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51. 发明授权

US4310716A Process for the oligomerization of ethylene in methanol 失效
公开(公告)号：US4310716A
公开(公告)日：1982-01-12
申请号：US179005
申请日：1980-08-18
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： C07C2/32 , B01J31/00 , B01J31/18 , B01J31/22 , B01J31/24 , C07B61/00 , C07C1/00 , C07C2/36 , C07C11/02 , C07C67/00 , C07F15/04 , C08F110/02 , C07C2/02
CPC分类号： B01J31/2247 , B01J31/2404 , C07C2/36 , C07F15/04 , C08F110/02 , B01J2231/20 , B01J2531/847 , B01J2540/32 , B01J31/1895 , C07C2531/24 , Y02P30/42
摘要： Ethylene is oligomerized by reacting ethylene in methanol under oligomerization conditions in contact with a nickel ylide defined by the following Formula I: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 are either alike or different members selected from the group consisting of hydrogen, alkyl radicals having from about one to about 24 carbon atoms, preferably from about one to about 10 carbon atoms; aryl radicals having from about six to about 20 carbon atoms, preferably from about six to about 10 carbon atoms; alkenyl radicals having from about two to about 30 carbon atoms, preferably from about two to about 20 carbon atoms; cycloalkyl radicals having from about three to about 40 carbon atoms, preferably about three to about 30 carbon atoms; aralkyl and alkaryl radicals having from about six to about 40 carbon atoms, preferably from about six to about 30 carbon atoms; a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine; a hydroxyl group; an alkoxy or aryloxy group; and a hydrocarbyl group, such as defined above, carrying halogen, hydroxyl or alkoxy or aryloxy; provided that at least one, preferably from about one to about four, of each of R.sub.1 to R.sub.8 is a sulfonato group (--SO.sub.3.sup.-) or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl group carrying a sulfonato group; M is sulfur or oxygen, preferably oxygen; E is phosphorus, arsenic, antimony or nitrogen, preferably phosphorus; and F is phosphorus, arsenic or antimony, preferably phosphorus. There is thus obtained a reaction product containing (A) a methanol phase having dissolved therein the nickel ylide catalyst and (B) an alpha olefin phase. These two phases are then separated from each other to recover the alpha olefin phase. The use of methanol as the solvent medium causes the reaction product to resolve itself into two phases, an upper phase containing most of the oligomer product and a lower methanol phase carrying the catalyst dissolved therein. This permits easy separation of the product from the reaction mixture and also permits effective recycle of methanol with dissolved catalyst. The product obtained contains normal alpha olefins having from about four to about 100 carbon atoms, generally from about four to about 50 carbon atoms.

52. 发明授权

US08859473B2 Post-treated additive composition and method of making the same 有权
公开(公告)号：US08859473B2
公开(公告)日：2014-10-14
申请号：US12341432
申请日：2008-12-22
申请人： James J. Harrison , Mitra Hosseini
发明人： James J. Harrison , Mitra Hosseini
IPC分类号： C10M133/56
CPC分类号： C08F8/32 , C08F8/00 , C08F2810/20 , C10L1/221 , C10L1/2364 , C10L10/18 , C10M133/56 , C10M177/00 , C10M2215/28 , C10N2230/041 , C10N2230/68 , C10N2240/10 , C10N2260/06 , C10N2260/00 , C08F255/08 , C08F8/48
摘要： An oil-soluble lubricating oil additive composition prepared by the process which comprises reacting (A) reacting a copolymer of an (i) an unsaturated acidic reagent; and (ii) a mono-olefin, with at least one linking hydrocarbyl di-primary amine, thereby producing a hybrid succinic anhydride copolymer having from about 10% to about 90% unreacted anhydride groups; and subsequently (B) reacting the hybrid succinic anhydride copolymer with a second amine compound, thereby producing the succinimide; and (C) reacting the succinimide with at least one post-treating agent selected from a cyclic carbonate, a linear mono-carbonate, a linear poly-carbonate, an aromatic polycarboxylic acid, an aromatic polycarboxylic anhydride, an aromatic polycarboxylic acid ester, or mixtures thereof.

53. 发明授权

US08748359B2 Post-treated additive composition and method of making the same 有权
标题翻译：后处理添加剂组合物及其制备方法
公开(公告)号：US08748359B2
公开(公告)日：2014-06-10
申请号：US13685904
申请日：2012-11-27
申请人： James J. Harrison , Mitra Hosseini
发明人： James J. Harrison , Mitra Hosseini
IPC分类号： C10M149/12
CPC分类号： C08F8/32 , C08F8/00 , C08F2810/20 , C10L1/221 , C10L1/2364 , C10L10/18 , C10M133/56 , C10M177/00 , C10M2215/28 , C10N2230/041 , C10N2230/68 , C10N2240/10 , C10N2260/06 , C10N2260/00 , C08F255/08 , C08F8/48
摘要： An oil-soluble lubricating oil additive composition prepared by the process which comprises reacting (A) reacting a copolymer of an (i) an unsaturated acidic reagent; and (ii) a mono-olefin, with at least one linking hydrocarbyl di-primary amine, thereby producing a hybrid succinic anhydride copolymer having from about 10% to about 90% unreacted anhydride groups; and subsequently (B) reacting the hybrid succinic anhydride copolymer with a second amine compound, thereby producing the succinimide; and (C) reacting the succinimide with at least one post-treating agent selected from a cyclic carbonate, a linear mono-carbonate, a linear poly-carbonate, an aromatic polycarboxylic acid, an aromatic polycarboxylic anhydride, an aromatic polycarboxylic acid ester, or mixtures thereof.
摘要翻译：一种通过该方法制备的油溶性润滑油添加剂组合物，其包括使（A）使（i）不饱和酸性试剂的共聚物与和（ii）具有至少一个连接的烃基二伯胺的单烯烃，从而产生具有约10％至约90％未反应的酸酐基团的杂化琥珀酸酐共聚物; 然后（B）使杂化琥珀酸酐共聚物与第二胺化合物反应，从而制备琥珀酰亚胺; 和（C）使琥珀酰亚胺与至少一种选自环状碳酸酯，直链单碳酸酯，直链多元碳酸酯，芳族多元羧酸，芳族多羧酸酐，芳族多元羧酸酯的后处理剂反应，或其混合物。

54. 发明授权

US08530586B2 Method for preparing polyolefins containing a high percentage of exo-olefin chain ends 有权
标题翻译：制备含有高百分比的外烯链末端的聚烯烃的方法
公开(公告)号：US08530586B2
公开(公告)日：2013-09-10
申请号：US12767672
申请日：2010-04-26
申请人： Casey D. Stokes , Kelby Simison , Robson F. Storey , James J. Harrison
发明人： Casey D. Stokes , Kelby Simison , Robson F. Storey , James J. Harrison
IPC分类号： C08F214/02
CPC分类号： C08F8/26 , C08F8/00 , C08F110/10 , C08F2810/30 , C08F2810/40 , C08F2/38 , C08F2500/03
摘要： The present invention is directed to a method for preparing polyolefins containing a high percentage of exo-olefin chain ends. The method involves ionizing a polyolefin containing tert-chloride chain ends and reacting the ionized polyolefin with one or more nitrogen-containing five-membered aromatic ring or one or more hindered secondary or tertiary amines, or mixtures thereof.
摘要翻译：本发明涉及一种制备含有高百分比的外烯链末端的聚烯烃的方法。该方法包括使包含氯化物链末端的聚烯烃电离，并使离子化聚烯烃与一种或多种含氮五元芳环或一个或多个受阻仲胺或叔胺或其混合物反应。

55. 发明授权

US08362153B2 Polyisobutenyl sulfonates having low polydispersity 有权
标题翻译：具有低多分散性的聚异丁烯基磺酸盐
公开(公告)号：US08362153B2
公开(公告)日：2013-01-29
申请号：US11611753
申请日：2006-12-15
申请人： James J. Harrison
发明人： James J. Harrison
IPC分类号： C08F271/02
CPC分类号： C10M151/02 , C08F8/44 , C08F110/10 , C10M135/10 , C10M151/04 , C10M159/24 , C10M2219/044 , C10M2219/046 , C10M2221/04 , C10N2220/021 , C10N2230/02 , C10N2230/04 , C08F2/42 , C08F2500/17 , C08F2500/03 , C10N2210/01 , C08F8/36
摘要： The present invention provides for polyisobutenyl sulfonates, methods for preparing them, and composition employing them; wherein said polyisobutenyl sulfonates have improved low temperature and high temperature viscometric properties. The polyisobutenyl sulfonates are prepared by sulfonating polyisobutene and reacting the polyisobutenyl sulfonate with an alkali metal or alkaline earth metal, wherein the polyisobutene is characterized by having at least 90 mole percent methyl-vinylidene, a number average molecular weight of about 350 to 5,000, and a ratio of weight average molecular weight to number average molecular weight Mw/Mn of from about 1.01 to about 1.4.
摘要翻译：本发明提供聚异丁烯基磺酸盐，其制备方法和使用它们的组合物; 其中所述聚异丁烯基磺酸盐具有改善的低温和高温粘度特性。聚异丁烯基磺酸盐通过磺化聚异丁烯并使聚异丁烯基磺酸盐与碱金属或碱土金属反应制备，其中聚异丁烯的特征在于具有至少90摩尔％的甲基亚乙烯基，数均分子量为约350至5,000，和重均分子量与数均分子量Mw / Mn的比例为约1.01至约1.4。

56. 发明申请

US20120310911A1 Search Engine Identifying Chemical Products 审中-公开
标题翻译：搜索引擎识别化学产品
公开(公告)号：US20120310911A1
公开(公告)日：2012-12-06
申请号：US13509570
申请日：2010-11-12
申请人： James J. Harrison
发明人： James J. Harrison
IPC分类号： G06F17/30
CPC分类号： G06Q30/0603 , G16C20/90
摘要： Systems and methods for efficiently searching a businesses' product inventory using competitor's trade name information as a search term to find relevant results. Such a system is for use on a general purpose computer in the form of a search engine using a user interface, a directory store of product information, according to a predetermined taxonomy and a way to display, print, or otherwise deliver search results.
摘要翻译：使用竞争对手的商品名称信息作为搜索词来有效地搜索企业的产品库存的系统和方法，以找到相关的结果。这样的系统用于使用用户界面的搜索引擎的形式的通用计算机，根据预定的分类法的产品信息的目录存储以及显示，打印或以其它方式传送搜索结果的方式。

57. 发明申请

US20120253065A1 MANNICH CONDENSATION PRODUCTS USEFUL AS SEQUESTERING AGENTS 有权
标题翻译： MANNICH CONDENSATION产品有用作为序列代理
公开(公告)号：US20120253065A1
公开(公告)日：2012-10-04
申请号：US13467336
申请日：2012-05-09
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C07C229/14 , C07C227/18
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.
摘要翻译：本发明涉及Mannich缩合产物螯合剂或用于燃料和润滑油的曼尼期缩合产物螯合剂的混合物。本发明还涉及制备曼尼期缩合产物螯合剂的方法。本发明还涉及通过在反应条件下将聚异丁基取代的羟基芳族化合物，醛，氨基酸或其酯与碱金属碱组合以形成曼尼期缩合产物螯合剂形成的产物。本发明还涉及具有本发明的曼尼期缩合产物螯合剂的润滑油组合物，润滑油浓缩物，燃料组合物和燃料浓缩物。

58. 发明申请

US20120190864A1 PROCESS FOR PREPARATION OF HIGH MOLECULAR WEIGHT MOLYBDENUM SUCCINIMIDE COMPLEXES 有权
标题翻译：高分子量钼多糖复合物的制备方法
公开(公告)号：US20120190864A1
公开(公告)日：2012-07-26
申请号：US13011520
申请日：2011-01-21
申请人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
发明人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
IPC分类号： C07F11/00
CPC分类号： C07D403/12 , C10M159/18 , C10M2201/062 , C10M2201/08 , C10M2201/081 , C10M2215/28 , C10M2227/09 , C10N2210/06 , C10N2270/00
摘要： Disclosed is a process for preparing a molybdated succinimide complex, the process comprising: (a) reacting an alkyl or alkenyl mono- or bis-succinimide of a polyamine of formula I or formula II or mixtures thereof: wherein R is an alkyl or alkenyl group having a number average molecular weight of about 500 to about 5,000, R′ is a straight or branched-chain alkylene group having 2 to 3 carbon atoms, x is 2 to 11, and y is 1 to 10, with an α,β-unsaturated mono-carboxylic acid or carboxylic acid ester, in a charge mole ratio of the α,β-unsaturated mono-carboxylic acid or carboxylic acid ester to the succinimide of formula I or formula II or mixtures thereof of greater than 1.05:1 to about 6:1, and wherein the reaction temperature is in the range of from greater than 80° C. to no greater than about 150° C.; and (b) reacting the succinimide product of step (a) with an acidic molybdenum compound to provide the molybdated succinimide complex, wherein the molybdated succinimide complex is a liquid at room temperature.
摘要翻译：公开了一种制备钼酸化琥珀酰亚胺复合物的方法，该方法包括：（a）使式I或式II的多胺或其混合物的烷基或烯基单 - 或二 - 琥珀酰亚胺反应：其中R是烷基或链烯基数均分子量为约500〜约5000，R'为碳原子数2〜3的直链或支链亚烷基，x为2〜11，y为1〜10，α，bgr; - 不饱和单羧酸或羧酸酯，以α，bgr-不饱和单羧酸或羧酸酯与式I或式II的琥珀酰亚胺或其混合物的摩尔比大于1.05:1 至约6:1，并且其中反应温度在大于80℃至不大于约150℃的范围内。和（b）使步骤（a）的琥珀酰亚胺产物与酸性钼化合物反应以提供钼酸化琥珀酰亚胺配合物，其中钼酸化琥珀酰亚胺络合物在室温下为液体。

59. 发明授权

US08198225B2 Sulfurized metal alkyl phenate compositions having a low alkyl phenol content 有权
标题翻译：具有低烷基苯酚含量的硫化金属烷基酚盐组合物
公开(公告)号：US08198225B2
公开(公告)日：2012-06-12
申请号：US11946878
申请日：2007-11-29
申请人： James J. Harrison , John McDonald
发明人： James J. Harrison , John McDonald
IPC分类号： C10M105/72 , C10M135/30 , C10M159/22
CPC分类号： C08G8/28 , C08L61/14 , C10M135/30 , C10M2219/087 , C10M2219/089 , C10N2230/04
摘要： Provided herein are sulfurized metal alkyl phenate compositions having a low alkyl phenol content. The sulfurized metal alkyl phenate compositions can be prepared by reacting a phenol compound of Formula (I) disclosed herein with an aldehyde to form a phenolic resin of Formula (II) disclosed herein and then by reacting the phenolic resin simultaneously with a metal base and a first sulfurizing agent. The sulfurized metal alkyl phenate compositions and the overbased sulfurized metal alkyl phenate compositions disclosed herein may be used as detergents for formulating lubricating oil compositions. The lubricating oil compositions disclosed herein have a reduced amount of the free phenol compound and a salt thereof.
摘要翻译：本文提供了具有低烷基苯酚含量的硫化金属烷基酚盐组合物。硫化金属烷基酚盐组合物可以通过使本文公开的式（I）的酚化合物与醛反应以形成本文公开的式（II）的酚醛树脂，然后通过使酚醛树脂与金属碱和第一次硫化剂。本文公开的硫化金属烷基酚盐组合物和高碱性硫化金属烷基酚盐组合物可用作配制润滑油组合物的洗涤剂。本文公开的润滑油组合物具有减少量的游离酚化合物及其盐。

60. 发明授权

US07964543B2 Mannich condensation products useful as sequestering agents 有权
标题翻译：曼尼希缩合产物可用作螯合剂
公开(公告)号：US07964543B2
公开(公告)日：2011-06-21
申请号：US11105606
申请日：2005-04-13
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C10M159/16 , C07C55/10
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.
摘要翻译：本发明涉及Mannich缩合产物螯合剂或用于燃料和润滑油的曼尼期缩合产物螯合剂的混合物。本发明还涉及制备曼尼期缩合产物螯合剂的方法。本发明还涉及通过在反应条件下将聚异丁基取代的羟基芳族化合物，醛，氨基酸或其酯与碱金属碱组合以形成曼尼期缩合产物螯合剂形成的产物。本发明还涉及具有本发明的曼尼期缩合产物螯合剂的润滑油组合物，润滑油浓缩物，燃料组合物和燃料浓缩物。

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