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41. 发明授权

US08574520B2 Metal oxide support material containing nanoscaled iron platinum group metal 失效
标题翻译：金属氧化物载体材料含有纳米级铁铂族金属
公开(公告)号：US08574520B2
公开(公告)日：2013-11-05
申请号：US13516291
申请日：2010-12-13
申请人： Tobias Joachim Koplin , Imme Domke , Christopher R. Castellano , Gerald Stephen Koermer , Wolfgang Schrof , Robert Feuerhake , Gunnar Schornick , Anna Cristadoro , Daniel Schönfelder , Hartmut Hibst , Mattijs Gregor Jurriaan Ten Cate
发明人： Tobias Joachim Koplin , Imme Domke , Christopher R. Castellano , Gerald Stephen Koermer , Wolfgang Schrof , Robert Feuerhake , Gunnar Schornick , Anna Cristadoro , Daniel Schönfelder , Hartmut Hibst , Mattijs Gregor Jurriaan Ten Cate
IPC分类号： B01D53/94 , B01J23/40 , B01J23/42 , B01J35/00 , B01J37/00
CPC分类号： B01J35/008 , B01D53/94 , B01D53/945 , B01D2255/1021 , B01D2255/1023 , B01D2255/1025 , B01D2255/9202 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/464 , B01J23/74 , B01J35/0006 , B01J35/006 , B01J37/0203 , B01J37/0219 , B01J37/16 , C07C5/00 , C07C5/02 , C07C5/32 , C10G45/00 , C10G45/52 , C10G2300/405 , Y02T10/22
摘要： Described is a metal oxide support material containing nanoscaled iron-platinum group metal particles having a particle size in the range of 0.5 to 10 nm. At least 70% of the nanoscaled iron-platinum group metal particles are located on an outside surface layer of the metal oxide support material. The outside surface layer has an average volume of less than 50% based on the total volume of the metal oxide support material. Additionally, described is a process for preparation of metal oxide support materials containing nanoscaled iron-platinum group metal particles. Furthermore, described is the use of metal oxides containing nanoscaled iron-platinum group metal particles as catalysts, for example as a diesel oxidation catalyst for the treatment of exhaust gas emissions from a diesel engine.
摘要翻译：描述了含有粒度在0.5至10nm范围内的纳米级铁 - 铂族金属颗粒的金属氧化物载体材料。至少70％的纳米级铁 - 铂族金属颗粒位于金属氧化物载体材料的外表面层上。基于金属氧化物载体材料的总体积，外表面层的平均体积小于50％。此外，描述了一种制备含有纳米级铁 - 铂族金属颗粒的金属氧化物载体材料的方法。此外，描述了使用含有纳米级铁 - 铂族金属颗粒的金属氧化物作为催化剂，例如作为用于处理来自柴油发动机的废气排放的柴油氧化催化剂。

42. 发明申请

US20120043537A1 PROCESS FOR PRODUCING SEMICONDUCTIVE LAYERS 有权
标题翻译：生产半导体层的工艺
公开(公告)号：US20120043537A1
公开(公告)日：2012-02-23
申请号：US13266935
申请日：2010-04-26
申请人： Andrey Karpov , Friederike Fleischhaker , Imme Domke , Marcel Kastler , Veronika Wloka , Lothar Weber
发明人： Andrey Karpov , Friederike Fleischhaker , Imme Domke , Marcel Kastler , Veronika Wloka , Lothar Weber
IPC分类号： H01L29/22 , H01L21/16 , C01B21/00
CPC分类号： C23C18/1216 , C23C18/1245 , H01L21/02381 , H01L21/02488 , H01L21/02554 , H01L21/02565 , H01L21/02628 , H01L27/1292 , H01L29/66742 , H01L29/66969 , H01L29/7869
摘要： The present invention relates to a process for producing a layer comprising at least one semiconductive metal oxide on a substrate, comprising at least the steps of: (A) preparing a solution comprising at least one precursor compound of the at least one metal oxide selected from the group consisting of carboxylates of mono-, di- or polycarboxylic acids having at least three carbon atoms, or derivatives of mono-, di- or polycarboxylic acids, alkoxides, hydroxides, semicarbazides, carbamates, hydroxamates, isocyanates, amidines, amidrazones, urea derivatives, hydroxylamines, oximes, urethanes, ammonia, amines, phosphines, ammonium compounds, azides of the corresponding metal and mixtures thereof, in at least one solvent, (B) applying the solution from step (A) to the substrate and (C) thermally treating the substrate from step (B) at a temperature of 20 to 200° C., in order to convert the at least one precursor compound to at least one semiconductive metal oxide, where, if electrically neutral [(OH)x(NH3)yZn]z where x, y and z are each independently 0.01 to 10 is used as the precursor compound in step (A), it is obtained by reacting zinc oxide or zinc hydroxide with ammonia, to a substrate which has been coated with at least one semiconductive metal oxide and is obtainable by this process, to the use of this substrate in electronic components, and to a process for preparing electrically neutral [(OH)x(NH3)yZn]z where x, y and z are each independently 0.01 to 10, by reacting zinc oxide and/or zinc hydroxide with ammonia.
摘要翻译：本发明涉及一种在基材上制备包含至少一种半导体金属氧化物的层的方法，至少包括以下步骤：（A）制备包含至少一种选自以下的金属氧化物的至少一种前体化合物的溶液：由具有至少三个碳原子的单羧酸，二羧酸或多羧酸的羧酸盐组成的组，或单羧酸，二羧酸或多元羧酸，醇盐，氢氧化物，氨基脲，氨基甲酸酯，异羟肟酸酯，异氰酸酯，脒，氨基腙，脲衍生物，羟胺，肟，氨基甲酸酯，氨，胺，膦，铵化合物，相应金属的叠氮化物及其混合物，在至少一种溶剂中，（B）将来自步骤（A）的溶液施加到基材上，（C）在20至200℃的温度下对来自步骤（B）的基底进行热处理，以将至少一种前体化合物转化为至少一种半导体金属氧化物，其中如果电中性[（OH）x（NH3）yZn] z其中x，y和z各自独立地为0.01〜10作为步骤（A）中的前体化合物，通过使氧化锌或氢氧化锌与氨反应得到已经涂覆有至少一种半导体金属氧化物并且可以通过该方法获得的衬底，用于电子部件中的该衬底以及制备电中性[（OH）x（NH 3）y Zn] z的方法，其中 x，y和z各自独立地为0.01〜10，通过使氧化锌和/或氢氧化锌与氨反应。

43. 发明申请

US20110163278A1 MODIFIED PARTICLES AND DISPERSIONS COMPRISING THESE 有权
标题翻译：改性颗粒和包含这些颗粒的分散体
公开(公告)号：US20110163278A1
公开(公告)日：2011-07-07
申请号：US13062229
申请日：2009-08-28
申请人： Imme Domke , Andrey Karpov , Hartmut Hibst , Radoslav Rarashkov , Ingolf Hennig , Marcel Kastler , Friederike Fleischhaker , Lothar Weber , Peter Eckerle
发明人： Imme Domke , Andrey Karpov , Hartmut Hibst , Radoslav Rarashkov , Ingolf Hennig , Marcel Kastler , Friederike Fleischhaker , Lothar Weber , Peter Eckerle
IPC分类号： H01B1/12 , B05D3/02 , B05D3/06
CPC分类号： B82Y30/00 , C01P2004/62 , C01P2004/64 , C09C1/043 , H01L21/02554 , H01L21/02565 , H01L21/02601 , H01L21/02628 , H01L29/7869 , Y10T428/29 , Y10T428/2995
摘要： The present invention relates to particles which have been modified by a modifier and a dispersion medium comprising the modified particles.The surface-modified metal, metal halide, metal chalcogenide, metal nitride, metal phosphide, metal boride or metal phosphate particles or mixtures thereof have an average particle diameter of from 1 to 500 nm and their surface has been modified by one or more modifiers of the formula (I) (II) and (III)
摘要翻译：本发明涉及通过改性剂改性的颗粒和包含改性颗粒的分散介质。表面改性的金属，金属卤化物，金属硫族化物，金属氮化物，金属磷化物，金属硼化物或金属磷酸盐颗粒或其混合物的平均粒径为1至500nm，并且其表面已经被一种或多种改性剂式（I）（II）和（III）

44. 发明申请

US20110020170A1 METAL NANOPARTICLES STABILIZED WITH DERIVATIZED POLYETHYLENEIMINES OR POLYVINYLAMINES 审中-公开
标题翻译：用衍生的聚乙烯或聚乙烯亚胺稳定的金属纳米颗粒
公开(公告)号：US20110020170A1
公开(公告)日：2011-01-27
申请号：US12933397
申请日：2009-03-17
申请人： Gerrit Luinstra , Wolfgang Schrof , Udo Gödert , Robert Feuerhake , Tobias Joachim Koplin , Imme Domke
发明人： Gerrit Luinstra , Wolfgang Schrof , Udo Gödert , Robert Feuerhake , Tobias Joachim Koplin , Imme Domke
IPC分类号： C22B11/00 , C22C5/04 , C22C5/06
CPC分类号： C09C1/62 , B22F1/0018 , B22F1/0059 , B22F9/24 , B82Y30/00 , C01G3/00 , C01G5/00 , C01G7/00 , C01G9/00 , C01G29/00 , C01G55/00 , C01P2002/01 , C01P2002/84 , C01P2004/04 , C01P2004/64 , C01P2006/40
摘要： The invention relates to metal nanoparticles and a process for the preparation thereof, in which a metal salt solution is reduced with a reducing agent in the presence of the derivatized polyethyleneimines or polyvinylamines. Metal salt solutions of two or more different metals can be reduced simultaneously or in succession, metal nanoparticles comprising two or more different metals being obtained. Preferred metals are silver, palladium, and platinum. Suitable reducing agents are, for example, formic acid, formaldehyde, diethanolamine, 5-pentenoic acid and sodium borohydride. Silver can be used in the form of silver oxide and/or silver nitrate, palladium in the form of alkali metal tetrachloropalladate or palladium(II) nitrate and platinum in the form of alkali metal tetrachloroplatinate or tetraamineplatinum(II) nitrate.
摘要翻译：本发明涉及金属纳米粒子及其制备方法，其中在衍生的聚乙烯亚胺或聚乙烯胺的存在下金属盐溶液用还原剂还原。可以同时或连续地还原两种或更多种不同金属的金属盐溶液，获得包含两种或更多种不同金属的金属纳米颗粒。优选的金属是银，钯和铂。合适的还原剂是例如甲酸，甲醛，二乙醇胺，5-戊烯酸和硼氢化钠。银可以以氧化银和/或硝酸银的形式使用，钯金属为四氯钯酸金属盐或硝酸钯（II），硝酸铂金属或四氨基铂（II）形式的铂。

45. 发明授权

US09129801B2 Thermally labile precursor compounds for improving the interparticulate contact sites and for filling the interstices in semiconductive metal oxide particle layers 有权
标题翻译：用于改善晶间接触部位并填充半导体金属氧化物颗粒层间隙的热不稳定前体化合物
公开(公告)号：US09129801B2
公开(公告)日：2015-09-08
申请号：US13378765
申请日：2010-06-15
申请人： Friederike Fleischhaker , Imme Domke , Andrey Karpov , Marcel Kastler , Veronika Wloka , Lothar Weber
发明人： Friederike Fleischhaker , Imme Domke , Andrey Karpov , Marcel Kastler , Veronika Wloka , Lothar Weber
IPC分类号： H01L21/00 , H01L21/16 , H01L21/02 , H01L29/10 , H01L29/12
CPC分类号： H01L21/02422 , H01L21/02554 , H01L21/02565 , H01L21/02573 , H01L21/02601 , H01L21/02628
摘要： The present invention relates to a process for producing a layer comprising at least one semiconductive metal oxide on a substrate, comprising at least the steps of: (A) applying a porous layer of at least one semiconductive metal oxide to a substrate, (B) treating the porous layer from step (A) with a solution comprising at least one precursor compound of the semiconductive metal oxide, such that the pores of the porous layer are at least partly filled with this solution and (C) thermally treating the layer obtained in step (B) in order to convert the at least one precursor compound of the semiconductive metal oxide to the semiconductive metal oxide, wherein the at least one precursor compound of the at least one semiconductive metal oxide in step (B) is selected from the group consisting of carboxylates of mono-, di- or polycarboxylic acids having at least three carbon atoms or derivatives of mono-, di- or polycarboxylic acids, alkoxides, hydroxides, semicarbazides, carbamates, hydroxamates, isocyanates, amidines, amidrazones, urea derivatives, hydroxylamines, oximes, oximates, urethanes, ammonia, amines, phosphines, ammonium compounds, nitrates, nitrites or azides of the corresponding metal, and mixtures thereof.
摘要翻译：本发明涉及一种在基材上制备包含至少一种半导体金属氧化物的层的方法，至少包括以下步骤：（A）将至少一种半导体金属氧化物的多孔层施加到基材上，（B）用包含半导体金属氧化物的至少一种前体化合物的溶液处理来自步骤（A）的多孔层，使得多孔层的孔至少部分地被该溶液填充，和（C）热处理步骤（B），以将半导体金属氧化物的至少一种前体化合物转化为半导体金属氧化物，其中步骤（B）中的至少一种半导体金属氧化物的至少一种前体化合物选自由具有至少三个碳原子的单，二或多元羧酸的羧酸盐或单羧酸，二羧酸或多元羧酸，醇盐，氢氧化物，氨基脲，氨基甲酸盐，水合物氨基甲酸酯，异氰酸酯，脒，氨基腙，脲衍生物，羟胺，肟，肟酸酯，氨基甲酸酯，氨，胺，膦，铵化合物，硝酸酯，亚硝酸酯或相应金属的叠氮化物及其混合物。

46. 发明申请

US20120263633A1 Metal Oxide Support Material Containing Nanoscaled Iron-Platinum Group Metal Particles 失效
标题翻译：含有纳米铁 - 铂族金属颗粒的金属氧化物载体材料
公开(公告)号：US20120263633A1
公开(公告)日：2012-10-18
申请号：US13516291
申请日：2010-12-13
申请人： Tobias Joachim Koplin , Imme Domke , Christopher R. Castellano , Gerald Stephen Koermer , Wolfgang Schrof , Robert Feuerhake , Gunnar Schornick , Anna Cristadoro , Daniel Schönfelder , Hartmut Hibst , Mattijs Gregor Jurriaan Ten Cate
发明人： Tobias Joachim Koplin , Imme Domke , Christopher R. Castellano , Gerald Stephen Koermer , Wolfgang Schrof , Robert Feuerhake , Gunnar Schornick , Anna Cristadoro , Daniel Schönfelder , Hartmut Hibst , Mattijs Gregor Jurriaan Ten Cate
IPC分类号： B01J23/40 , B01J23/44 , B01J31/06 , B01D53/94 , B01J21/04 , B01J23/46 , B82Y40/00 , B82Y30/00
CPC分类号： B01J35/008 , B01D53/94 , B01D53/945 , B01D2255/1021 , B01D2255/1023 , B01D2255/1025 , B01D2255/9202 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/464 , B01J23/74 , B01J35/0006 , B01J35/006 , B01J37/0203 , B01J37/0219 , B01J37/16 , C07C5/00 , C07C5/02 , C07C5/32 , C10G45/00 , C10G45/52 , C10G2300/405 , Y02T10/22
摘要： Described is a metal oxide support material nanoscaled iron-platinum group metal particles having a particle size in the range of 0.5 to 10 nm, wherein at least 70% of all nanoscaled iron-platinum group metal particles are located on an outside surface layer of the metal oxide support material, and wherein the outside surface layer has an average volume of less than 50% based on the total volume of the metal oxide support material.Additionally, described is a process for the preparation of such metal oxide support material comprising nanoscaled iron-platinum group metal particles. Furthermore, described is the use of metal oxides containing nanoscaled iron-platinum group metal particles as catalysts, for example as a diesel oxidation catalyst for the treatment of exhaust gas emissions from a diesel engine.
摘要翻译：描述了一种金属氧化物载体材料纳米级铁 - 铂族金属颗粒，其粒径在0.5至10nm的范围内，其中至少70％的所有纳米级铁 - 铂族金属颗粒位于金属氧化物载体材料，并且其中所述外表面层的平均体积基于所述金属氧化物载体材料的总体积小于50％。此外，描述了制备包含纳米级铁 - 铂族金属颗粒的这种金属氧化物载体材料的方法。此外，描述了使用含有纳米级铁 - 铂族金属颗粒的金属氧化物作为催化剂，例如作为用于处理来自柴油发动机的废气排放的柴油氧化催化剂。

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