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51. 发明公开

KR1020090067670A 하수 슬러지에서 ＰＦＯＳ 또는 ＰＦＯＡ를 제거하는 방법 无效
标题翻译：废除污水中PFOS或PFOA的方法
公开(公告)号：KR1020090067670A
公开(公告)日：2009-06-25
申请号：KR1020070135409
申请日：2007-12-21
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： C02F11/14 , C02F1/30 , C02F9/00
CPC分类号： C02F11/14 , C02F1/30 , C02F9/00 , C02F2201/002
摘要： A method for removing PFOS(Perfluorooctane Sulfonate) or PFOA(Perfluorooctanoic Acid) from sewage sludge inexpensively and safely is provided. A method for removing PFOS(Perfluorooctane Sulfonate) or PFOA(Perfluorooctanoic Acid) from sewage sludge comprises a step(S1) of adding an oxidizer to sewage sludge containing PFOS or PFOA and a step(S2) of irradiating electromagnetic waves to the sewage sludge. The oxidizer is hydrogen peroxide or superphosphate. The electromagnetic waves are irradiated to the sewage sludge at a frequency of 2000 to 2500 MHz and an output of 80 to 120W for 2 to 10 minutes.
摘要翻译：提供了从污水污泥中廉价，安全地去除PFOS（全氟辛烷磺酸盐）或PFOA（全氟辛酸）的方法。从污水污泥中除去PFOS（全氟辛烷磺酸盐）或PFOA（全氟辛酸）的方法包括向含有PFOS或PFOA的污水污泥添加氧化剂的步骤（S1）和向污水污泥照射电磁波的步骤（S2）。氧化剂是过氧化氢或过磷酸盐。电磁波以2000〜2500MHz的频率和80〜120W的输出照射到污水污泥2〜10分钟。

52. 发明公开

KR1020090067664A 토양에서 ＰＦＯＳ 또는 ＰＦＯＡ를 제거하는 방법 失效
标题翻译：在土壤中去除PFOS或PFOA的方法
公开(公告)号：KR1020090067664A
公开(公告)日：2009-06-25
申请号：KR1020070135403
申请日：2007-12-21
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09C1/08
CPC分类号： B09C1/08 , A62D3/30
摘要： A method for removing PFOS(Perfluorooctane Sulfonate) and PFOA(Perfluorooctanoic Acid) from soil is provided to effectively remove the PFOS or PFOA contained in the soil and maintain a neutral pH suitable for the growth of the crops in the soil. A method for removing PFOS(Perfluorooctane Sulfonate) and PFOA(Perfluorooctanoic Acid) from soil comprises: a step(S1) of preparing soil contaminated with PFOS or PFOA; and a step of purifying the contaminated soil using iron oxides and sodium borohydride(NaBH4) as decomposition agents. The step of purifying the contaminated soil comprises a step(S2) of adding 1 to 100 parts by weight of the decomposition agents to 100 parts by weight of the contaminated soil and a step(S3) of leaving the decomposition agent-added soil alone for 5 days or more. The iron oxides including Fe2O3 and FeO are by-products of the pickling process in the ironmaking process. The iron oxides are formed in the form of a powder having an average particle diameter of 0.2 to 50 microns.
摘要翻译：提供从土壤中去除PFOS（全氟辛烷磺酸盐）和PFOA（全氟辛酸）的方法，以有效去除土壤中所含的全氟辛烷磺酸或PFOA，并保持适合土壤中作物生长的中性pH。从土壤中去除PFOS（全氟辛烷磺酸盐）和PFOA（全氟辛酸）的方法包括：制备受PFOS或PFOA污染的土壤的步骤（S1）; 以及使用氧化铁和硼氢化钠（NaBH4）作为分解剂来净化污染土壤的步骤。净化污染土壤的步骤包括向100重量份的污染土壤中加入1至100重量份的分解剂的步骤（S2）和将分解剂添加的土壤单独留下的步骤（S3） 5天以上。包括Fe2O3和FeO在内的铁氧化物是炼铁过程中酸洗工艺的副产物。铁氧化物以平均粒径为0.2至50微米的粉末的形式形成。

53. 发明公开

KR1020060071566A 기름에 함유된 폴리염화비페닐의 무해화 처리방법 无效
标题翻译：变压器油中PCBS的处理方法
公开(公告)号：KR1020060071566A
公开(公告)日：2006-06-27
申请号：KR1020040110186
申请日：2004-12-22
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： A62D3/00 , A62D3/30 , B01J20/00 , B01D17/02
CPC分类号： A62D3/30 , B01D17/0202 , B01J20/00
摘要： 본 발명은 기름에 함유된 폴리염화비페닐의 무해화 처리방법을 제공하기 위한 것으로, 산화칼슘과 오일을 혼합하여 소수성의 산화칼슘을 제조하는 제 1 단계와; 상기 제 1 단계에서 제조된 소수성의 산화칼슘을 기름 분해제, 이온 교환성 다공체와 함께 변압기 오일에 혼합하여 방치하는 제 2 단계로 이루어진다.
상기의 본 발명에 의한 기름에 함유된 폴리염화비페닐의 무해화 처리방법은 기름이 첨착되고 소수성이 부여된 산화칼슘, 흡착과 이온 교환성이 있는 다공체, 폴리염화비페닐을 함유한 기름 및 상기 산화칼슘에 첨착한 기름을 분해하는 기름분해제를 사용하여 간단하게 저온에서 유분을 분해하여 분말화함과 동시에 이온 교환성에 의한 폴리염화비페닐의 염소를 유리시켜 무해한 염소화합물로 변화시킬수 있는 방법을 제공하여 폴리염화비페닐 함유 기름을 포스겐, 다이옥신 등의 독성이 강한 물질이 발생되는 염려가 없고, 안전하게 무해화 처리할 수 있는 효과가 있다.
폴리염화비페닐, Poly Chlorinated Biphenyls, PCBs, 무해화

54. 发明授权

KR100440465B1 옥타클로로디벤조퓨란의 정량 방법 失效
标题翻译： 옥타클로로디벤조퓨란의정량방법
公开(公告)号：KR100440465B1
公开(公告)日：2004-07-15
申请号：KR1020000049299
申请日：2000-08-24
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼 , 탁진권
IPC分类号： C07D307/91
摘要： PURPOSE: Provided is a method for quantifying octachlorodibenzofuran by non-polar gas chromatography column coated with stationary phase of which the functional group having a high polarity is substituted with alkylsilyl group. CONSTITUTION: Octachlorodibenzofuran is quantified by using non-polar gas chromatography column which is pre-treated by the steps of: inserting a solution of alkylsilyl group dissolved in polar solvent into polar gas chromatography column, in an oven of 220-275 deg.C; then inserting a solution of lower(primary)alcohol dissolved in non-polar solvent. Where, the non-polar solvent is selected from the group consisting of C5-C6 saturated hydrocarbon and the lower(primary)alcohol is selected from the group consisting of C1-C3 primary alcohol.
摘要翻译：目的：提供一种用非极性气相色谱柱定量八氯二苯并呋喃的方法，所述非极性气相色谱柱用固定相涂覆，其中具有高极性的官能团被烷基甲硅烷基取代。构成：使用非极性气相色谱柱对八氯二苯并呋喃进行定量，所述非极性气相色谱柱通过以下步骤进行预处理：将溶解在极性溶剂中的烷基甲硅烷基溶液置于极性气相色谱柱中，在220-275℃的烘箱中; 然后插入溶解在非极性溶剂中的低级（伯）醇的溶液。其中，非极性溶剂选自C5-C6饱和烃，较低（伯）醇选自C1-C3伯醇。

55. 发明授权

KR100435421B1 비산재에 포함된 다이옥신 정량방법 失效
标题翻译：通过电子邮件发送给朋友
公开(公告)号：KR100435421B1
公开(公告)日：2004-06-10
申请号：KR1019990059500
申请日：1999-12-20
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼 , 탁진권
IPC分类号： G01N31/00
摘要： PURPOSE: A quantifying method of dioxin contained in fly ash is provided to obtain a correlation formula between a concentration of Chlorine ions and a concentration of dioxin for simply and reliably obtaining a content of dioxin without carrying out any complicated pre-processing for quantifying dioxin or using any high precision quantifying machines. CONSTITUTION: A quantifying method of dioxin contained in fly ash includes the steps of removing inorganic chlorine ions by cleaning the fly ash, dissolving the cleaned fly ash with acid to dissolve the chlorine ions and quantifying the concentration of the Chlorine ions, and obtaining a whole dioxin concentration by a formula(whole dioxin concentration(ng/g)=2.80x10-2(Chlorine ion concentration in the sample(microgram/g))1.45(R=0.829)) on the basis of the concentration of the Chlorine ions.
摘要翻译：目的：提供一种飞灰中所含二恶英的定量方法，以获得氯离子浓度与二恶英浓度之间的相关公式，以简单且可靠地获得二恶英含量，而无需进行任何复杂的用于定量二恶英的预处理或使用任何高精度量化机器。本发明提供了一种飞灰中二恶英的定量方法，包括通过清除飞灰去除无机氯离子，用酸溶解清洗后的飞灰溶解氯离子并定量氯离子浓度，得到一个完整的基于氯离子的浓度，通过公式（全二氧己二
烯浓度（ng / g）= 2.80×10-2（样品中的氯离子浓度（微克/克））1.45（R = 0.829）

56. 发明公开

KR1020130074843A 황에 대한 내구성이 우수한 메탄 개질용 촉매, 이의 제조방법 및 이를 이용한 메탄개질 방법 有权
标题翻译：甲烷改性催化剂与硫化物组分的增强稳定性，其制备方法和使用催化剂的甲醇改性方法
公开(公告)号：KR1020130074843A
公开(公告)日：2013-07-05
申请号：KR1020110142267
申请日：2011-12-26
申请人： 재단법인 포항산업과학연구원
发明人： 장점석 , 김경태 , 배종욱 , 사영삼 , 고동준 , 백준현 , 김효식 , 이윤조
IPC分类号： B01J23/46 , B01J21/06 , B01J23/10 , C07C9/04
CPC分类号： B01J23/464 , B01J21/066 , B01J23/10 , B01J35/1014 , B01J37/00 , B01J2523/3712 , C01B3/40
摘要： PURPOSE: A catalyst for reforming methane with enhanced stability for sulfur components, a preparing method of the same, and a methane reforming method using the same are provided to show superior catalytic activity and stability in a methane reforming reaction using by-product gas containing sulfur, specifically hydrogen sulfide. CONSTITUTION: A catalyst carries 0.2-5 parts by weight of rhodium based on 100 parts by weight of a CeO2-ZrO2 support. The specific surface area of the catalyst is 20-50 m^2/g. The specific surface area of the CeO2-ZrO2 support is 20-80 m^2/g. The weight ratio of CeO2/ZrO2 is 0.3-4.0. The catalyst is used for a methane reforming reaction using by-product gas containing 3000ppmv or less of H2S. A preparing method of the catalyst includes the steps of: carrying 0.2-5 parts by weight of rhodium in 100 parts by weight of CeO2-ZrO2 support based on the content of metals; and plasticizing at a temperature between 400 and 800°C. [Reference numerals] (AA) CH4 conversion rate (mol%); (BB) Time (h) (time in stream); (CC) Example 1; (DD) Example 3; (EE) Comparative example 7
摘要翻译：目的：提供用于硫组分稳定性提高的甲烷催化剂及其制备方法和使用该催化剂的甲烷重整方法，以显示使用含硫的副产物气体在甲烷重整反应中的优异的催化活性和稳定性，特别是硫化氢。构成：基于100重量份的CeO 2 -ZrO 2载体，催化剂携带0.2-5重量份的铑。催化剂的比表面积为20-50m 2 / g。 CeO 2 -ZrO 2载体的比表面积为20-80m 2 / g。 CeO2 / ZrO2的重量比为0.3-4.0。该催化剂用于使用含有3000ppmv或更少的H 2 S的副产物气体进行甲烷重整反应。该催化剂的制备方法包括以下步骤：基于金属含量，在100重量份的CeO 2 -ZrO 2载体中携带0.2-5重量份的铑; 并在400至800℃的温度下增塑。（AA）CH4转化率（mol％）; （BB）时间（h）（时间流）; （CC）实施例1; （DD）实施例3; （EE）比较例7

57. 发明公开

KR1020080056982A ＰＡＨｓ로 오염된 토양의 정화방법 失效
标题翻译： PAHS污染土壤的脱氧方法
公开(公告)号：KR1020080056982A
公开(公告)日：2008-06-24
申请号：KR1020060130251
申请日：2006-12-19
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09C1/08
CPC分类号： B09C1/08 , A62D3/38
摘要： A remediating method of soils contaminated with PAHs(Poly Aromatic Hydrocarbons) is provided to remediate the contaminated soils or sediments within a short time while less affecting the environment by adding an oxidizer to contaminated soils or sediments containing the PAHs and projecting ultrasonic waves onto the contaminated soils or sediments. A remediating method of soils contaminated with poly aromatic hydrocarbons comprises: a first step of adding 100 mM to 1 M of an oxidizer to 50 to 500 g of soils contaminated with poly aromatic hydrocarbons; a second step of adding 150 mg to 1 g of a metal oxide as a catalyst to the oxidizer added contaminated soils; a third step of agitating the oxidizer and the metal oxide added contaminated soils; and a fourth step of irradiating ultrasonic waves onto the agitation-completed soils for at least one hour. The oxidizer is hydrogen peroxide. The metal oxide includes CuO, Al2O3, and ZnO. The contaminated soils are particularly marine sediments.
摘要翻译：提供了多环芳烃污染土壤的补救方法（聚芳香烃），可在短时间内对污染土壤或沉积物进行修复，同时对受污染的土壤或含有PAHs的沉积物添加氧化剂，并将超声波投射到污染物土壤或沉积物。用聚芳烃污染的土壤的补救方法包括：向50-500克被多芳香烃污染的土壤中加入100mM至1M的氧化剂的第一步骤; 向作为催化剂的1g金属氧化物中加入150mg添加污染土壤的第二步骤; 搅拌氧化剂和添加污染土壤的金属氧化物的第三步骤; 以及将超声波照射到搅拌完成的土壤上至少1小时的第四步骤。氧化剂是过氧化氢。金属氧化物包括CuO，Al 2 O 3和ZnO。受污染的土壤特别是海洋沉积物。

58. 发明授权

KR100402031B1 염소화반응을 이용한 다이옥신의 신속한 검출방법 失效
标题翻译：用于解决问题的方法
公开(公告)号：KR100402031B1
公开(公告)日：2003-10-17
申请号：KR1019990058353
申请日：1999-12-16
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼 , 탁진권
IPC分类号： G01N30/02
摘要： PURPOSE: A method for promptly detecting dioxin is provided for accomplishing higher detection limit and correct quantification of dioxin with inexpensive gas chromatography/electron detection device by using antimony chloride to chlorinate dioxin isomers into dioxin octa-chloride. CONSTITUTION: The detection method comprises adding antimony chloride to an extract containing dioxin and heating it to 236-288 deg.C. to produce dioxin octa-chloride; adding HCl to the obtained dioxin octa-chloride to extract hexane material; removing high polar interference material; and detecting dioxin from the extract by means of gas chromatography/electron capturing detector. The method is useful for detecting the dioxin without alternately separating isomers because of the chlorination process and with no requiring commercial pre-treatment step separating isomers.
摘要翻译：目的：通过使用氯化锑将二恶英异构体氯化成二恶英八氯化物，用便宜的气相色谱/电子检测装置实现了二恶英的快速检测方法以实现更高的检测限和正确定量二恶英。组成：检测方法包括将氯化锑加入到含有二恶英的提取物中并将其加热至236-288℃。生产二氯辛烷氯化物; 向获得的二辛氧基氯化锡中加入HCl以提取己烷物质; 去除高极性干扰物质; 并通过气相色谱/电子捕获检测器从提取物中检测二恶英。该方法可用于检测二恶英，而不用交替分离异构体，因为氯化过程和不需要商业预处理步骤分离异构体。

59. 发明公开

KR1020030053233A 소각로 배출가스의 다이옥신 저감방법 失效
标题翻译：焚烧炉排气的二氧化碳还原方法
公开(公告)号：KR1020030053233A
公开(公告)日：2003-06-28
申请号：KR1020010083391
申请日：2001-12-22
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： F23G7/00
摘要： PURPOSE: A method for reducing dioxin of incinerator exhaust gas is provided to reduce dioxin of incinerator exhaust gas by using low-priced slag generated from an iron mill and effectively reduce dioxin of incinerator exhaust gas. CONSTITUTION: In a method for reducing dioxin of incinerator exhaust gas, chlorophenol, precursor metabolite of dioxin is adhered by bring blast furnace slag of an iron mill contact with the chlorophenol. The slag is dried at 180¯220 degrees centigrade and then is activated in an electric muffle furnace at 550¯650 degrees centigrade. Dioxin is efficiently reduced, using the cheap slag of the iron mill instead of an expensive adsorbent.
摘要翻译：目的：提供一种减少焚烧废气二恶英的方法，通过使用铁厂生产的低价炉渣，有效减少焚烧炉废气二恶英，减少焚烧炉废气二恶英。构成：在减少焚烧炉排气二恶英的方法中，通过使铁厂的高炉渣与氯酚接触，氯酚，二恶英的前体代谢物被粘附。炉渣在180-220摄氏度下干燥，然后在550-650摄氏度的电动马弗炉中活化。使用铁粉的廉价矿渣代替昂贵的吸附剂，有效地减少二恶英。

60. 发明授权

KR101520729B1 일산화탄소 흡수액의 제조방법 및 상기 흡수액을 이용하여 전로가스로부터 일산화탄소를 분리 및 회수하는 방법 有权
标题翻译：用于制备一氧化碳吸收剂的方法以及使用其从LDG气体中分离和回收一氧化碳的方法
公开(公告)号：KR101520729B1
公开(公告)日：2015-05-20
申请号：KR1020130128569
申请日：2013-10-28
申请人： 재단법인 포항산업과학연구원
发明人： 이시훈 , 최진순 , 김국희 , 임동하 , 김경태 , 사영삼 , 김태훈
IPC分类号： B01D53/14 , B01D53/62 , B01D53/96 , B01D53/74
CPC分类号： Y02A50/2341
摘要： 본발명은톨루엔의용매에염화구리(Ⅰ) 및염화알루미늄을특정무게비로혼합하여일산화탄소흡수액을제조하는방법을제공하고, 상기흡수액을이용하여전로가스로부터일산화탄소를흡수하고, 흡수된일산화탄소는가열에의해분리및 회수하는방법을제공함으로써, 일산화탄소가다량으로포함된전로가스로부터일산화탄소만을고순도로회수할수 있도록한다.

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