC分类号： C07D249/12 , C07D249/14 , C07D401/04 , C07D409/04
CPC分类号： C07D249/12
摘要： A process for the preparation of 4-amino-1,2,4-triazol-5-one of the formula ##STR1## in which p0 R represents unsubstituted or substituted alkyl, alkenyl, cycloalkenyl, cycloalkyl, aralkyl, aryl or heterocyclyl,which comprises reacting a carbodihydrazide of the formula ##STR2## with a nitrile of the formulaR--C.tbd.N (II)The carbodihydrazide of the formula (II) may be produced in a preliminary stage by reacting a carbonic acid derivative with hydrazine or hydrazine hydrate.
摘要翻译：制备式（Ⅰ）的4-氨基-1,2,4-三唑-5-酮的方法，其中pO R表示未取代或取代的烷基，烯基，环烯基，环烷基，芳烷基，芳基或杂环基，其包括使式II（II）的碳二酰肼与式RC 3BOND N（II）的腈反应。式（II）的碳二酰肼可以在预备阶段通过使碳酸衍生物与肼或水合肼。

68. 发明授权

US4952701A Preparation of 4-amino-1,2,4-triazol-5-ones 失效
标题翻译：制备4-氨基-1,2,4-三唑-5-酮
公开(公告)号：US4952701A
公开(公告)日：1990-08-28
申请号：US284965
申请日：1988-12-15
申请人： Klaus-Helmut Muller , Klaus Konig , Peter Heitkamper
发明人： Klaus-Helmut Muller , Klaus Konig , Peter Heitkamper
IPC分类号： C07D249/12 , C07D271/10
CPC分类号： C07D249/12
摘要： A process for the preparation of 4-amino-1,2,4-triazol-5-one of the formula ##STR1## in which R is alkyl, comprising in a first step reacting phosgene with an acylhydrazide of the formula ##STR2## to produce an oxadiazolinone of the formula ##STR3## and in a second step reacting the oxadiazolinone with hydrazine hydrate.
摘要翻译：制备式（Ⅰ）的4-氨基-1,2,4-三唑-5-酮的方法，其中R是烷基，该方法包括在第一步中将光气与下式的酰基酰肼反应：（II）制备式（III）的恶二唑啉酮，第二步使恶二唑啉酮与水合肼反应。

69. 发明授权

US4803246A Process for the preparation of polymers containing hydroxyl groups and their use for the production of polyurethanes 失效
标题翻译：制备含羟基聚合物的方法及其用于生产聚氨酯的方法
公开(公告)号：US4803246A
公开(公告)日：1989-02-07
申请号：US849649
申请日：1986-04-09
申请人： Manfred Dietrich , Josef Pedain , Klaus Konig , Peter Hohlein
发明人： Manfred Dietrich , Josef Pedain , Klaus Konig , Peter Hohlein
IPC分类号： C08G18/00 , C08F8/00 , C08F8/14 , C08G18/62 , C08L75/00
CPC分类号： C08F8/14 , C08G18/6258
摘要： The present invention is directed to a process for the preparation of polymers containing hydroxyl groups by reacting polymers based on acrylic acid and/or methacrylic acid and containing carboxyl groups with alkylene oxides in the presence of catalysts, characterized in that the catalysts used are(a) addition products containing two thioether groups of (i) mercaptoalkanols corresponding to the formula ##STR1## and (ii) doubly unsaturated terpene hydrocarbons and/or condensation products with a maximum molecular weight of 5000 obtained by the condensation of such addition products on their own or with other polyhydric alcohols having a molecular weight of 62 to about 200, and/or(b) relatively high molecular weight thioethers having a molecular weight of about 500 to 5000 obtainable by the condensation of thiodiglycols corresponding to the formula ##STR2## optionally in admixture with up to 50 hydroxyl equivalents percent, based on the total mixture, of other polyhydroxyl compounds having a molecular weight of 62 to about 200, in which formula, R and R' may be identical or different and denote hydrogen or a methyl group.The present invention is further directed to the use of the hydroxyl containing alkoxylation products obtained by this process as reactants for organic polyisocyanates (optionally blocked with blocking agents for isocyanate groups) in the production of polyurethane plastics, in particular high quality polyurethane coatings.
摘要翻译：本发明涉及一种通过在催化剂存在下，通过使基于丙烯酸和/或甲基丙烯酸的聚合物与烯化氧反应的聚合物制备含羟基的聚合物的方法，其特征在于所用的催化剂是（a ）含有两个硫醚基团的加成产物（i）对应于式“IMAGE”的巯基链烷醇和（ii）通过自身缩合产生的双不饱和萜烯烃和/或最大分子量为5000的缩合产物或分子量为62至约200的其它多元醇，和/或（b）分子量为约500至5000的相对较高分子量的硫醚，其可通过任选地在式与其他多羟基化合物的混合物混合至多50个羟基当量百分比分子量为62至约200，其中R和R'可以相同或不同，表示氢或甲基。本发明还涉及通过该方法获得的含羟基烷氧基化产物作为有机多异氰酸酯的反应物（任选地用异氰酸酯基团的封闭剂封端）用于生产聚氨酯塑料，特别是高质量聚氨酯涂料中的用途。

70. 发明授权

US4386033A Process for the continuous thermal cleavage of carbamic acid esters and preparation of isocyanates from the products thereof 失效
标题翻译：用于连续热裂解氨基甲酸酯的方法和由其产物制备异氰酸酯
公开(公告)号：US4386033A
公开(公告)日：1983-05-31
申请号：US331412
申请日：1981-12-16
申请人： Klaus Konig , Peter Heitkamper
发明人： Klaus Konig , Peter Heitkamper
IPC分类号： B01J23/06 , B01J27/08 , B01J31/02 , B01J31/04 , B01J31/12 , C07B61/00 , C07C27/00 , C07C29/00 , C07C29/147 , C07C31/02 , C07C31/13 , C07C33/18 , C07C35/02 , C07C37/00 , C07C67/00 , C07C241/00 , C07C263/04 , C07C263/12 , C07C265/00 , C07C265/04 , C07C265/06 , C07C265/10 , C07C265/12 , C07C271/06 , C07C118/00
CPC分类号： C07C263/04 , C07C2101/14 , Y02P20/582
摘要： A carbamic acid ester corresponding to the formula R.sup.1 --NH--CO--OR.sup.2 is thermally cleaved to form isocyanate R.sup.1 --NCO and alcohol R.sup.2 --OH fractions. This cleavage is accomplished by boiling the carbamic acid ester, condensing the vapor given off in a first fractionation column, and condensing the vapor from the first fractionation column in a second fractionation column. The boiling of the carbamic acid ester is carried out in a manner such that the average dwell time in the reaction vessel is from 1 to 20 hours, the temperature is from 160.degree. to 260.degree. C. and the pressure is from 0.001 to 2 bar. The isocyanate fraction obtained by this cleavage process may be used as a starting material for a transurethanation reaction in which a lower boiling isocyanate R.sup.3 --NCO is produced. The radicals R.sup.1, R.sup.2, and R.sup.3 are defined herein.
摘要翻译：将对应于式R 1 -NH-CO-OR 2的氨基甲酸酯热裂解形成异氰酸酯R 1 -NCO和醇R 2 -OH部分。该裂解是通过沸腾氨基甲酸酯，将在第一分馏塔中排出的蒸气冷凝，并在第二分馏塔中将来自第一分馏塔的蒸气冷凝来完成的。氨基甲酸酯的沸腾以使得反应容器中的平均停留时间为1〜20小时，温度为160〜260℃，压力为0.001〜2巴的方式进行。通过该裂解方法得到的异氰酸酯部分可以用作产生低沸点异氰酸酯R 3 -NCO的经反氨化反应的原料。基团R 1，R 2和R 3在本文中定义。

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