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61. 发明申请

US20070270597A1 Process for preparing maleic anhydride in a microchannel reactor 审中-公开
标题翻译：在微通道反应器中制备马来酸酐的方法
公开(公告)号：US20070270597A1
公开(公告)日：2007-11-22
申请号：US11798707
申请日：2007-05-16
申请人： Hagen Wilmer , Torsten Maurer , Frank Rosowski , Rudolf Schuch
发明人： Hagen Wilmer , Torsten Maurer , Frank Rosowski , Rudolf Schuch
IPC分类号： C07D307/34
CPC分类号： C07D307/34
摘要： The present invention relates to a process for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon, which comprises feeding a hydrocarbon-comprising stream and a stream comprising oxygen or an oxygen source into a microchannel reactor and carrying out the reaction to form maleic anhydride in the explosive range in the microchannel reactor comprising the catalyst.
摘要翻译：本发明涉及通过烃的非均相催化气相氧化制备马来酸酐的方法，该方法包括将包含烃的料流和包含氧或氧源的物流进入微通道反应器并进行反应以形成在包含催化剂的微通道反应器的爆炸范围内的马来酸酐。

62. 发明授权

US07134848B2 Pump for transporting heat-exchange medium for a multi-tube reactor 有权
标题翻译：用于输送多管反应器的热交换介质的泵
公开(公告)号：US07134848B2
公开(公告)日：2006-11-14
申请号：US10479625
申请日：2002-06-05
申请人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Rühl , Frank Rosowski
发明人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Rühl , Frank Rosowski
IPC分类号： G21C19/04
CPC分类号： F04D3/00 , F04D29/406
摘要： The invention relates to a pump (1) having a pump guide tube (13) for the transport of a heat-exchange medium (6) for a reactor having a bundle of catalyst tubes (2), where the pump (1) has a casing (14) which surrounds the pump guide tube (13), having an aperture (15) in the lower part of the casing (14) via which the heat-exchange medium (6) discharged from the lower region of the reactor by means of the pump (1) flows into the casing (14), flows upward in the region between the inner wall of the casing (14) and the outer wall of the pump guide tube (13), if desired via a heat exchanger (18), flows into the interior of the pump guide tube (13) via an aperture (16) in the upper region of the pump guide tube (13), flows through the pump guide tube (13) from top to bottom and flows via an aperture (17) in the lower region of the pump guide tube (13) into the reactor, into the upper region of the interspace between the catalyst tubes (2).
摘要翻译：本发明涉及一种具有泵引导管（13）的泵（1），用于输送用于具有一束催化剂管（2）的反应器的热交换介质（6），其中泵（1）具有围绕所述泵引导管（13）的壳体（14），在所述壳体（14）的下部具有孔（15），所述热交换介质（6）经由所述开口（15）从所述反应器的下部区域排出，如果需要，通过热交换器（18）将泵（1）流入壳体（14）中，在壳体（14）的内壁和泵引导管（13）的外壁之间的区域中向上流动）通过泵引导管（13）的上部区域中的孔（16）流入泵引导管（13）的内部，从上到下流过泵引导管（13），并经由在泵引导管（13）的下部区域中的孔（17）进入反应器，进入催化剂管（2）之间的间隙的上部区域。

63. 发明授权

US06781017B2 Method for the production of acrolein or acrylic acid or the mixture thereof from propane 有权
标题翻译：从丙烷生产丙烯醛或丙烯酸或其混合物的方法
公开(公告)号：US06781017B2
公开(公告)日：2004-08-24
申请号：US10297602
申请日：2002-12-13
申请人： Otto Machhammer , Goetz-Peter Schindler , Andreas Tenten , Klaus Harth , Peter Zehner , Klaus Joachim Müller-Engel , Frank Rosowski , Frieder Borgmeier
发明人： Otto Machhammer , Goetz-Peter Schindler , Andreas Tenten , Klaus Harth , Peter Zehner , Klaus Joachim Müller-Engel , Frank Rosowski , Frieder Borgmeier
IPC分类号： C07C4500
CPC分类号： C07C51/215 , C07C5/333 , C07C45/33 , C07C45/35 , C07C51/252 , C07C11/06 , C07C47/22 , C07C57/04
摘要： In a process for the preparation of acrolein or acrylic acid or a mixture thereof from propane, the propane is subjected, in a first reaction stage, to a partial dehydrogenation under heterogeneous catalysis to give propene, of the components contained in the product gas mixture formed in the first reaction stage other than propene and propane at least a portion of the molecular hydrogen present is then separated off from said mixture and the product gas mixture is then used for the preparation of acrolein and/or acrylic acid by gas-phase catalytic propylene oxidation, molecular nitrogen being present for diluting the reaction gas mixture during the propylene oxidation.
摘要翻译：在从丙烷制备丙烯醛或丙烯酸或其混合物的方法中，丙烷在第一反应阶段中在非均相催化下进行部分脱氢以形成产物气体混合物中所含组分的丙烯在除丙烯和丙烷之外的第一反应阶段中，存在的分子氢的至少一部分然后从所述混合物中分离出来，然后将产物气体混合物用于通过气相催化丙烯制备丙烯醛和/或丙烯酸存在氧化，分子氮，用于在丙烯氧化期间稀释反应气体混合物。

64. 发明授权

US08901320B2 Process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride 有权
标题翻译：控制气相氧化反应器制备邻苯二甲酸酐的方法
公开(公告)号：US08901320B2
公开(公告)日：2014-12-02
申请号：US13085537
申请日：2011-04-13
申请人： Stefan Altwasser , Jürgen Zühlke , Hao Chen , Cornelia Katharina Dobner , Frank Rosowski
发明人： Stefan Altwasser , Jürgen Zühlke , Hao Chen , Cornelia Katharina Dobner , Frank Rosowski
IPC分类号： C07D307/89
CPC分类号： C07D307/89
摘要： In a process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride, by passing a gas stream which comprises an aromatic hydrocarbon and molecular oxygen through a multitude of reaction tubes arranged in the gas phase oxidation reactor, each of which comprises a bed of at least one catalyst and the temperature of which can be controlled by means of a heat transfer medium, at least one control parameter is measured and correcting interventions for control of the control parameter are determined, the at least one control parameter comprising the phthalic anhydride yield and the correcting parameter used being the temperature of the heat carrier medium. Over at least 90% of the lifetime of the catalyst, the change in the correcting parameter is limited to a maximum of 0.5 K within a period of 30 days. In this way, the cumulated phthalic anhydride yield over the lifetime of the catalyst is maximized.
摘要翻译：在控制用于制备邻苯二甲酸酐的气相氧化反应器的方法中，通过将包含芳族烃和分子氧的气流通过布置在气相氧化反应器中的多个反应管通过，每个反应管包括一个床至少一种催化剂，其温度可以通过传热介质控制，测量至少一个控制参数，并且确定用于控制控制参数的校正干预，所述至少一个控制参数包括邻苯二甲酸酐产率并且所使用的校正参数是热载体介质的温度。在催化剂寿命的至少90％之内，校正参数的变化在30天的时间内被限制为最大0.5K。以这种方式，在催化剂寿命期间累积的邻苯二甲酸酐产率最大化。

65. 发明申请

US20140213801A1 MULTILAYER CATALYST HAVING VANADIUM ANTIMONATE IN AT LEAST ONE CATALYST LAYER FOR PREPARING CARBOXYLIC ACIDS AND/OR CARBOXYLIC ANHYDRIDES AND PROCESS FOR PREPARING PHTHALIC ANHYDRIDE HAVING A LOW HOT SPOT TEMPERATURE 审中-公开
标题翻译：用于制备碳羧酸和/或羧酸酐的至少一种催化剂层中的抗氧化剂的多层催化剂和用于制备具有低热点温度的苯基氢醌的方法
公开(公告)号：US20140213801A1
公开(公告)日：2014-07-31
申请号：US14242979
申请日：2014-04-02
申请人： Stefan Altwasser , Jürgen Zühlke , Frank Rosowski , Cornelia Katharina Dobner
发明人： Stefan Altwasser , Jürgen Zühlke , Frank Rosowski , Cornelia Katharina Dobner
IPC分类号： C07D307/89
CPC分类号： C07D307/89 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/53 , B01J2523/55
摘要： The present invention relates to a catalyst system for preparing carboxylic acids and/or carboxylic anhydrides, which system comprises a plurality of superposed catalyst layers arranged in a reaction tube, where vanadium antimonate is introduced into the active material in at least one of the catalyst layers. The present invention further relates to a process for gas-phase oxidation, in which a gaseous stream comprising at least one hydrocarbon and molecular oxygen is passed through a plurality of catalyst layers and the maximum hot spot temperature is below 425° C.
摘要翻译：本发明涉及一种用于制备羧酸和/或羧酸酐的催化剂体系，该系统包括布置在反应管中的多个重叠的催化剂层，其中锑酸锑在至少一个催化剂层中被引入到活性材料中。本发明还涉及一种用于气相氧化的方法，其中包含至少一种烃和分子氧的气流通过多个催化剂层，最大热点温度低于425℃。

66. 发明授权

US08580982B2 Use of structured catalyst beds for preparing ethylene oxide 有权
标题翻译：使用结构化催化剂床制备环氧乙烷
公开(公告)号：US08580982B2
公开(公告)日：2013-11-12
申请号：US13376879
申请日：2010-06-09
申请人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
发明人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
IPC分类号： C07D301/03
CPC分类号： C07D301/10
摘要： The present invention relates to a process for preparing ethylene oxide by reaction of ethylene with oxygen in the presence of at least one silver-comprising catalyst, wherein the reaction takes place in a reactor which has a catalyst packed bed having at least two zones (i) and (ii) and the silver content of the catalyst in zone (i) is lower than the silver content of the catalyst in zone (ii). The catalyst packed bed preferably has a further zone (a) with which the reaction mixture comes into contact before the zones (i) and (ii). According to the invention, the silver content of the catalyst in the zone (a) is higher than the silver content of the catalyst in zone (i).
摘要翻译：本发明涉及通过乙烯与氧在至少一种含银催化剂存在下反应来制备环氧乙烷的方法，其中该反应在具有至少两个区域的催化剂填充床（i ）和（ii），并且（i）区域中的催化剂的银含量低于区域（ii）中的催化剂的银含量。催化剂填充床优选具有另外的区域（a），反应混合物在区域（i）和（ii）之前与其接触。根据本发明，区域（a）中催化剂的银含量高于区域（i）中催化剂的银含量。

67. 发明授权

US08492566B2 Method for starting a gas-phase oxidation reactor 有权
标题翻译：启动气相氧化反应器的方法
公开(公告)号：US08492566B2
公开(公告)日：2013-07-23
申请号：US12936807
申请日：2009-04-07
申请人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Katharina Dobner
发明人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Katharina Dobner
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , C07D307/89
摘要： What is described is a process for starting up a gas phase oxidation reactor for oxidation of o-xylene to phthalic anhydride, said reactor comprising at least one catalyst layer and being temperature-controllable by means of a heat carrier medium, wherein a) the catalyst layer is interrupted by a moderator layer which is less catalytically active than the catalyst layer or is catalytically inactive, b) a gas stream is passed through the reactor with an initial loading of o-xylene and at an initial temperature of the heat transfer medium, c) the loading of the gas stream is increased to a target loading and, in parallel, the temperature of the heat transfer medium is lowered to an operating temperature. The introduction of the moderator layer allows the loading to be increased more rapidly and the startup time to be shortened.
摘要翻译：描述的是用于启动用于将邻二甲苯氧化成邻苯二甲酸酐的气相氧化反应器的方法，所述反应器包括至少一个催化剂层，并且可通过热载体介质温度控制，其中a）催化剂层被催化剂层催化活性较低或催化无活性的中间体层中断，b）气流以邻二甲苯的初始负荷和传热介质的初始温度通过反应器， c）将气流的负载增加到目标负载，并且并联地将传热介质的温度降低到工作温度。调节器层的引入允许加载更快速并且启动时间被缩短。

68. 发明申请

US20130123517A1 SILVER VANADIUM PHOSPHATES 审中-公开
标题翻译：银芒果磷酸盐
公开(公告)号：US20130123517A1
公开(公告)日：2013-05-16
申请号：US13672855
申请日：2012-11-09
申请人： Andrey Karpov , Cornelia Katharina Dobner , Frank Rosowski , Patrick Hubach , Robert Glaum , Stephan Schunk , Gerhard Cox
发明人： Andrey Karpov , Cornelia Katharina Dobner , Frank Rosowski , Patrick Hubach , Robert Glaum , Stephan Schunk , Gerhard Cox
IPC分类号： B01J27/198 , C07D307/60
CPC分类号： B01J27/198 , B01J23/002 , B01J35/002 , B01J35/1009 , B01J35/1014 , B01J37/0036 , B01J37/0045 , B01J37/009 , B01J37/08 , B01J37/14 , B01J37/16 , B01J2523/00 , C07D307/60 , B01J2523/18 , B01J2523/51 , B01J2523/55
摘要： The invention relates to novel silver vanadium phosphates, catalysts based on these silver vanadium phosphates and the use of these catalysts for carrying out organic reactions in the gas phase.
摘要翻译：本发明涉及新的银钒磷酸盐，基于这些银钒磷酸盐的催化剂以及这些催化剂在气相中进行有机反应的用途。

69. 发明申请

US20120308840A1 FORMULATION AND USE THEREOF 审中-公开
标题翻译：配方及其用途
公开(公告)号：US20120308840A1
公开(公告)日：2012-12-06
申请号：US13518768
申请日：2010-12-13
申请人： Michael Maier , Jörg Habicht , Alexander Kraus , Andrey Karpov , Frank Rosowski , Frank Müller
发明人： Michael Maier , Jörg Habicht , Alexander Kraus , Andrey Karpov , Frank Rosowski , Frank Müller
IPC分类号： A01N59/20 , B32B21/00 , A01P3/00 , A01N25/04 , A01P7/04 , A01N59/26
CPC分类号： A01N59/20 , A01N25/04 , A01N25/30 , A01N43/653 , B27K3/15 , C08K3/30 , C08L61/28 , C08L61/34 , C08L97/02 , Y10T428/662
摘要： A formulation is claimed, which contains at least one protective substance that is active with respect to cellulose-containing materials, such as wood-containing building materials in the form of solid wood or wood-based materials, and at least one specific compound with dispersing properties. The dispersants are branched comb-shaped polymers with polyether side chains, naphthalene-sulfonate-formaldehyde condensation products, melamine-sulfonate-formaldehyde condensation products and phosphatized polycondensation products. The formulations according to the invention are suitable in particular as plant protection agents and wood preservatives and are preferably used in the form of suspensions for pressure treatment of the respective building materials.
摘要翻译：要求保护的物质包含至少一种相对于含纤维素的材料具有活性的保护性物质，例如实木或木质材料形式的含木材建筑材料，以及至少一种具有分散性的特定化合物属性。分散剂是具有聚醚侧链的支链梳状聚合物，萘磺酸盐 - 甲醛缩合产物，三聚氰胺 - 磺酸 - 甲醛缩合产物和磷酸化缩聚产物。根据本发明的制剂特别适用于植物保护剂和木材防腐剂，并且优选以用于各种建筑材料的压力处理的悬浮液的形式使用。

70. 发明申请

US20120149919A1 MALEIC ANHYDRIDE SYNTHESIS CATALYST PRECURSOR AND PROCESS FOR ITS PREPARATION 审中-公开
标题翻译：马来酸酐合成催化剂前体及其制备方法
公开(公告)号：US20120149919A1
公开(公告)日：2012-06-14
申请号：US13391958
申请日：2010-08-23
申请人： Stefan Altwasser , Cornelia Katharina Dobner , Hagen Wilmer , Frank Rosowski
发明人： Stefan Altwasser , Cornelia Katharina Dobner , Hagen Wilmer , Frank Rosowski
IPC分类号： B01J27/198 , C07D307/60 , C01B25/37
CPC分类号： B01J27/198 , B01J23/002 , B01J35/002 , B01J35/023 , B01J35/026 , B01J37/0009 , B01J37/031 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C57/145 , B01J2523/51 , B01J2523/55
摘要： A process for preparing a vanadium, phosphorus, and oxygen comprising catalyst precursor for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon having at least four carbon atoms, which comprises (a) reacting vanadium pentoxide with 102% to 110% strength phosphoric acid in the presence of isobutanol and optionally of a primary or secondary, noncyclic or cyclic, unbranched or branched, saturated alcohol having 3 to 6 carbon atoms in a temperature range from 80 to 160° C.; (b) isolating the precipitate formed; (c) (i) drying the isolated precipitate down to a residual isobutanol content of less than 5% by weight; (ii) then passing a gas which in addition to one or more inert gases comprises 0.1% to 9% by volume of oxygen through the dried precipitate, directly or after isolation, in the temperature range from 130° C. to 200° C.
摘要翻译：一种制备钒，磷和氧的方法，包括通过异构催化气相氧化具有至少四个碳原子的烃来制备马来酸酐的催化剂前体，其包括（a）五氧化二钒与102％至110％的强度磷酸在异丁醇存在下和任选的在80至160℃的温度范围内具有3至6个碳原子的伯或仲，非环或环状，无支链或支链的饱和醇。（b）分离形成的沉淀物; （c）（i）将分离的沉淀物干燥至低于5重量％的残余异丁醇含量; （ii）然后在130℃至200℃的温度范围内直接或分离后通过除一种或多种惰性气体外还含有0.1％至9％（体积）氧气的气体。

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