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51. 发明授权

US5218044A Blends of modified radial polymers and engineering thermoplastic polymers 失效
标题翻译：改性径向聚合物和工程热塑性聚合物的共混物
公开(公告)号：US5218044A
公开(公告)日：1993-06-08
申请号：US505373
申请日：1990-04-06
申请人： Richard Gelles , Carl L. Willis , John E. Gorman , Andres M. Arismendi, Jr.
发明人： Richard Gelles , Carl L. Willis , John E. Gorman , Andres M. Arismendi, Jr.
IPC分类号： C08L53/00 , C08L67/02 , C08L71/12 , C08L77/00
CPC分类号： C08L53/005 , C08L67/02 , C08L71/123 , C08L77/00
摘要： A super-tough polymeric composition comprising an engineering thermoplastic and a modified radial polymer. The engineering thermoplastic is selected from the group consisting of polyamides, thermoplastic polyesters, polyphenylene ether resins, polyarylene sulfide resins, polysulfone and the like. The modified radial polymer is modified by grafting a compound containing a carboxylic acid or carboxylic acid derivative group. The modified, radial polymer has from about 3 to about 50 arms, as determined using light scattering techniques and the arms will be olefin polymers. The polymer compositions will yield shaped articles which fail ductilely when tested using ASTM procedure D-256 at room temperature and some at -20.degree. F.
摘要翻译：包含工程热塑性塑料和改性径向聚合物的超韧性聚合物组合物。工程热塑性塑料选自聚酰胺，热塑性聚酯，聚苯醚树脂，聚芳硫醚树脂，聚砜等。通过接枝含有羧酸或羧酸衍生物基团的化合物改性改性的径向聚合物。修饰的径向聚合物具有约3至约50个臂，如使用光散射技术测定的，臂将为烯烃聚合物。聚合物组合物将产生成形制品，当在室温下使用ASTM程序D-256进行测试并且在-20°F下测试时，会使其延性失效。

52. 发明授权

US5002676A Block copolymers 失效
标题翻译：嵌段共聚物
公开(公告)号：US5002676A
公开(公告)日：1991-03-26
申请号：US446827
申请日：1989-12-06
申请人： Carl L. Willis , Donn A. DuBois
发明人： Carl L. Willis , Donn A. DuBois
IPC分类号： C08F8/04 , C08F297/02 , C10M145/14 , C10N30/02 , C10N30/04 , C10N60/02
CPC分类号： C10M145/14 , C08F8/04 , C10M2205/06 , C10M2209/084 , C10N2240/02 , C10N2240/08
摘要： Novel, selectively hyrogenated block compolymers, which compolymers comprise at least one block of polymerized alkyl methacrylate and one block of polymerized conjugated alkadiene, provide improved dispersant properties and viscosity index improvement to hydrocarbon lubricating oils.

53. 发明授权

US4970265A Functionalized polymers and process for modifying unsaturated polymers 失效
标题翻译：官能化聚合物和改性不饱和聚合物的方法
公开(公告)号：US4970265A
公开(公告)日：1990-11-13
申请号：US329059
申请日：1989-03-27
申请人： Carl L. Willis
发明人： Carl L. Willis
IPC分类号： C08F8/00 , C08F8/04
CPC分类号： C08F8/00 , C08F8/04
摘要： Unsaturated hydrocarbon polymers are hydrogenated in the presence of a catalyst obtained by combining a Group VIII-A metal alkoxide or carboxylate and an alkyl or hydride of a metal selected from Groups I-A, II-A and III-B and then functionalized by contacting the hydrogenated polymer with a functionalizing agent before the hydrogenation catalyst is quenched or otherwise deactivated. The hydrogenation is, generally, accomplished at relatively mild conditions to avoid degradation of the polymer and, in the case of unsaturated copolymers comprising aromatic unsaturation, to avoid any significant hydrogenation of the aromatic unsaturation. Generally, the hydrogen partial pressure employed will be below about 1000 psig and the hydrogenation temperature will be below about 125.degree. C. The hydrogenated polymer may be functionalized by reaction with functionalizing agent select from the group carbon dioxide, ethylene oxide, aldehydes, ketones, carboxylic acid salts and esters, halides, epoxides, sulfur, boron alkoxides, isocyanates, various silicon compounds and the like. Carbon dioxide is a particularly preferred functionalizing agent since the thus functionalized polymer is useful as a modifier in sheet and bulk molding compositions and readily responds to the presence of thickening agents.
摘要翻译：不饱和烃聚合物在通过将VIII-A族金属醇盐或羧酸盐与选自IA，II-A和III-B族的金属的烷基或氢化物组合而获得的催化剂存在下氢化，然后通过使氢化在氢化催化剂淬灭或以其它方式失活之前，使用官能化剂的聚合物。通常在相对温和的条件下进行氢化以避免聚合物的降解，并且在包含芳族不饱和键的不饱和共聚物的情况下，以避免芳族不饱和度的任何明显氢化。一般来说，所用的氢气分压将低于约1000psig，氢化温度将低于约125℃。氢化聚合物可以通过与选自二氧化碳，环氧乙烷，醛，酮，羧酸盐和酯，卤化物，环氧化物，硫，硼醇盐，异氰酸酯，各种硅化合物等。二氧化碳是特别优选的官能化剂，因为如此官能化的聚合物可用作片材和本体模塑组合物中的改性剂，并且容易响应增稠剂的存在。

54. 发明授权

US4868245A Modified block copolymers having carboxyl groups grafted on the alkenyl arene blocks 失效
标题翻译：具有接枝在烯基芳烃嵌段上的羧基的改性嵌段共聚物
公开(公告)号：US4868245A
公开(公告)日：1989-09-19
申请号：US79380
申请日：1987-07-30
申请人： Lorelle Pottick , Carl L. Willis , William P. Gergen , Robert G. Lutz
发明人： Lorelle Pottick , Carl L. Willis , William P. Gergen , Robert G. Lutz
IPC分类号： C08L67/00 , C08F8/00 , C08F8/04 , C08F8/30 , C08F285/00 , C08F287/00 , C08L23/00 , C08L51/00 , C08L51/02 , C08L53/02 , C08L77/00 , C08L101/00
CPC分类号： C08F8/00 , C08F8/04 , C08F8/30 , C08L53/025
摘要： A thermoplastic polymer and an article of manufacture consisting essentially of this polymer are described herein which possess excellent mechanical properties at both room and elevated temperatures. The polymer is obtained by modifying a block copolymer composed of a conjugated diene compound and an alkenyl arene compound. The block copolymer is first selectively hydrogenated and thereafter modified by grafting carboxyl containing functional groups primarily in the alkenyl arene block via metalation. The mechanical properties may be varied and controlled by varying the degree of functionalization (amount of carboxyl groups), and the degree of neutralization of the carboxyl groups from an acid to a metal carboxylate salt.
摘要翻译：本文描述了基本上由该聚合物组成的热塑性聚合物和制品，其在室温和高温下具有优异的机械性能。通过改性由共轭二烯化合物和烯基芳烃化合物组成的嵌段共聚物来获得聚合物。首先将嵌段共聚物选择性氢化，然后通过金属化将羧基官能团主要在烯基芳烃嵌段中接枝进行改性。可以通过改变官能度（羧基量）和羧基从酸中和到金属羧酸盐的程度来改变和控制机械性能。

55. 发明授权

US4433981A CO.sub.2 Removal from gaseous streams 失效
标题翻译： CO2从气流中去除
公开(公告)号：US4433981A
公开(公告)日：1984-02-28
申请号：US277513
申请日：1981-06-26
申请人： Lynn H. Slaugh , Carl L. Willis
发明人： Lynn H. Slaugh , Carl L. Willis
IPC分类号： B01J20/04 , B01D53/04
CPC分类号： B01J20/041 , B01J20/08 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J20/3433 , B01J20/3483 , Y02C10/08
摘要： Carbon dioxide is removed from a gaseous stream by contacting the stream with an adsorbent prepared by impregnating a porous aluminum with an alkali metal or alkaline earth metal oxide or salt decomposable upon calcination and subsequently calcining the impregnated alumina at about 350.degree. C.-700.degree. C.
摘要翻译：通过使物流与通过浸渍具有碱金属或碱土金属氧化物的多孔铝或通过煅烧分解的盐制备的吸附剂接触，从而从气流中除去二氧化碳，随后在约350℃-700℃下煅烧浸渍的氧化铝 C。

56. 发明授权

US4405772A Butene-1/4-vinylcyclohexene copolymer 失效
标题翻译：丁烯-1 / 4-乙烯基环己烯共聚物
公开(公告)号：US4405772A
公开(公告)日：1983-09-20
申请号：US391202
申请日：1982-06-23
申请人： Pui K. Wong , Carl L. Willis , Thomas F. Brownscombe
发明人： Pui K. Wong , Carl L. Willis , Thomas F. Brownscombe
IPC分类号： C08F210/08 , C08F236/20
CPC分类号： C08F236/20 , C08F210/08
摘要： Solid copolymers of butene-1 and 4-vinylcyclohexene prepared by copolymerizing the monomers in the presence of a titanium halide coordination catalyst have an unobvious balance of properties including a broader molecular weight distribution, shorter crystallization half-time, greater isotacticity and greater crystallinity than butene-1 homopolymers prepared with identical catalysts.
摘要翻译：通过在卤化钛配位催化剂存在下共聚单体制备的丁烯-1和4-乙烯基环己烯的固体共聚物具有非常显着的性能平衡，包括比丁烯更宽的分子量分布，更短的结晶半衰期，更大的全同立构规整度和更大的结晶度 -1均聚物用相同的催化剂制备。

57. 发明授权

US09861941B2 Modified sulfonated block copolymers and the preparation thereof 有权
公开(公告)号：US09861941B2
公开(公告)日：2018-01-09
申请号：US13181306
申请日：2011-07-12
申请人： Carl L. Willis
发明人： Carl L. Willis
IPC分类号： B01D61/46 , B01D71/80 , C08F8/36 , B01D61/44 , B01D61/48 , B01D71/28 , B01D71/68 , C02F1/44 , C02F1/469 , H01M8/1023 , H01M8/103
CPC分类号： B01D71/80 , B01D61/445 , B01D61/48 , B01D71/28 , B01D71/68 , C02F1/441 , C02F1/445 , C02F1/4693 , C02F1/4695 , C08F8/36 , H01M8/1023 , H01M8/103 , Y10T442/20 , Y10T442/2762 , C08F297/02
摘要： Described herein are modified sulfonated block copolymers which comprise at least two polymer end blocks A and at least one polymer interior block B, wherein each A block contains essentially no sulfonic acid or sulfonate functional groups and each B block comprises sulfonation susceptible monomer units and, based on the number of the sulfonation susceptible monomer units, from about 10 to about 100 mol % of a functional group of formula (I) —SO2—NR1R2 (I) or of a salt thereof, methods of making them as well as methods of using them, e.g., as membrane materials for electrically or osmotically driven applications.

58. 发明申请

US20130015071A1 MODIFIED SULFONATED BLOCK COPOLYMERS AND THE PREPARATION THEREOF 有权
标题翻译：改性磺化嵌段共聚物及其制备方法
公开(公告)号：US20130015071A1
公开(公告)日：2013-01-17
申请号：US13181306
申请日：2011-07-12
申请人： Carl L. Willis
发明人： Carl L. Willis
IPC分类号： B01D61/46 , B32B5/02 , C08F236/10
CPC分类号： B01D71/80 , B01D61/445 , B01D61/48 , B01D71/28 , B01D71/68 , C02F1/441 , C02F1/445 , C02F1/4693 , C02F1/4695 , C08F8/36 , H01M8/1023 , H01M8/103 , Y10T442/20 , Y10T442/2762 , C08F297/02
摘要： Described herein are modified sulfonated block copolymers which comprise at least two polymer end blocks A and at least one polymer interior block B, wherein each A block contains essentially no sulfonic acid or sulfonate functional groups and each B block comprises sulfonation susceptible monomer units and, based on the number of the sulfonation susceptible monomer units, from about 10 to about 100 mol % of a functional group of formula (I) —SO2—NR1R2 (I) or of a salt thereof, methods of making them as well as methods of using them, e.g., as membrane materials for electrically or osmotically driven applications.
摘要翻译：本文描述的是改性的磺化嵌段共聚物，其包含至少两个聚合物端嵌段A和至少一个聚合物内部嵌段B，其中每个A嵌段基本上不含磺酸或磺酸盐官能团，并且每个B嵌段包含磺化敏感的单体单元和基于对于磺化易感单体单元的数量，约10至约100摩尔％的式（I）-SO 2 -NR 1 R 2（I）的官能团或其盐，制备它们的方法以及使用方法它们例如用作用于电驱动或渗透驱动应用的膜材料。

59. 发明申请

US20090234059A1 MIKTOPOLYMER COMPOSITIONS 有权
标题翻译： MIKTOPOLYMER组合物
公开(公告)号：US20090234059A1
公开(公告)日：2009-09-17
申请号：US12401878
申请日：2009-03-11
申请人： Dale Lee Handlin, JR. , Peter Pasman , Glenn H. Fredrickson , Carl L. Willis , Robert C. Bening
发明人： Dale Lee Handlin, JR. , Peter Pasman , Glenn H. Fredrickson , Carl L. Willis , Robert C. Bening
IPC分类号： C08L53/00 , C08F2/01
CPC分类号： C08F236/10 , C08F297/04 , C08F297/044 , C08L53/02 , C08L53/025 , C08L2666/02
摘要： The present invention provides a block copolymer composition and method of making the same having the structures (A2-B)n-X-(A1) or (A2-B2)n-X-(B1A1), where A1 and A2 are each a polymer block of a monoalkenyl arene and B, B1, and B2 are each a polymer block of one or more conjugated dienes or a hydrogenated diene polymer, n is an integer from 2 to 30 and X is the residue of a coupling agent.
摘要翻译：本发明提供了具有（A2-B）nX-（A1）或（A2-B2）nX-（B1A1）结构的嵌段共聚物组合物及其制备方法，其中A1和A2各自为单链烯基芳烃和B，B1和B2各自为一个或多个共轭二烯或氢化二烯聚合物的聚合物嵌段，n为2至30的整数，X为偶联剂的残基。

60. 发明授权

US07141621B2 Gels from controlled distribution block copolymers 有权
公开(公告)号：US07141621B2
公开(公告)日：2006-11-28
申请号：US10359462
申请日：2003-02-06
申请人： David J. St. Clair , Dale Lee Handlin, Jr. , Carl L. Willis
发明人： David J. St. Clair , Dale Lee Handlin, Jr. , Carl L. Willis
IPC分类号： C08L53/02
CPC分类号： C09J153/02 , C08F287/00 , C08F297/04 , C08L23/10 , C08L53/02 , C08L53/025 , C08L77/00 , C08L95/00 , C08L101/00 , C08L2666/02 , C08L2666/24 , C09D153/02 , C09D153/025 , C09J153/025 , C08L2666/04 , C08L53/00
摘要： The present invention relates to gels prepared from novel anionic block copolymers of mono alkenyl arenes and conjugated dienes, and to blends of such block copolymers with other polymers. The block copolymers are selectively hydrogenated and have mono alkenyl arene end blocks and controlled distribution blocks of mono alkenyl arenes and conjugated dienes. The block copolymer may be combined with tackifying resins, oils and other components to form the gels of the present invention.

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