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51. 发明授权

US4439354A Tricyclic alcohols, ethers and esters, process for preparing same and use thereof in augmenting or enhancing the organoleptic properites of consumable materials 失效
标题翻译：三环醇，醚和酯，其制备方法及其在增强或增强消耗材料感官特性中的用途
公开(公告)号：US4439354A
公开(公告)日：1984-03-27
申请号：US311291
申请日：1981-10-13
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C31/137 , C07C43/18 , C07C45/00 , C07C45/67 , C07C49/453
CPC分类号： C07C49/453 , A23L27/203 , C07C403/02 , C07C45/00 , C07C45/67 , C07C2101/16
摘要： Described are compounds having the generic structure: ##STR1## wherein R.sub.1 represents hydrogen, methyl or acetyl and wherein R.sub.2, R.sub.3, R.sub.4 and R.sub.5 represent the same or different hydrogen, methyl or ethyl; a process for preparing same using compounds designed according to the generic structure: ##STR2## and organoleptic uses thereof in perfumes, colognes and perfumed articles.
摘要翻译：描述了具有以下通用结构的化合物：其中R 1表示氢，甲基或乙酰基，并且其中R 2，R 3，R 4和R 5表示相同或不同的氢，甲基或乙基; 使用根据通用结构设计的化合物的方法制备方法：＆lt; IMAGE＆gt;和其在香水，古龙水和香料制品中的感官用途。

52. 发明授权

US4411830A Bridged tricyclic alcohol, process for preparing same and perfumery use thereof 失效
标题翻译：桥接三环醇，其制备方法和香料用途
公开(公告)号：US4411830A
公开(公告)日：1983-10-25
申请号：US396258
申请日：1982-07-08
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C45/67 , C07C49/453 , C11B9/00 , A61K7/46
CPC分类号： C07C49/453 , A23L27/203 , C07C45/67
摘要： Described are the compounds covered by the generic structure: ##STR1## wherein "R" represents hydrogen or lithium. The compound having the structure: ##STR2## is useful in augmenting or enhancing the patchouli aroma of a perfume, cologne or perfumed article, such as a solid or liquid anionic, cationic, nonionic or zwitterionic detergent. The compound having the structure: ##STR3## is an intermediate for preparing the compound having the structure: ##STR4## according to the process defined by the reaction: ##STR5## .
摘要翻译：描述了通用结构覆盖的化合物：其中“R”表示氢或锂。具有以下结构的化合物：可用于增强或增强香料，古龙水或香水制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂的广藿香香气。具有以下结构的化合物：是根据由反应定义的方法制备具有以下结构的化合物的中间体：。

53. 发明授权

US4368128A Tricyclic alcohols, ethers and esters, process for preparing same and use thereof in augmenting or enhancing the organoleptic properties of consumable materials 失效
标题翻译：三环醇，醚和酯，其制备方法及其在增加或增强消耗材料的感官特性方面的用途
公开(公告)号：US4368128A
公开(公告)日：1983-01-11
申请号：US311141
申请日：1981-10-13
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C45/00 , C07C45/67 , C07C49/453 , D06M13/144 , D06M13/18 , D06M13/20
CPC分类号： C07C49/453 , A23L27/203 , C07C403/02 , C07C45/00 , C07C45/67 , C07C2101/16
摘要： Described are compounds having the generic structure: ##STR1## wherein R.sub.1 represents hydrogen, methyl or acetyl and wherein R.sub.2, R.sub.3, R.sub.4 and R.sub.5 represent the same or different hydrogen, methyl or ethyl; a process for preparing same using compounds designed according to the generic structure: ##STR2## and organoleptic uses thereof in perfumes, colognes, perfumed articles such as anionic, cationic, nonionic or zwitterionic solid or liquid detergents, cosmetic powders, fabric softener compositions and dryer-added fabric softener articles, as well as in foodstuffs, chewing tobaccos, smoking tobaccos and smoking tobacco articles, e.g., the body of smoking tobacco, the wrapper or the filter therefor.Thus, the tricyclic alcohol, ether or ester compounds of our invention having the generic structure: ##STR3## impart, augment or enhance dry woody (cedary, vetiver), thymol-like, camphoraceous, amber, sandalwood-like, fresh, sweaty, fruity, castoreum, cedrus atlantica, patchouli-like, labdanum, green, fruity, woody, cigar box-like, oriental, cedarwood-like, minty, spicy, floral (rose), vetiver-like, grapefruit oil-like, fruity and sweet aromas in or to perfume compositions, colognes and perfumed articles as well as oriental/incense, herbaceous, minty, earthy, woody, tobacco-like and cedarwood-like aromas and tastes to foodstuffs, chewing tobaccos, smoking tobaccos and smoking tobacco articles; wherein in the smoking tobaccos and smoking tobacco articles, these aromas and tastes are both prior to and on smoking in both the main stream and the side stream.
摘要翻译：描述了具有以下通用结构的化合物：其中R 1表示氢，甲基或乙酰基，并且其中R 2，R 3，R 4和R 5表示相同或不同的氢，甲基或乙基; 使用根据通用结构设计的化合物的方法：在图像和其在香料，古龙水，香料制品如阴离子，阳离子，非离子或两性离子固体或液体洗涤剂，化妆品粉末，织物柔软剂组合物和干燥剂中的感官用途添加织物柔软剂制品，以及食品，咀嚼烟草，烟草烟草和烟草制品，例如吸烟烟草，包装纸或其过滤器。因此，本发明的具有以下通用结构的三环醇，醚或酯化合物：赋予，增强或增强干木香（香蕉，香根草），百里酚状，樟脑，琥珀，檀香样，新鲜，汗状，水果，蓖麻，西葫芦，广藿香，乳黄，绿色，水果，木质，雪茄盒状，东方，雪松状，小，辣，花香（玫瑰），香根草样，葡萄柚油状，香水，香水和香水制品，东方香，香草，草本，泥土，泥土，木本，烟草样和雪松般的香气和口味到食物，咀嚼烟草，吸烟烟草和烟草制品中的香味; 其中在吸烟烟草和吸烟烟草制品中，这些香气和口味都在主流和侧流中都在吸烟之前和之后。

54. 发明授权

US4489009A Process for producing solanone, norsolanadione and intermediates therefor 失效
标题翻译：制备索罗酮，二酰甘油和其中间体的方法
公开(公告)号：US4489009A
公开(公告)日：1984-12-18
申请号：US511944
申请日：1983-07-08
申请人： Kenneth K. Light , William L. Schreiber , Joseph A. McGhie , Ronald P. Schreck , Takao Yoshida , Loren B. Schreiber , Ranya Muralidhara
发明人： Kenneth K. Light , William L. Schreiber , Joseph A. McGhie , Ronald P. Schreck , Takao Yoshida , Loren B. Schreiber , Ranya Muralidhara
IPC分类号： A23L27/20 , A24B15/32 , C07C45/51 , C07C45/59 , C07C45/66 , C07C309/28 , C07D295/02 , C07D295/03 , C07D295/145 , C07D295/155 , C07D317/30 , C07C121/34 , C07C121/30
CPC分类号： C07D295/03 , A23L27/202 , A24B15/32 , C07C255/00 , C07C309/28 , C07C45/516 , C07C45/59 , C07C45/66 , C07D295/145 , C07D295/155 , C07D317/30
摘要： Described is a process for preparing solanone and norsolanadione using chemical intermediates: which provide an organoleptically improved smoking tobacco product and additives therefor.
摘要翻译：描述了使用化学中间体制备Solone和Norsolanadione的方法：其提供感官改进的吸烟产品及其添加剂。 + PG]

55. 发明授权

US4412083A Process for producing solanone, norsolanadione and intermediates therefor 失效
标题翻译：制备索罗酮，二酰甘油和其中间体的方法
公开(公告)号：US4412083A
公开(公告)日：1983-10-25
申请号：US357158
申请日：1982-03-11
申请人： Kenneth K. Light , William L. Schreiber , Joseph A. McGhie , Ronald P. Schreck , Takao Yoshida , Loren B. Schreiber , Ranya Muralidhara
发明人： Kenneth K. Light , William L. Schreiber , Joseph A. McGhie , Ronald P. Schreck , Takao Yoshida , Loren B. Schreiber , Ranya Muralidhara
IPC分类号： A23L27/20 , A24B15/32 , C07C45/42 , C07C45/51 , C07C45/59 , C07C45/66 , C07D295/02 , C07D295/03 , C07D295/145 , C07D295/155 , C07D309/28 , C07D317/30 , C07C119/12
CPC分类号： C07D295/03 , A23L27/2024 , A24B15/32 , C07C255/00 , C07C45/42 , C07C45/516 , C07C45/59 , C07C45/66 , C07D295/145 , C07D295/155 , C07D309/28 , C07D317/30
摘要： Described is a process for preparing solanone and norsolanadione using chemical intermediates defined according to the generic structure: ##STR1## wherein X is one of the moieties: ##STR2## wherein R represents hydrogen or methyl; wherein Y represents one of the structures: ##STR3## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; with the provisos that:(i) when Y is the moiety having the structure: ##STR4## then X is the moiety having the structure: ##STR5## (ii) when X is the moiety having the structure: ##STR6## then Y is the moiety having the structure:--C.tbd.N]In preparing solanone, the compound having the structure: ##STR7## or a mixture of compounds defined according to the structure: ##STR8## is reacted with methyl lithium and the resulting intermediate is hydrolyzed and the resulting compound is dehydrated. In producing the norsolanadione, the compound having the structure: ##STR9## or a mixture of compounds according to the structure: ##STR10## is reacted with ethylene glycol or propylene glycol thereby forming a ketal and the resulting ketal is reacted with methyl lithium and the resulting intermediate is then hydrolyzed in the presence of acid.
摘要翻译：描述了使用根据以下通用结构定义的化学中间体制备索罗酮和尼考兰那酮的方法：其中X是部分之一：其中R表示氢或甲基; 其中Y表示以下结构之一：其中一条虚线表示碳 - 碳单键，另一条虚线表示碳 - 碳双键; 条件是：（i）当Y是具有以下结构的部分时：X是具有以下结构的部分：（ⅱ）当X是具有以下结构的部分时，则Y是具有以下结构的部分：-C 3 N N]在制备solone的过程中，将具有以下结构的化合物：IMAGE或根据结构定义的化合物的混合物与甲基锂反应，并将所得中间体水解，所得化合物脱水。在制备硝酰甘油的过程中，将具有以下结构的化合物：IMAGE或根据以下结构的化合物的混合物与乙二醇或丙二醇反应，从而形成缩酮，得到的缩酮与甲基锂反应，得到的中间体然后在酸的存在下水解。

56. 发明授权

US4136120A Process for the preparation of butenoyl norbornenes 失效
标题翻译：制备丁腈橡胶的方法
公开(公告)号：US4136120A
公开(公告)日：1979-01-23
申请号：US860141
申请日：1977-12-13
申请人： Kenneth K. Light , James M. Sanders , Manfred H. Vock , Edward J. Schuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja D. Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James M. Sanders , Manfred H. Vock , Edward J. Schuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja D. Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44 , C07C45/00
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： A process is disclosed comprising adding a compound, 2-acetyl-3,3-dimethyl-5-norbornene having the structure: ##STR1## to acetaldehyde according to the reaction sequence: ##STR2## whereby a compound having the structure: ##STR3## is formed useful as an organoleptic.

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