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61. 发明授权

US07169598B2 Polyhydroxyalkanoate, method for production thereof and microorganisms for use in the same 失效
标题翻译：聚羟基链烷酸酯，其制备方法和用于其的微生物
公开(公告)号：US07169598B2
公开(公告)日：2007-01-30
申请号：US10649646
申请日：2003-08-28
申请人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
发明人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
IPC分类号： C12N1/20
CPC分类号： C12P7/62 , C08G63/06 , C08G63/6822 , C08G63/6852 , Y10S435/874
摘要： A polyhydroxyalkanoate having a monomer unit composition represented by General Formula (1): AmB(1-m) (1) wherein A is represented by General Formula (2), B is at least one selected from the group consisting of monomer units represented by General Formula (3) or (4), and m has a value of 0.01 or larger and smaller than 1: wherein n has a value of 0 to 10, k has a value of 3 or 5, and R is at least one group selected from the group consisting of groups represented by General Formulae (5) to (7): in Formula (5) R1 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5. and —C3F7; and q is an integer selected from 1 to 8; in Formula (6) R2 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and r is an integer selected from 1 to 8; in Formula (7) R3 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and s is an integer selected from 1 to 8. The efficient production methods are also provided.
摘要翻译：具有由通式（1）表示的单体单元组成的聚羟基链烷酸酯：<？in-line-formula description =“In-line Formulas”end =“lead”？> A （1-m）（1）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中A由通式（2）表示，B为至少一个选自由通式（3）或（4）表示的单体单元组，并且m具有0.01以上且小于1的值：其中n具有0至10的值，k的值为3 或5，并且R是选自由通式（5）至（7）表示的基团中的至少一个基团：在式（5）中，R 1是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 H 5。和-C 3 N 3 R 7; q为选自1至8的整数; 在式（6）中，R 2是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3， C 2 F 5和-C 3 F 7; 并且r是选自1至8的整数; 在式（7）中，R 3是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3 N， C 2 F 5和-C 3 F 7; s是选自1至8的整数。还提供了有效的制备方法。

62. 发明授权

US07135540B2 Polyhydroxyalkanoate copolymer including unit having bromo group in side chain and method for producing the same 失效
标题翻译：聚羟基链烷酸酯共聚物，包括在侧链中具有溴基的单元及其制备方法
公开(公告)号：US07135540B2
公开(公告)日：2006-11-14
申请号：US10359600
申请日：2003-02-07
申请人： Tsutomu Honma , Shinya Kozaki , Takeshi Imamura , Takashi Kenmoku , Tatsuki Fukui , Etsuko Sugawa , Tetsuya Yano
发明人： Tsutomu Honma , Shinya Kozaki , Takeshi Imamura , Takashi Kenmoku , Tatsuki Fukui , Etsuko Sugawa , Tetsuya Yano
IPC分类号： C08G63/02
CPC分类号： C12P7/625 , C08G63/6822 , C08G63/6882 , C12P11/00
摘要： The invention provides a polyhydroxyalkanoate having a bromo group in a unit and being thermally stable and capable of arbitrarily controlling physical properties, and a producing method thereof. According to the invention, there are provided a polyhydroxyalkanoate copolymer including a 3-hydroxy-ω-bromoalkanoic acid unit represented by a formula—[OCH((CH2)nBr)CH2C(O)]— (n=1 to 8) (1) and a unit represented by a formula —[OCH((CH2)mR)CH2C(O)]— (2) within a same molecule, and a method for producing a polyhydroxyalkanoate copolymer by microorganisms, utilizing a ω-bromoalkanoic acid represented by a formula Br(CH2)pCH2CH2COOH (p=1 to 8) (20) and a compound represented by a formula R(CH2)qCH2CH2COOH (21) as raw materials.
摘要翻译：本发明提供一种具有溴基团并且是热稳定的并能够任意控制物理性能的聚羟基链烷酸酯及其制备方法。根据本发明，提供了一种包含由式 - [OCH（（CH 2）n）n Br表示的3-羟基-ω-溴代链烷酸单元的聚羟基链烷酸酯共聚物）CH 2 C（O）] - （n = 1-8）（1）和由式 - [OCH（（CH 2）2）（O）] - （2），以及通过微生物制备聚羟基链烷酸酯共聚物的方法，使用由以下化合物表示的ω-溴烷酸：式（Br 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 COOH（p = 1〜8）（20 ）和由式R（CH 2 CH 2）q CH 2 CH 2 COOH（21）表示的化合物作为原料。

63. 发明授权

US07045321B2 POLYHYDROXYALKANOATE CONTAINING UNIT WITH PHENYLSULFANYL STRUCTURE IN THE SIDE CHAIN, PROCESS FOR ITS PRODUCTION, CHARGE CONTROL AGENT, TONER BINDER AND TONER WHICH CONTAIN NOVEL POLYHYDROXYALKANOATE, AND IMAGE-FORMING METHOD AND IMAGE-FORMING APPARATUS WHICH MAKE USE OF THE TONER 失效
标题翻译：含有侧链中的酚醛结构的聚羟基烷酸酯单体，其生产方法，充电控制剂，含有新型聚羟基烷基酯的调色剂和调色剂，以及使用该调色剂的图像形成方法和成像装置
公开(公告)号：US07045321B2
公开(公告)日：2006-05-16
申请号：US10084172
申请日：2002-02-28
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
IPC分类号： C12P11/00 , C12P13/00 , C08G63/02
CPC分类号： G03G9/08755 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08791 , G03G9/09733 , G03G9/09775
摘要： A polyhydroxyalkanoate characterized by having in the molecule a unit represented by Chemical Formula (1): wherein n may assume any one integral value within the range of from 1 to 8. Also disclosed are a process for producing the polyhydroxyalkanoate by the use of a microorganism having the ability to produce the polyhydroxyalkanoate and accumulate it in the bacterial body; a charge control agent, a toner binder and a toner which contain this polyhydroxyalkanoate; and an image-forming method and an image-forming apparatus which make use of the toner.
摘要翻译：公开了在分子中具有由化学式（1）表示的单元的聚羟基链烷酸酯。其中R选自氢原子，卤原子，CN，NO 2，COOR'，SO 2 R“，CH 3，C 2 H 5，C 3 H 7，C（CH 3）2 H和C（CH 3）3; 其中R'是H，Na，K，CH3或C2H5，R“是OH，ONa，OK，卤素原子，OCH3或OC2H5; x是任意选自1至8的整数; 条件是排除了具有氢原子作为R的聚羟基链烷酸酯，并且所有单元中的x均为2或4.还公开了通过使用具有生产聚羟基链烷酸酯的能力的微生物来生产聚羟基链烷酸酯并累积它在细菌体内

64. 发明申请

US20060040366A1 New polyhydroxyalkanoate comprising unit having (phenylmethyl) oxy structure on side chain thereof, and method for producing the same 审中-公开
标题翻译：包含在其侧链上具有（苯基甲基）氧基结构的单元的新的聚羟基链烷酸酯及其制造方法
公开(公告)号：US20060040366A1
公开(公告)日：2006-02-23
申请号：US10531572
申请日：2003-10-23
申请人： Takashi Kenmoku , Tetsuya Yano , Shinya Kozaki , Tsutomu Honma
发明人： Takashi Kenmoku , Tetsuya Yano , Shinya Kozaki , Tsutomu Honma
IPC分类号： C12P7/62 , C08G69/44
CPC分类号： C12P7/625 , C08G63/06 , C08G63/664 , C08G63/6882
摘要： Provided are a PHA having an active group, which is produced by microorganisms with high productivity, and in which the ratio of units on its side chain having an active group can be controlled and the physical properties can be arbitrarily controlled so that its application as a polymer is not limited, and a method for producing the same. A 3-hydroxy-ω-[(phenylmethyl)oxy]alkanoic acid unit expressed by the following chemical formula (1): wherein x can be one or more integers within the range shown in the chemical formula.
摘要翻译：提供具有活性基团的PHA，其由高生产率的微生物产生，并且其中可以控制具有活性基团的侧链上的单元比例，并且物理性质可以任意控制，使得其作为聚合物不受限制，也可以是其制造方法。由以下化学式（1）表示的3-羟基-ω（ - （（苯甲基）氧基）链烷酸单元：其中x可以是化学式所示范围内的一个或多个整数。

65. 发明授权

US06911521B2 Polyhydroxyalkanoate that comprises unit having substituted or unsubstituted (phenylmethyl) sulfanyl structure in side chain thereof and process for producing the same 失效
标题翻译：包含在侧链具有取代或未取代（苯基甲基）硫烷基结构的单元的聚羟基链烷酸酯及其制备方法
公开(公告)号：US06911521B2
公开(公告)日：2005-06-28
申请号：US10157142
申请日：2002-05-30
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G63/06 , C08G63/02 , C08G63/688 , C08G63/78 , C12P7/62 , C12P11/00
CPC分类号： C12P11/00 , C08G63/6882 , C12P7/625
摘要： A polyhydroxyalkanoate that comprises a unit represented by the following chemical formula (1): wherein R1 is a substituent of an aromatic ring selected from the group consisting of H, CH3, C2H5, CH3CH2CH2, (CH3)2CH, (CH3)3C, a halogen atom, CN, NO2, COOR′, and SO2R″, wherein R′ is selected from the group consisting of H, Na, K, CH3, and C2H5, and R″ is selected from the group consisting of OH, a halogen atom, ONa, OK, OCH3, and OC2H5; and x represents an integer of 1 to 8 being the same or different each other in the polyhydroxyalkanoate. A method for producing the polyhydroxyalkanoate is also provided.
摘要翻译：一种聚羟基链烷酸酯，其包含由以下化学式（1）表示的单元：其中R1是选自H，CH 3，C 2， CH 3，CH 3，CH 2，CH 2，CH 3，CH 3，CH 3，CH 3，）CH 2（CH 3）3 C，卤素原子，CN，NO 2，COOR' ，和SO 2 R“，其中R'选自H，Na，K，CH 3，和C 2 H 5，并且R“选自OH，卤素原子，ONa，OK，OCH 3和OC 2， 5 H 5; x表示在聚羟基链烷酸酯中相同或不同的1〜8的整数。还提供了生产聚羟基链烷酸酯的方法。

66. 发明授权

US06911520B2 Polyhydroxyalkanoate, method of producing the same, charge controlling agent containing polyhydroxyalkanoate, toner binder and toner, and image formation method and image forming apparatus using toner 失效
标题翻译：聚羟基链烷酸酯，其制备方法，含有聚羟基链烷酸酯的电荷控制剂，调色剂粘合剂和调色剂，以及成像方法和使用调色剂的图像形成装置
公开(公告)号：US06911520B2
公开(公告)日：2005-06-28
申请号：US10373851
申请日：2003-02-27
申请人： Tatsuki Fukui , Etsuko Sugawa , Tetsuya Yano , Chieko Mihara , Takeshi Imamura , Takashi Kenmoku
发明人： Tatsuki Fukui , Etsuko Sugawa , Tetsuya Yano , Chieko Mihara , Takeshi Imamura , Takashi Kenmoku
IPC分类号： C08G63/06 , C08G63/688 , C08G63/91 , C08L101/16 , G03G9/087 , G03G9/097 , C08G63/02
CPC分类号： C08G63/912 , C08G63/06 , C08G63/6882 , G03G9/08791 , G03G9/097 , G03G9/09733
摘要： Provided is a polyhydroxyalkanoate containing in a molecule thereof one or more units each selected from the following formulae (1) (2), (3) and (4): wherein R1 and R6 are each OH, halogen, ONa, OK, OCH3 or OC2H5; A1 and J6 are each a substituted or unsubstituted aliphatic hydrocarbon; m and n are each 0 to 7; r is 1 to 500; and R1′ to R5′ are each hydrogen or halogen.
摘要翻译：提供一种分子中含有一个或多个选自下式（1）（3）和（4）中的单元的聚羟基链烷酸酯：其中R 1和R 6 每个OH，卤素，ONa，OK，OCH 3或OC 2 H 5; A 1和J 6各自为取代或未取代的脂族烃; m和n各自为0至7; r为1〜500; R 1至R 5'各自为氢或卤素。

67. 发明授权

US06908721B2 POLYHYDROXYALKANOATE HAVING AMIDE GROUP AND SULFONIC GROUP, METHOD OF PRODUCING THE SAME, CHARGE CONTROLLING AGENT CONTAINING NOVEL POLYHYDROXYALAKNAOTE, TONER BINDER, TONER, AND IMAGE FORMING APPARATUS USING THE TONER 失效
标题翻译：具有酰胺基和磺酰基的聚羟基烷酸酯，其制备方法，含有新型聚羟基烷基酮酸酯的电荷控制剂，调色剂粘合剂，调色剂和使用该调色剂的图像形成装置
公开(公告)号：US06908721B2
公开(公告)日：2005-06-21
申请号：US10367951
申请日：2003-02-19
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Chieko Mihara , Takeshi Imamura , Tatsuki Fukui
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Chieko Mihara , Takeshi Imamura , Tatsuki Fukui
IPC分类号： G03G9/097 , C08G63/688 , C08G63/91 , C08L101/16 , C12P7/62 , C12P11/00 , G03G9/087 , C08G63/02
CPC分类号： G03G9/08755 , C08G63/6882 , C08G63/912 , C12P7/625 , C12P11/00 , G03G9/08791
摘要： A polyhydroxyalkanoate comprises a unit of formula (1): —(O—CH((CH2)mSASO2R)CH2C(═O))— wherein R is selected from the group consisting of OH, a halogen atom, ONa, OK, OCH3 and OC2H5; A represents a substituted or unsubstituted aliphatic hydrocarbon structure; m is an integer number selected from 1 to 8; and in the case where a plurality of units exist in the same molecule, R, A and m in one unit can be different from them in another unit respectively. A method of producing the polyhydroxyalkanoate comprises the step of reacting a polyhydroxyalkanoate comprising a unit of formula (18): —(O—CH((CH2)mBr)CH2C(═O))—, wherein m is an integer number selected from 1 to 8, and in the case where a plurality of units exist in the same molecule, m in one unit can be different from that in another unit, with at least one type of compounds of formula (19): HS-A1-SO2R15 wherein R15 is selected from the group consisting of OH, a halogen atom, ONa, OK, OCH3 and OC2H5 and A1 is a substituted or unsubstituted aliphatic hydrocarbon structure, and in the case where a plurality of types of compounds exist in the same molecule, R15 and A1 in one unit can be different from them in another unit respectively.
摘要翻译：聚羟基链烷酸酯包含式（1）的单元： - （O-CH（（CH 2）2）NH 2 R 2 CH 2 （O）） - 其中R选自OH，卤素原子，ONa，OK，OCH 3和OC 2 可以分别与另一个单元中的不同。

68. 发明授权

US06908720B2 Polyhydroxyalkanoate, its production method, charge control agent containing the polyhydroxyalkanoate, toner binder and toner, and image forming method and image forming apparatus using the toner 失效
标题翻译：聚羟基链烷酸酯，其制备方法，含有聚羟基链烷酸酯的电荷控制剂，调色剂粘合剂和调色剂，以及使用该调色剂的图像形成方法和图像形成装置
公开(公告)号：US06908720B2
公开(公告)日：2005-06-21
申请号：US10133576
申请日：2002-04-29
申请人： Takashi Kenmoku , Toyoko Kobayashi , Etsuko Sugawa , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Tsutomu Honma
发明人： Takashi Kenmoku , Toyoko Kobayashi , Etsuko Sugawa , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Tsutomu Honma
IPC分类号： C08G63/688 , C12P7/62 , C12P11/00 , G03G9/087 , G03G9/097 , C08G13/06 , C08F20/00
CPC分类号： G03G9/08771 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08728 , G03G9/0874 , G03G9/08768 , G03G9/08773 , G03G9/08791 , G03G9/08795 , G03G9/08797 , G03G9/09733 , G03G9/09775
摘要： The present invention provides a novel PHA comprising a unit containing thioether with high reactivity, and its production method. The present invention also provides polyhydroxyalkanoate (PHA) comprising units having defined chemical formulas (1) and (2), and at least one of four units having defined chemical formulas (3), (4), (5) and (6); its production method; a charge control agent containing the PHA; a toner binder containing the charge control agent; an electrostatic latent image developing toner; and an image forming method and an image forming apparatus using the electrostatic latent image developing toner.
摘要翻译：本发明提供了包含含有高反应性的硫醚的单元的新型PHA及其制造方法。本发明还提供了包含具有确定的化学式（1）和（2）的单元和具有确定的化学式（3），（4），（5）和（6）的四个单元中的至少一个的聚羟基链烷酸酯（PHA）其生产方式; 含有PHA的电荷控制剂; 含有电荷控制剂的调色剂粘合剂; 静电潜像显影调色剂; 以及使用静电潜像显影用调色剂的图像形成方法和图像形成装置。

69. 发明授权

US06869782B2 Polyhydroxyalkanoate that comprises unit having (methylsulfanyl) phenoxy structure in side chain thereof and process for producing the same 失效
标题翻译：包含在侧链具有（甲基硫烷基）苯氧基结构的单元的聚羟基链烷酸酯及其制造方法
公开(公告)号：US06869782B2
公开(公告)日：2005-03-22
申请号：US10187808
申请日：2002-07-03
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Takeshi Imamura
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Takeshi Imamura
IPC分类号： C08G63/49 , C08G63/688 , C12P7/62 , C12P11/00 , C08G63/02 , C08G79/00
CPC分类号： C12P11/00 , C08G63/6882 , C12P7/625
摘要： A polyhydroxyalkanoate that comprises a unit represented by the following chemical formula (1): wherein x is an integer of 1 to 8 being the same or different in the polyhydroxyalkanoate. The microbial production process is also disclosed.
摘要翻译：包含由以下化学式（1）表示的单元的聚羟基链烷酸酯：其中x是1至8的整数，在聚羟基链烷酸酯中相同或不同。还公开了微生物生产过程。

70. 发明授权

US06855472B2 POLYHYDROXYALKANOATE, PRODUCING METHOD THEREFOR, CHARGE CONTROL AGENT CONTAINING SUCH POLYHYDROXYALKANOATE, TONER CONTAINING SUCH CONTROL AGENT AND IMAGE FORMING METHOD AND IMAGE FORMING APPARATUS UTILIZING SUCH TONER 失效
标题翻译：聚羟基烷酸酯，其制造方法，含有这样的聚羟基烷酸酯的充电控制剂，含有这种控制剂的调色剂和图像形成方法以及使用这种色粉的图像形成装置
公开(公告)号：US06855472B2
公开(公告)日：2005-02-15
申请号：US10133379
申请日：2002-04-29
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Takashi Kenmoku
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Takashi Kenmoku
IPC分类号： C08G63/49 , C08G63/688 , C12P7/62 , C12P11/00 , G03G9/087 , G03G9/08 , C08C75/00
CPC分类号： C12P11/00 , C08G63/6882 , C12P7/625 , G03G9/08755
摘要： The invention is to provide polyhydroxyalkanoate of a novel structure enabling application to wider fields, and a producing method therefor. The invention also provides a biodegradable charge control agent having excellent charging characteristics, excellent dispersibility in the toner resin and improved spent property. The polyhydroxyalkanoate of the present invention is featured by including, in the polymer molecule, a units represented by the general formulas (1) and (2) and at least one of the units represented by the general formulas (3) to (6).
摘要翻译：本发明提供具有能够应用于更广领域的新型结构的聚羟基链烷酸酯及其制造方法。本发明还提供了具有优异的充电特性，在调色剂树脂中优异的分散性和改善的废弃性能的可生物降解的电荷控制剂。本发明的聚羟基链烷酸酯的特征在于，在聚合物分子中包含由通式（1）和（2）表示的单元和由通式（3）〜（6）表示的单元中的至少一个。

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