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51. 发明申请

US20170018793A1 POLYMER ELECTROLYTE MEMBRANE, CATALYST COATED MEMBRANE, MEMBRANE ELECTRODE ASSEMBLY, AND POLYMER ELECTROLYTE FUEL CELL 审中-公开
标题翻译：聚合物电解质膜，催化涂层膜，膜电极组件和聚合物电解质燃料电池
公开(公告)号：US20170018793A1
公开(公告)日：2017-01-19
申请号：US15124044
申请日：2015-03-06
申请人： Toray Industries, Inc.
发明人： Tomoyuki Kunita , Daisuke Izuhara , Hiroaki Umeda
IPC分类号： H01M8/103 , H01M8/1027 , C08G75/23 , C08J5/22 , C08G73/18
CPC分类号： H01M8/103 , C08G65/4012 , C08G65/405 , C08G65/4056 , C08G73/18 , C08G75/23 , C08G2650/40 , C08J5/2256 , C08J5/2268 , C08J2379/04 , C08J2381/06 , C08J2479/04 , C08L71/00 , C08L71/08 , C08L79/04 , H01B1/122 , H01M8/1025 , H01M8/1027 , H01M8/1032 , H01M8/1044 , H01M2008/1095 , H01M2300/0082
摘要： A polymer electrolyte composition is excellent in practicality which has such an excellent chemical stability as to be able to withstand a strong oxidizing atmosphere during operation of a fuel cell and is capable of achieving excellent proton conductivity under a low-humidified condition and excellent mechanical strength and physical durability as well as a polymer electrolyte membrane, a membrane electrode assembly, and a polymer electrolyte fuel cell which use the polymer electrolyte composition. The polymer electrolyte membrane is a polymer electrolyte membrane that contains at least an ionic group-containing polymer electrolyte and a polyazole, which is a polymer electrolyte membrane in which a phase separation of 2 nm or larger in which the polyazole is a main component is not observed in transmission type electron microscopic observation.
摘要翻译：聚合物电解质组合物的实用性优异，具有能够在燃料电池运行时能够承受强氧化性气氛的优异的化学稳定性，能够在低加湿条件下优异的质子传导性和优异的机械强度，物理耐久性以及使用该聚合物电解质组合物的聚合物电解质膜，膜电极组件和聚合物电解质燃料电池。高分子电解质膜是含有至少含有离子性基团的高分子电解质和聚合物电解质膜的高分子电解质膜，聚合物电解质膜是聚合物电解质膜，其中以聚合物为主要成分的相位为2nm以上的相分离观察透射型电子显微镜观察。

52. 发明申请

US20160340460A1 SULFONATED POLYPHOSPHAZENE COPOLYMER PROTON EXCHANGE MEMBRANE MATERIAL AND METHOD FOR PREPARING SUCH MEMBRANE 有权
标题翻译：磺化聚苯乙烯共聚物原子交换膜材料及其制备方法
公开(公告)号：US20160340460A1
公开(公告)日：2016-11-24
申请号：US15033829
申请日：2015-03-20
申请人： Hulin XU
发明人： Hulin XU , Changjin ZHU
IPC分类号： C08F283/00 , H01M8/103 , H01M8/1034 , C08J5/22 , B01J39/18
CPC分类号： C08F283/00 , B01J39/19 , C08F8/12 , C08F8/36 , C08F212/14 , C08F2438/01 , C08F2500/26 , C08F2810/20 , C08G79/025 , C08J5/22 , C08J5/2268 , C08J5/2287 , C08J2325/08 , C08J2351/08 , C08J2385/02 , H01M2/16 , H01M8/02 , H01M8/103 , H01M8/1034 , H01M2008/1095 , C08F212/08
摘要： A sulfonated polyphosphazene copolymer proton exchange membrane material, and a method for preparing such membrane includes a macromolecule initiator as bromo polyphosphazene is subjected to atom transfer radical polymerization with styrene, yielding a graft copolymer, which is hydrazinolyzed with hydrazine hydrate resulting in a copolymer including a hydroxyl group. The copolymer is reacted with 1,4-butane sultone to yield a sulfonated copolymer finally. The polymer is cross-linked with 2,6-di(hydroxymethyl)-4-methyl phenol (BHMP) as a cross linking agent in the presence of methyl sulfonic acid, yielding cross-linked proton exchange membrane. Such cross-linked graft copolymer membrane has high proton conductivity, low methanol hindrance, and low cost, and has ideal effect when applied in fuel cells as proton exchange membrane material.
摘要翻译：一种磺化聚磷腈共聚物质子交换膜材料及其制备方法，其特征在于，将溴代聚磷腈的高分子引发剂与苯乙烯进行原子转移自由基聚合，得到接枝共聚物，并与水合肼进行肼解，形成共聚物，羟基。共聚物与1,4-丁烷磺内酯反应，最终得到磺化共聚物。聚合物在甲基磺酸存在下与2,6-二（羟甲基）-4-甲基苯酚（BHMP）交联，产生交联的质子交换膜。这种交联接枝共聚物膜具有高质子传导性，低甲醇阻力和低成本，并且在作为质子交换膜材料用于燃料电池中具有理想的效果。

53. 发明申请

US20150217239A1 METHODS FOR MANUFACTURING ION EXCHANGE MEMBRANES 审中-公开
标题翻译：用于制造离子交换膜的方法
公开(公告)号：US20150217239A1
公开(公告)日：2015-08-06
申请号：US14426517
申请日：2013-07-19
申请人： GENERAL ELECTRIC COMPANY
发明人： Harikrishnan Ramanan
IPC分类号： B01D69/12 , B32B38/10 , B32B37/06 , B01D67/00 , B32B37/00
CPC分类号： B01D69/122 , B01D67/0083 , B01D69/125 , B01D2323/46 , B32B37/0046 , B32B37/06 , B32B38/0008 , B32B38/10 , B32B2305/02 , B32B2307/726 , B32B2309/02 , B32B2333/04 , B32B2398/00 , C08J5/2268 , C08J5/2275
摘要： To make membranes, a plurality of membrane substrates are each wetted with a curable liquid mixture, arranged in a stack such that every pair of substrates are separated by at least one film, and moved simultaneously through a common curing region. Each wetted substrate sheet may be sandwiched between two films. After curing, the stack comprises two or more membranes with each pair of membranes separated by a film. An apparatus for making membranes comprises at least two substrate feeding devices, at least one film feeding device, one or more chemical wetting devices, a curing region, optionally, a stack separating region, and, optionally, a membrane binding or fusing region. Membrane production rate may be increased while the curing energy required per unit area of membrane is decreased. The method can make, for example, ion exchange membranes.
摘要翻译：为了制造膜，多个膜基板各自用可固化的液体混合物润湿，其被布置成堆叠，使得每对基板被至少一个膜分离，同时通过共同的固化区域移动。每个润湿的基片可夹在两片之间。固化后，堆叠包括两个或更多个膜，每对膜由膜分隔。一种用于制造膜的设备包括至少两个基材进料装置，至少一个胶片输送装置，一个或多个化学润湿装置，固化区域，任选的叠层分离区域，以及任选的膜结合或熔合区域。膜生产率可能会提高，而每单位面积膜所需的固化能量则降低。该方法可以制成例如离子交换膜。

54. 发明申请

US20140363754A1 POLYMER ELECTROLYTE COMPOSITION, ELECTROLYTE MEMBRANE, MEMBRANE-ELECTRODE ASSEMBLY AND FUEL CELL 有权
标题翻译：聚合物电解质组合物，电解质膜，膜电极组件和燃料电池
公开(公告)号：US20140363754A1
公开(公告)日：2014-12-11
申请号：US14127703
申请日：2013-03-15
申请人： LG Cham, Ltd.
发明人： Seong Ho Choi , Hye Mi Kim , Hye Sung Cho , Hyuk Kim , Youngcheol Choi , Sangwoo Lee , Tae Geun Noh , Kyunga Sung , Doyoung Kim , Minkyu Min
IPC分类号： H01M8/10
CPC分类号： H01M8/1027 , C08J5/2268 , C08J2387/00 , H01M8/103 , H01M8/1032 , H01M8/1037 , H01M8/1039 , H01M8/1081 , H01M2008/1095 , H01M2300/0082 , Y02P70/56
摘要： Provided are a polymer electrolyte composition, an electrolyte membrane, a membrane electrolyte assembly, and a fuel cell. The polymer electrolyte composition according to an exemplary embodiment of this application includes a first solvent, a second solvent which is different from the first solvent, and a polymer which is reacted with the first solvent and the second solvent, in which the polymer includes a functional group which reacts with the first solvent by a first reaction energy and with the second solvent by a second reaction energy, and the second reaction energy is smaller than the first reaction energy.
摘要翻译：提供聚合物电解质组合物，电解质膜，膜电解质组件和燃料电池。根据本申请的一个示例性实施方案的聚合物电解质组合物包括第一溶剂，不同于第一溶剂的第二溶剂和与第一溶剂和第二溶剂反应的聚合物，其中聚合物包括官能该基团通过第一反应能与第一溶剂反应，并且通过第二反应能与第二溶剂反应，第二反应能小于第一反应能。

55. 发明授权

US08263710B2 Solid polymer electrolyte material, liquid composition, solid polymer fuel cell and fluoropolymer 有权
标题翻译：固体聚合物电解质材料，液体组合物，固体聚合物燃料电池和含氟聚合物
公开(公告)号：US08263710B2
公开(公告)日：2012-09-11
申请号：US13214273
申请日：2011-08-22
申请人： Atsushi Watakabe , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
发明人： Atsushi Watakabe , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
IPC分类号： C08F14/18 , C08F16/24
CPC分类号： H01M8/1067 , B01D71/32 , B01D71/44 , B01D71/72 , B01D71/76 , C08F216/1466 , C08F228/02 , C08J5/2268 , C08J2327/18 , C08J2365/00 , C08J2387/00 , C08L65/00 , H01B1/122 , H01M6/181 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M10/0525 , H01M10/0565
摘要： A solid polymer electrolyte material made of a copolymer comprising a repeating unit based on a fluoromonomer A which gives a polymer having an alicyclic structure in its main chain by radical polymerization, and a repeating unit based on a fluoromonomer B of the following formula (1): CF2═CF(Rf)jSO2X (1) wherein j is 0 or 1, X is a fluorine atom, a chlorine atom or OM {wherein M is a hydrogen atom, an alkali metal atom or a group of NR1R2R3R4 (wherein each of R1, R2, R3 and R4 which may be the same or different, is a hydrogen atom or a monovalent organic group)}, and Rf is a C1-20 polyfluoroalkylene group having a straight chain or branched structure which may contain ether oxygen atoms.
摘要翻译：一种由共聚物制成的固体聚合物电解质材料，该共聚物包含基于通过自由基聚合在主链中具有脂环结构的聚合物的基于含氟单体A的重复单元和基于下式（1）的含氟单体B的重复单元，：CF2 = CF（Rf）jSO2X（1）其中j为0或1，X为氟原子，氯原子或OM（其中M为氢原子，碱金属原子或NR1R2R3R4基团 R 1，R 2，R 3和R 4可以相同或不同，为氢原子或一价有机基团}}，R f为可含有醚氧原子的具有直链或支链结构的C1-20多氟亚烷基。

56. 发明授权

US07951494B2 Solid electrolyte with high ion-conductivity and method for manufacturing the same, and electrochemical system using solid electrolyte 有权
标题翻译：具有高离子电导率的固体电解质及其制造方法，以及使用固体电解质的电化学系统
公开(公告)号：US07951494B2
公开(公告)日：2011-05-31
申请号：US12165860
申请日：2008-07-01
申请人： Haruo Sawa , Haruyuki Nakanishi , Shinichi Matsumoto
发明人： Haruo Sawa , Haruyuki Nakanishi , Shinichi Matsumoto
IPC分类号： H01M6/18 , G01N27/26
CPC分类号： C25B13/08 , C08J5/2256 , C08J5/2268 , C08J2329/04 , C08J2379/04 , H01M6/181 , H01M6/188 , H01M8/0289 , H01M8/1027 , H01M8/103 , H01M8/1046 , H01M8/1072 , H01M10/056 , H01M10/26 , H01M10/347 , H01M2300/0082 , H01M2300/0091 , Y02P70/56
摘要： The present invention provides a solid electrolyte with high ion-conductivity which is cheap and exhibits high conductivity in an alkaline form, and stably keeps high conductivity because of a small amount of the leak of a compound bearing conductivity even in a wet state. The invention is useful in an electrochemical system using the solid electrolyte, such as a fuel cell.The solid electrolyte with high ion-conductivity comprises a hybrid compound which contains at least polyvinyl alcohol and a zirconic acid compound, and also a nitrogen-containing organic compound having a structure of amine, quaternary ammonium compound and/or imine, obtained by hydrolyzing a zirconium salt or an oxyzirconium salt in a solution including water, polyvinyl alcohol, a zirconium salt or an oxyzirconium salt and a nitrogen-containing organic compound having a structure of amine, quaternary ammonium compound and/or imine coexist, removing a solvent and contacting with alkali.
摘要翻译：本发明提供一种廉价且具有高导电性的碱性形式的高离子电导率的固体电解质，并且由于即使在潮湿状态下也具有导电性的化合物的泄漏量少，因而稳定地保持高导电性。本发明在使用诸如燃料电池的固体电解质的电化学系统中是有用的。具有高离子传导性的固体电解质包括至少包含聚乙烯醇和锆酸化合物的杂化化合物，以及具有胺，季铵化合物和/或亚胺结构的含氮有机化合物，其通过水解锆盐或氧锆盐在包括水，聚乙烯醇，锆盐或氧锆盐的溶液中，以及具有胺，季铵化合物和/或亚胺结构的含氮有机化合物共存，除去溶剂并与碱。

57. 发明授权

US07816052B2 Portion conductive electrolyte, method of preparing the same, electrode for fuel cell, method of manufacturing the electrode, and fuel cell including the same 有权
标题翻译：部分导电电解质，其制备方法，燃料电池用电极，电极的制造方法以及包含该电极的燃料电池
公开(公告)号：US07816052B2
公开(公告)日：2010-10-19
申请号：US11441000
申请日：2006-05-26
申请人： Myung-dong Cho , Jung-ock Park
发明人： Myung-dong Cho , Jung-ock Park
IPC分类号： H01M6/14
CPC分类号： H01M8/1081 , C08J5/2268 , C08J2375/04 , C08J2387/00 , H01B1/122 , H01M4/8605 , H01M4/8803 , H01M8/1023 , H01M8/1027 , H01M8/103 , H01M8/1039 , H01M8/1044 , H01M2008/1095 , H01M2300/0082 , Y02P70/56
摘要： A proton conductive electrolyte including a polymerized polyurethane, polyethylene(metha)acrylic acid (PEAA), and a cross-linking agent mixture; a method of preparing the same; an electrode including a support and a catalyst layer, the catalyst layer including a supported catalyst and a polymerized mixture of a polyurethane based compound and a polyethylene(metha)acrylic acid; a method of preparing the electrode; and a fuel cell including the proton conductive electrolyte and/or the electrode. The proton conductive electrolyte can be prepared at lower costs than conventionally used polybenzimidazole and NAFION and can be easily formed into a membrane with a controlled thickness by casting. The polymer electrolyte membrane has high mechanical strength, flexibility, and excellent ionic conductivity. The electrode remains stable under high temperature operation, a strong binding force is maintained between the support and the catalyst layer, and the electrode has excellent ionic conductivity. The fuel cell produced using the proton conductive electrolyte and/or the electrode can operate at 100° C. or higher under non-humidified conditions and exhibits an improved performance.
摘要翻译：包含聚合的聚氨酯，聚乙烯（甲基）丙烯酸（PEAA）和交联剂混合物的质子传导电解质; 其制备方法; 包括载体和催化剂层的电极，所述催化剂层包括负载型催化剂和聚氨酯基化合物与聚乙烯（甲基）丙烯酸的聚合混合物; 制备电极的方法; 以及包括质子传导性电解质和/或电极的燃料电池。质子传导电解质可以以比常规使用的聚苯并咪唑和NAFION更低的成本制备，并且可以通过铸造容易地形成具有受控厚度的膜。聚合物电解质膜具有高机械强度，柔韧性和优异的离子导电性。电极在高温操作下保持稳定，在支撑体和催化剂层之间保持牢固的结合力，电极具有优异的离子导电性。使用质子传导电解质和/或电极制造的燃料电池可在非加湿条件下在100℃或更高温度下工作，并且表现出改进的性能。

58. 发明申请

US20080014490A1 SOLID POLYMER ELECTROLYTE MATERIAL LIQUID COMPOSITION, SOLID POLYMER FUEL CELL AND FLUOROPOLYMER 有权
标题翻译：固体聚合物电解质材料液体组合物，固体聚合物燃料电池和氟聚合物
公开(公告)号：US20080014490A1
公开(公告)日：2008-01-17
申请号：US11671665
申请日：2007-02-06
申请人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
发明人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
IPC分类号： H01M8/10
CPC分类号： H01M8/1067 , B01D71/32 , B01D71/44 , B01D71/72 , B01D71/76 , C08F216/1466 , C08F228/02 , C08J5/2268 , C08J2327/18 , C08J2365/00 , C08J2387/00 , C08L65/00 , H01B1/122 , H01M6/181 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M10/0525 , H01M10/0565
摘要： A solid polymer electrolyte material made of a copolymer comprising a repeating unit based on a fluoromonomer A which gives a polymer having an alicyclic structure in its main chain by radical polymerization, and a repeating unit based on a fluoromonomer B of the following formula (1): CF2═CF(Rf)jSO2X (1) wherein j is 0 or 1, X is a fluorine atom, a chlorine atom or OM {wherein M is a hydrogen atom, an alkali metal atom or a group of NR1R2R3R4 (wherein each of R1, R2, R3 and R4 which may be the same or different, is a hydrogen atom or a monovalent organic group)}, and Rf is a C1-20 polyfluoroalkylene group having a straight chain or branched structure which may contain ether oxygen atoms.
摘要翻译：一种由共聚物制成的固体聚合物电解质材料，该共聚物包含基于通过自由基聚合在主链中具有脂环结构的聚合物的基于含氟单体A的重复单元和基于下式（1）的含氟单体B的重复单元，：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF -CF（R）其中j为0或1，X为氟原子，X为1或2，，氯原子或OM（其中M为氢原子，碱金属原子或NR 1 R 2 O 3 R 3的基团） 4（其中R 1，R 2，R 3和R 4中的每一个）其可以相同或不同，是氢原子或一价有机基团）}，并且R f是具有直链的C 1〜20个多氟亚烷基或可以含有醚氧原子的支链结构。

59. 发明申请

US20050244694A1 Proton-conducting polymer membrane comprising polymers containing phosphonic acid groups and its use in fuel cells 失效
标题翻译：导电聚合物膜，其包含含有膦酸基团的聚合物及其在燃料电池中的应用
公开(公告)号：US20050244694A1
公开(公告)日：2005-11-03
申请号：US10522839
申请日：2003-07-31
申请人： Joachim Kiefer , Oemer Uensal , Gordon Calundann
发明人： Joachim Kiefer , Oemer Uensal , Gordon Calundann
IPC分类号： C08J7/04 , B01D71/58 , C08F230/02 , C08F271/02 , C08F275/00 , C08F291/00 , C08G61/12 , C08G73/06 , C08G73/08 , C08G73/10 , C08G73/18 , C08G73/22 , C08J5/22 , H01B1/06 , H01B13/00 , H01M4/86 , H01M4/88 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2268 , C08F230/02 , C08F271/02 , C08F275/00 , C08F291/00 , C08G61/122 , C08G73/08 , C08G73/10 , C08G73/18 , C08G73/22 , C08J2379/06 , H01M8/1004 , H01M8/1023 , H01M8/103 , H01M8/1041 , H01M8/1072 , Y02P70/56
摘要： The present invention relates to a proton-conducting polymer membrane comprising polymers containing phosphonic acid groups which is obtainable by a process comprising the steps A) mixing of vinyl-containing phosphonic acid with one or more aromatic tetraamino compounds with one or more aromatic carboxylic acids, esters thereof, acid halides thereof or anhydrides thereof which contain at least two acid groups per carboxylic acid monomer, and/or mixing of vinyl-containing phosphonic acid with one or more aromatic and/or heteroaromatic diamino carboxylic acids, esters thereof, acid halides thereof or anhydrides thereof, B) heating of the mixture obtainable according to step A) under inert gas at temperatures of up to 350° C. to form polyazole polymers, C) application of a layer using the mixture from step A) and/or B) to a support, D) polymerization of the vinyl-containing phosphonic acid present in the sheet-like structure obtainable according to step C).
摘要翻译：本发明涉及包含含有膦酸基团的聚合物的质子传导聚合物膜，其可通过包括以下步骤的方法获得：A）将含乙烯基的膦酸与一种或多种芳族四氨基化合物与一种或多种芳族羧酸混合，其酯，其酰卤或其酸酐，其每个羧酸单体含有至少两个酸基，和/或含乙烯基的膦酸与一种或多种芳族和/或杂芳族二氨基羧酸，其酯，其酰卤的混合或其酸酐，B）在惰性气体下在高达350℃的温度下加热根据步骤A）获得的混合物，以形成聚唑聚合物，C）使用来自步骤A）和/或B的混合物），D）根据步骤C）获得的片状结构中存在的含乙烯基膦酸的聚合。

60. 发明授权

US06180007B2 Membrane formed by an acrylonitrile-based polymer 失效
标题翻译：由丙烯腈基聚合物形成的膜
公开(公告)号：US06180007B2
公开(公告)日：2001-01-30
申请号：US09016518
申请日：1998-01-31
申请人： Frank Gentile , Molly Shoichet , Milton Harris
发明人： Frank Gentile , Molly Shoichet , Milton Harris
IPC分类号： C08L2044
CPC分类号： C08L71/02 , C08F8/12 , C08G81/025 , C08J5/2268 , C08J2327/06 , C08J2371/02 , C08F20/44 , C08L2666/24 , C08L2666/04
摘要： A permselective graft polymer is disclosed that is formed by converting into intermediate reactive sites a portion of the cyano groups of a backbone polymer containing —CH2—CH(—C≡N)— units, and grafting polyalkylene oxide polymer chains to the backbone polymer through the reactive sites. Either the backbone polymer of a polymer resin or a permselective polymer membrane can be grafted. When a resin is used, it is formed into a permselective polymer membrane using known methods. The resulting permselective membrane can be formed into hollow fibers or flat sheets for the encapsulation of living cells. The encapsulated cells are then implanted into a patient in need of the biologically active factors produced by the cells. The permselective graft polymer membrane exhibits good molecular diffusion with minimal protein adsorption.
摘要翻译：公开了通过将包含-CH 2 -CH（-C = N） - 单元的主链聚合物的一部分氰基转化为中间反应性位点而形成的选择性接枝聚合物，并且将聚环氧烷聚合物链通过反应场地。聚合物树脂或选择性聚合物膜的主链聚合物可以被接枝。当使用树脂时，使用已知的方法将其形成为选择性选择性聚合物膜。所得到的选择性渗透膜可以形成用于活细胞包封的中空纤维或平板。然后将包封的细胞植入需要由细胞产生的生物活性因子的患者体内。选择性接枝聚合物膜表现出良好的分子扩散和最小的蛋白质吸附。

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