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51. 发明申请

US20080096761A1 Preparation of supports for catalysts 审中-公开
标题翻译：催化剂载体的制备
公开(公告)号：US20080096761A1
公开(公告)日：2008-04-24
申请号：US10588390
申请日：2005-02-02
申请人： Shahram Mihan , Michael Hesse
发明人： Shahram Mihan , Michael Hesse
IPC分类号： B01J32/00
CPC分类号： C08F210/16 , B01J37/036 , C08F4/65912 , C08F4/65925 , C08F10/00 , C08F4/025 , C08F4/24 , C08F4/65916
摘要： The invention relates to a process for preparing a support for catalysts, which comprises: a) preparing a hydrogel; b) milling the hydrogel to give a finely particulate hydrogel; c) producing a slurry based on the finely particulate hydrogel; d) drying the slurry comprising the finely particulate hydrogel to give the support for catalysts, wherein a finely particulate hydrogel in which at least 5% by volume of the particles, based on the total volume of the particles, have a particle size in the range from >0 μm to ≦3 μm; and/or at least 40% by volume of the particles, based on the total volume of the particles, have a particle size in the range from >0 μm to ≦12 μm, and/or at least 75% by volume of the particles, based on the total volume of the particles, have a particle size in the range from >0 μm to ≦35 μm, is produced in step b).
摘要翻译：本发明涉及一种制备催化剂载体的方法，其包括：a）制备水凝胶; b）研磨水凝胶以得到细颗粒水凝胶; c）基于细颗粒水凝胶生产浆料; d）干燥包含细颗粒状水凝胶的浆料，得到催化剂载体，其中细颗粒状水凝胶，其中基于颗粒总体积的至少5体积％的颗粒的粒径范围从0um到<= 3mum; 和/或至少40体积％的颗粒，基于颗粒的总体积，其粒度范围为>0μm至≤12μm，和/或至少75体积％基于粒子的总体积的颗粒的粒度在>0μm至<=35μm的范围内，在步骤b）中产生。

52. 发明申请

US20070227898A1 Method for Electrochemical Production of a Crystalline Porous Metal Organic Skeleton Material 有权
标题翻译：一种结晶多孔金属有机骨架材料的电化学生产方法
公开(公告)号：US20070227898A1
公开(公告)日：2007-10-04
申请号：US10580407
申请日：2004-11-22
申请人： Ulrich Muller , Hermann Putter , Michael Hesse , Markus Schubert , Helge Wessel , Jurgen Huff , Marcus Guzmann
发明人： Ulrich Muller , Hermann Putter , Michael Hesse , Markus Schubert , Helge Wessel , Jurgen Huff , Marcus Guzmann
IPC分类号： C25B3/12
CPC分类号： C25B3/12 , B01D53/02 , B01D2253/204 , B01J20/226 , B01J20/28014 , B01J20/28042 , B01J31/1691 , B01J31/1805 , B01J31/1815 , B01J31/2239 , B01J31/226 , B01J2531/16 , B01J2531/26 , B01J2531/842 , C01B3/0015 , C01B21/0455 , C01B23/0057 , F17C11/005 , H01M8/04216 , Y02C10/08 , Y02E60/327 , Y02E60/328 , Y02P20/133 , Y02P70/56 , Y10S95/90 , Y10S502/526
摘要： A method of electrochemically preparing a crystalline, porous, metal-organic framework material comprising at least one at least bidentate organic compound coordinately bound to at least one metal ion, in a reaction medium comprising the at least one bidentate organic compound, wherein at least one metal ion is provided in the reaction medium by the oxidation of one anode comprising the corresponding metal.
摘要翻译：一种在包含至少一种二齿有机化合物的反应介质中电化学制备结晶多孔的金属 - 有机骨架材料的方法，其包含与至少一种金属离子配位结合的至少二齿有机化合物，其中至少一种金属离子通过包含相应金属的一个阳极的氧化在反应介质中提供。

53. 发明申请

US20070036697A1 Multi-zone jacketed pipe reactor for carrying out exothermic gaseous phase reactions 审中-公开
标题翻译：用于进行放热气相反应的多区夹套管式反应器
公开(公告)号：US20070036697A1
公开(公告)日：2007-02-15
申请号：US10482398
申请日：2003-12-31
申请人： Friedrich Gutlhuber , Manfred Lehr , Gunnar Heydrich , Gunther Windecker , Stephan Schlitter , Michael Hesse , Markus Rosch , Alexander Weck , Rolf Fischer
发明人： Friedrich Gutlhuber , Manfred Lehr , Gunnar Heydrich , Gunther Windecker , Stephan Schlitter , Michael Hesse , Markus Rosch , Alexander Weck , Rolf Fischer
IPC分类号： B01J19/00 , F28D21/00
CPC分类号： B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/0053 , B01J2208/00849 , B01J2219/00259 , F28D7/0066 , F28D7/0091 , F28F9/22
摘要： A multi-zone jacketed pipe reactor (2; 60; 90; 130) for carrying out exothermic gaseous phase reactions and with at least one reaction zone (I) working with vaporisation cooling, at least one reaction zone (II) working with circulation cooling and, possibly, with additional zones (III, IV) is characterised in that one reaction zone (I) working with vaporisation cooling forms the first reaction zone to which is connected an additional reaction zone (II) working with circulation cooling. In this way there occurs at the beginning of the reaction, when the latter is most violent, very intensive cooling at a precisely controllable temperature and especially as well a temperature that is constant across the entire cross-section of the reactor while subsequently in a subsequent reaction zone working with circulating cooling by means of global counter-flow guidance of the heat transfer agent a constant cooling of the reaction gas is achieved.
摘要翻译：用于进行放热气相反应的多区夹套管式反应器（2; 60; 90; 130）和至少一个用蒸发冷却工作的反应区（I），至少一个循环冷却工作的反应区（II）并且可能地具有另外的区域（III，IV），其特征在于用蒸发冷却工作的一个反应区域（I）形成连接有循环冷却工作的附加反应区域（II）的第一反应区域。以这种方式，在反应开始时发生，当后者在精确控制的温度下是最猛烈的，非常强烈的冷却，特别是在反应器的整个横截面上恒定的温度，随后在随后的反应区域通过传热剂的全局逆流引导进行循环冷却，实现了反应气体的恒定冷却。

54. 发明申请

US20060135824A1 Process for the alkoxylation of monools in the presence of metallo-organic framework materials 失效
标题翻译：在金属 - 有机骨架材料存在下烷基化单醇的方法
公开(公告)号：US20060135824A1
公开(公告)日：2006-06-22
申请号：US11285070
申请日：2005-11-23
申请人： Ulrich Mueller , Olga Metelkina , Michael Hesse , Michael Stoesser , Peter Haas , Omar Yaghi
发明人： Ulrich Mueller , Olga Metelkina , Michael Hesse , Michael Stoesser , Peter Haas , Omar Yaghi
IPC分类号： C07C41/03
CPC分类号： C08G65/2606 , C07C41/03 , C08G18/283 , C08G65/2645 , C08G65/266 , C08G2101/00 , C07C43/11
摘要： The present invention relates to a process for the alkoxylation of a monool with at least one alkoxylating agent to an alkoxylated alcohol wherein a catalyst is employed which comprises a metallo-organic framework material of metal ions and at least bidentate coordinately bound organic ligands.
摘要翻译：本发明涉及使用至少一种烷氧基化剂将烷氧基化为烷氧基化醇的方法，其中使用包含金属离子的金属有机骨架材料和至少二齿配位结合的有机配体的催化剂。

55. 发明申请

US20060099398A1 Shaped bodies containing metal-organic frameworks 有权
公开(公告)号：US20060099398A1
公开(公告)日：2006-05-11
申请号：US10983629
申请日：2004-11-09
申请人： Michael Hesse , Ulrich Muller
发明人： Michael Hesse , Ulrich Muller
IPC分类号： B27N3/00 , B32B3/00
CPC分类号： F17C11/005 , B01J20/0244 , B01J20/226 , B01J20/28011 , B01J20/2803 , B01J20/28042 , B01J20/28057 , B01J20/3007 , B01J20/3035 , B01J20/3042 , B01J31/1691 , B01J35/1028 , B01J37/0009 , B01J2231/005 , B01J2531/26 , Y02E60/324 , Y10T428/249953 , Y10T428/249967 , Y10T428/24997 , Y10T428/25 , Y10T428/298
摘要： The present invention relates to shaped bodies containing a metal-organic framework material (MOF) as well as a process for the preparation thereof and their use especially as catalyst or storage medium.

56. 发明申请

US20060052239A1 Supported catalyst containing rhenium and method for hydrogenation of hydrogenation of carbonyl compounds in liquid phase by means of said catalyst 有权
标题翻译：含有铼的载体催化剂和通过所述催化剂在液相中氢化羰基化合物的方法
公开(公告)号：US20060052239A1
公开(公告)日：2006-03-09
申请号：US10534621
申请日：2003-11-06
申请人： Markus Schubert , Michael Hesse , Rolf-Hartmuth Fischer , Take Constantinescu
发明人： Markus Schubert , Michael Hesse , Rolf-Hartmuth Fischer , Take Constantinescu
IPC分类号： B01J27/24 , C07D305/12 , C07D307/02
CPC分类号： C07D307/33 , B01J21/18 , B01J23/007 , B01J23/6567 , B01J23/688 , B01J23/84 , B01J23/8896 , B01J35/002 , B01J37/0213 , C07D307/08 , C07D315/00 , Y10S502/506 , Y10S502/512
摘要： The present invention provides a process for hydrogenating carbonyl compounds, in particular C4-dicarboxylic acids to mixtures of tetrahydrofuran and gamma-butyrolactone, over supported rhenium catalysts, wherein rhenium and at least one further metal of groups VIII or Ib of the Periodic Table of the Elements, in particular ruthenium (Ru), rhodium (Rh), palladium (Pd), osmium (Os), iridium (Ir), platinum (Pt), copper (Cu), silver (Ag) or cobalt (Co), is applied to the support in the form of at least one bimetallic precursor compound, and also to these catalysts.
摘要翻译：本发明提供了一种将羰基化合物，特别是C 4 - 二羧酸氢化成四氢呋喃和γ-丁内酯的混合物在负载的铼催化剂上的方法，其中铼和至少一种另外的VIII族金属或铑（Ru），铑（Rh），钯（Pd），锇（Os），铱（Ir），铂（Pt），铜（Cu），银（Ag ）或钴（Co）以至少一种双金属前体化合物的形式施用于载体，以及这些催化剂。

57. 发明申请

US20060035784A1 Method for removing sulfur compounds from gases containing hydrocarbons 有权
标题翻译：从含有碳氢化合物的气体中除去硫化合物的方法
公开(公告)号：US20060035784A1
公开(公告)日：2006-02-16
申请号：US10539613
申请日：2003-12-13
申请人： Helge Wessel , Markus Holzle , Bernd Vogel , Roland Hageboke , Michael Hesse , Norbert Wilden
发明人： Helge Wessel , Markus Holzle , Bernd Vogel , Roland Hageboke , Michael Hesse , Norbert Wilden
IPC分类号： B01J23/06
CPC分类号： C10L3/102 , B01D53/8603 , C10L3/10
摘要： The present invention relates to processes for removing sulfur compounds from hydrocarbonaceous gases by using catalysts, with the exception of activated carbons and zeolites, which comprise copper, silver, zinc, molybdenum, iron, cobalt, nickel or mixtures thereof at temperatures of from (−50) to 150° C. and a pressure of from 0.1 to 10 bar.
摘要翻译：本发明涉及通过使用催化剂除去含有铜，银，锌，钼，铁，钴，镍或其混合物的活性炭和沸石的烃化合物的方法，所述方法包括在（ - 50）至150℃，压力为0.1至10巴。

58. 发明授权

US06274700B1 Catalyst and method for producing polytetrahydrofuran 失效
标题翻译：催化剂和生产聚四氢呋喃的方法
公开(公告)号：US06274700B1
公开(公告)日：2001-08-14
申请号：US09555872
申请日：2000-06-08
申请人： Karsten Eller , Heinz Rütter , Michael Hesse , Rainer Becker
发明人： Karsten Eller , Heinz Rütter , Michael Hesse , Rainer Becker
IPC分类号： C08G5968
CPC分类号： C08G65/2657 , C08G65/20
摘要： In a process for preparing polytetrahydrofuran, polytetrahydrofuran copolymers or diesters or monoesters thereof by polymerization of tetrahydrofuran in the presence of at least one telogen and/or comonomer over acid-activated montmorillonite catalysts, the montmorillonite catalyst after acid activation has a ratio of montmorillonite structure to the sum of muscovite and kaolin structures, determined from the intensities of the reflections at 2&thgr;=5.5° for montmorillonite, 2&thgr;=9.0° for muscovite and 2&thgr;=12.5° for kaolin measured in the X-ray powder pattern, of at least 5:1.
摘要翻译：在通过在酸活化蒙脱石催化剂上存在至少一种环糊精和/或共聚单体的情况下通过四氢呋喃聚合制备聚四氢呋喃，聚四氢呋喃共聚物或二酯或其单酯的方法中，酸活化后的蒙脱石催化剂具有蒙脱石结构与根据X射线粉末图案测定的蒙脱石的2θ= 5.5°的反射强度，白云母的2θ= 9.0°，高岭土的2θ= 12.5°，确定白云母和高岭土结构的总和为5： 1。

59. 发明授权

US06252039B1 Method for decoloring tetrahydrofuran polymers or copolymers 失效
标题翻译：四氢呋喃聚合物或共聚物脱色方法
公开(公告)号：US06252039B1
公开(公告)日：2001-06-26
申请号：US09402895
申请日：1999-10-13
申请人： Rainer Becker , Karsten Eller , Michael Hesse
发明人： Rainer Becker , Karsten Eller , Michael Hesse
IPC分类号： C08F600
CPC分类号： C08G65/20 , C08G65/30
摘要： A process for decolorizing polymers or copolymers which are obtained by cationic polymerization of tetrahydrofuran or of tetrahydrofuran and alkylene oxide, in the presence or absence of a telogen, comprises a) first, if desired, removing the low-boiling components by vacuum distillation or extraction and b) heating the remaining polymer or copolymer in the presence of at least one auxiliary selected from the group consisting of solid oxides and/or sheet silicates to from 20 to 150° C.
摘要翻译：在存在或不存在季铵盐时，通过四氢呋喃或四氢呋喃和环氧烷的阳离子聚合获得的聚合物或共聚物的脱色方法包括：a）如果需要，首先通过真空蒸馏或萃取除去低沸点组分在选自固体氧化物和/或片状硅酸盐的至少一种辅助剂存在下将剩余的聚合物或共聚物加热至20-150℃。

60. 发明授权

US6093677A Catalyst for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone 有权
标题翻译：将1,4-丁二醇脱氢为γ-丁内酯的催化剂
公开(公告)号：US6093677A
公开(公告)日：2000-07-25
申请号：US323919
申请日：1999-06-02
申请人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
发明人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
IPC分类号： C07D307/33 , B01J23/72 , B01J23/78 , C07B61/00 , C07D315/00 , B01J23/70
CPC分类号： C07D315/00 , B01J23/78 , B01J23/72 , B01J35/0053 , B01J35/0066
摘要： A process for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone in the gas phase in the presence of a copper-containing catalyst, wherein the catalyst contains 4-40% by weight of copper and 0-5% by weight of Na.sub.2 O, based on the total weight of the catalyst, on a carrier consisting of 80-100% by weight of SiO.sub.2 and 0-20% by weight of CaO.
摘要翻译：在含铜催化剂存在下，在气相中将1,4-丁二醇脱氢为γ-丁内酯的方法，其中催化剂含有4-40重量％的铜和0-5重量％的Na 2 O，基于在由80-100重量％的SiO 2和0-20重量％的CaO组成的载体上的催化剂的总重量。

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