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41. 发明专利

JPH10182598A PRODUCTION OF FLUORINE-CONTAINING PROSTAGLANDIN DERIVATIVE 失效
公开(公告)号：JPH10182598A
公开(公告)日：1998-07-07
申请号：JP34628696
申请日：1996-12-25
申请人： ASAHI GLASS CO LTD
发明人： NAKANO TAKASHI , MORI NOBUAKI , SAKATA KAZUHISA , MATSUMURA YASUSHI , MORISAWA YOSHITOMI
IPC分类号： C07D307/93 , C07C405/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorine-containing prostaglandin derivative having high activities as a medicine and further having fluorine atom at 15-position having no side effect by allowing specific phosphoranes to act on a specified fluorine-containing lactols. SOLUTION: Alcohols of formula I (A is ethylene, etc.; R is a 3-8C alkyl, etc.; R is H or a protecting group of OH) is fluorinated by a trifluorinated dialkylaminosulfur derivative, which is a nucleophilic fluorinating agent, etc., e.g. morpholinosulfur trifluoride to provide fluorine-containing lactones of formula II, and the lactones is reduced by diisobutylaluminum hydride, etc., to provide a fluorine-containing lactones of formula III. The objective compound having a structure of formula V is obtained by reacting 1 equivalent compound of formula III with 0.1-20 equivalents phosphoranes of formula IV [R is a protecting group of H or OH; X is CH2 , O or S; Z is OR , etc., (R is H, an alkyl, etc.); R is an aryl, an alkyl, etc.] by a so-called Wittig-type reaction to provide the objective compound of formula V.

42. 发明专利

JPH08143560A PRODUCTION OF DIFLUOROLACTONES 失效
公开(公告)号：JPH08143560A
公开(公告)日：1996-06-04
申请号：JP28385794
申请日：1994-11-17
申请人： ASAHI GLASS CO LTD
发明人： MATSUMURA YASUSHI , NAKANO TAKASHI , MORISAWA YOSHITOMI
IPC分类号： C07D307/32 , C07B39/00 , C07D305/12 , C07D307/33 , C07D307/935 , C07D309/30 , C07D311/20 , C07D311/94 , C07D313/00 , C07D407/12 , C07F7/18
摘要： PURPOSE: To efficiently and readily obtain a difluorolactone containing two fluorine atoms at the 7-position useful as an intermediate for synthesizing medicines, agrochemicals or difluoroprostaglandins. CONSTITUTION: This compound of formula I (R , R , R and R are each independently H, a halogen, protected OH, NH2 or CO2 H or nR , nR or any two selected from R and R are mutually bonded to form a to R are independently H, a halogen, etc.; (n) is an integer of 0-10) is obtained by fluorinating a lactone of formula II with an electrophilic fluorinating agent such as N-fluorosulfonimide under basic conditions of Li in the presence of a metal compound reaction agent such as B or Mg. In the reaction, 1 pt.wt. of the lactone is reacted with 2-10 pts.wt. of the electrophilic fluorinating agent in the presence of 2-10 pts.wt. of the base and 0.1-10 pts.wt. of the metal compound reaction agent in 10-100 pts.wt. of an inert solvent such as diethyl ether at -8 deg.C to +40 deg.C.

43. 发明专利

JP2013234209A Method for producing fluororesin organosol, fluororesin organosol, and coating composition 审中-公开
标题翻译：生产氟菊酯有机物，氟菊酯有机物和涂料组合物的方法
公开(公告)号：JP2013234209A
公开(公告)日：2013-11-21
申请号：JP2010198288
申请日：2010-09-03
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： NAKANO TAKASHI , SHIROTA NAOKO
IPC分类号： C08J3/09 , C08L27/18 , C09D127/18
CPC分类号： C08J3/09 , C08J2323/08 , C08J2327/18 , C09D127/18
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluororesin organosol, which produces, at a relatively low temperature, the fluororesin organosol in which a fluorine-containing copolymer (ETFE) containing a repeating unit based on ethylene and a repeating unit based on tetrafluoroethylene is dispersed in a high concentration and homogeneously in an organic medium; a fluororesin organosol produced by the method; and a coating composition containing the fluororesin organosol as a main component.SOLUTION: A method for producing a fluororesin organosol uses ETFE as a dispersoid and a solvent capable of dissolving the ETFE at a temperature equal to or lower than the melting point of the ETFE as a disperse medium, and includes: a dissolution step of dissolving ETFE in the solvent to make a solution; a deposition step of depositing the ETFE in the solution in the solvent as microparticles; and a crushing and dispersing step of applying a high shear force to a mixture of the solvent containing ETFE as microparticles and ETFE, to homogeneously disperse the ETFE microparticles in the solvent.
摘要翻译：要解决的问题：提供一种氟树脂有机溶胶的制造方法，该氟树脂有机溶胶在相对较低的温度下生成含有基于乙烯的重复单元的含氟共聚物（ETFE）和基于乙烯的重复单元的含氟共聚物（ETFE）四氟乙烯以高浓度分散并均匀地存在于有机介质中; 通过该方法制备的氟树脂有机溶胶; 以及含有氟树脂有机溶胶作为主要成分的涂料组合物。本发明的氟树脂有机溶胶的制造方法使用作为分散质的ETFE和能够在ETFE的熔点以下的温度下溶解ETFE的溶剂，分散介质，并且包括：将ETFE溶解在溶剂中以形成溶液的溶解步骤; 沉积步骤，将ETFE沉积在溶剂中的溶液中作为微粒; 以及对含有ETFE的溶剂作为微粒和ETFE的混合物施加高剪切力的粉碎分散工序，使ETFE微粒均匀分散于溶剂中。

44. 发明专利

JP2012052107A Vinyl ether compound, copolymer and optical element 审中-公开
标题翻译：乙烯基化合物，共聚物和光学元素
公开(公告)号：JP2012052107A
公开(公告)日：2012-03-15
申请号：JP2011170384
申请日：2011-08-03
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： KAIDA YURIKO , YAMAMOTO YUJI , OGUCHI RYOHEI , NAKANO TAKASHI , FUKUDA MIYAKO , FUJITA SATOYUKI , MORISAWA YOSHITOMI , TAWARA SHINYA , KONISHI TEPPEI , OKADA SATOSHI
IPC分类号： C08F16/26 , C07C69/753 , C08F214/18 , C09K19/38 , G02F1/13363
摘要： PROBLEM TO BE SOLVED: To provide a copolymer and an optical element having high refractive index anisotropy and excellent blue laser light resistance, capable of suppressing film thickness irregularity and orientation disturbance, and to provide a new compound for acquiring them.SOLUTION: A new vinyl ether compound is represented by formula (1): CH=CH-O-(CH)-R-(CH)-O-w-(E)-w-(E)-(E)-E-R(in the formula, R is an alkylene group, a polyfluoroalkylene group or the like, Ris an alkyl group, a cyano group or the like, Eis a 1,4 phenylene group, E, E, Eare each 1,4 phenylene group, a trans-1,4-cyclohexylene group, or a trans-2,6-decahydronaphthalenyl group, and w1, w2 are each a carbonyl group or a single bond).
摘要翻译：解决的问题：提供能够抑制膜厚不均匀性和取向紊乱的共聚物和具有高折射率各向异性和优异的蓝色激光耐光性的光学元件，并提供用于获得它们的新化合物。解决方案：新的乙烯基醚化合物由式（1）表示：CH 2 = CH-O-（CH 2 < SB>） m -R-（CH 2 ） n -Ow 1 - （E 1 ） h -w 2 - （E 2 ） j - （E 3 ） k -E 4 -R 1 式中，R为亚烷基，多氟亚烷基等，作为烷基，氰基等，E 1 是1,4-亚苯基，E 2 ，E 3 ，E 4 分别为1,4-亚苯基，反式-1,4-亚环己基或反式-2,6-癸氢合萘基，w1，w2分别为羰基或单键）。版权所有（C）2012，JPO＆INPIT

45. 发明专利

JP2007022953A MANUFACTURING METHOD OF α-FLUOROCYCLIC SULFONES 审中-公开
标题翻译： α-氟代硫化物的制备方法
公开(公告)号：JP2007022953A
公开(公告)日：2007-02-01
申请号：JP2005206008
申请日：2005-07-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： NAKANO TAKASHI , SAWAGUCHI MASANORI , MORISAWA YOSHITOMI
IPC分类号： C07D333/48
摘要： PROBLEM TO BE SOLVED: To provide a practical method for selectively manufacturing α-fluorocyclic sulfones exhibiting excellent stability. SOLUTION: The cyclic sulfones having a fluorine atom selectively introduced into its α-position is manufactured by causing cyclic sulfoxides or cyclic sulfides having at least one hydrogen atom in the α-position to react with fluorine and water in a liquid phase. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供选择性制备显示出优异稳定性的α-氟代环砜的实用方法。解决方案：通过使在α-位上具有至少一个氢原子的环状亚砜或环状硫化物与液相中的氟和水反应来制备具有选择性地引入其α-位的氟原子的环状砜。版权所有（C）2007，JPO＆INPIT

46. 发明专利

JP2006237572A Liquid immersion-type exposure method and medium for liquid immersion-type exposure 审中-公开
标题翻译：液体渗透式暴露方法和液体浸渍型曝光介质
公开(公告)号：JP2006237572A
公开(公告)日：2006-09-07
申请号：JP2005377709
申请日：2005-12-28
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： IRISAWA JUN , NAKANO TAKASHI , YOKOKOJI OSAMU , SASAKI TAKASHI
IPC分类号： H01L21/027 , G03F7/20
摘要： PROBLEM TO BE SOLVED: To provide a medium for a liquid immersion-type exposure and a method thereof capable of realizing a higher pattern resolution since a specific organic sulfur compound with a small extinction coefficient to a light of a projection optical system and with a higher refractive index than a conventional compound is used as a liquid medium, wherein an interaction of the liquid medium to an organic resist material is small and a dissolution and a swelling of the organic resist material can be controlled. SOLUTION: This invention relates to a liquid immersion-type exposure method of the liquid medium in which an organic compound having a sulfur atom of 6 valences is indispensable, and the medium for the liquid immersion-type exposure consisting of the liquid medium used for a liquid immersion-type exposure method, in a method of filling the liquid medium permeating through a wavelength light of less than 220 nm between a projection optical system projecting the wavelength light to a substrate and the substrate and of projecting the wavelength light from the projection optical system to the substrate. For example, a compound expressed by a formula R 1 -Y-SO 2 -Z-R 2 where R 1 and R 2 are an alkyl group which may independently have fluorine atoms of carbon numbers 1 to 12, respectively or form an alkylene group which may have fluorine atoms of carbon numbers 2 to 16 together. Y and Z are independently an organic compound which is single bond or oxygen atom, respectively. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种液浸式曝光介质及其能够实现更高图案分辨率的方法，因为具有对投影光学系统的光的消光系数小的特定有机硫化合物和使用比常规化合物更高的折射率作为液体介质，其中液体介质与有机抗蚀剂材料的相互作用小，并且可以控制有机抗蚀剂材料的溶解和溶胀。本发明涉及其中硫原子为6价有机化合物是必不可少的液体介质的浸液式曝光方法，以及由液体介质组成的液浸型曝光介质用于浸液式曝光方法，在将波长范围内的投影光学系统与基板和基板之间填充透过小于220nm的波长光的液体介质的方法中，并且将波长的光从投影光学系统到基板。例如，由式R 1表示的化合物，其中R 1 -Y-SO 2 R 2是分别独立地具有碳原子数为1〜12的氟原子的烷基，或者可以一起形成碳原子数为2〜16的氟原子的亚烷基。 Y和Z分别是单键或氧原子的有机化合物。版权所有（C）2006，JPO＆NCIPI

47. 发明专利

JPH1017561A ALLYLALCOHOL COMPOUNDS AND THEIR PRODUCTION 失效
公开(公告)号：JPH1017561A
公开(公告)日：1998-01-20
申请号：JP16485196
申请日：1996-06-25
申请人： ASAHI GLASS CO LTD
发明人： MATSUMURA YASUSHI , NAKANO TAKASHI
IPC分类号： C07D307/935 , B01J31/14 , C07B53/00 , C07B61/00 , C07C405/00
摘要： PROBLEM TO BE SOLVED: To industrially advantageously obtain the subject new alcohol compound important as an intermediate for prostaglandins from easily available raw materials in advantageous productivity by stereospecifically reducing an α,β-unsaturated ketone. SOLUTION: The alcohol compound of formula I [R is methyl, ethyl, trifluoromethyl; R is methyl, ethyl, n-propyl; R is H, an OH-protecting group; (n) is 0, 1, 2]. The alcohol compound is preferably obtained by stereospecifically reducing (A) an α-unsaturated ketone of formula II with (B) a selective reducing agent, especially a reagent of formula III [R is a (substituted) 6-20C aryl; R is a (substituted) 2-6C alkyl]. The component A is preferably obtained by reacting (i) an aldehyde of formula IV with a phosphonate of formula V (R is a lower alkyl).

48. 发明专利

JP2013103172A Coating method of metal plate and coated metal plate 审中-公开
标题翻译：金属板和涂层金属板的涂层方法
公开(公告)号：JP2013103172A
公开(公告)日：2013-05-30
申请号：JP2011248784
申请日：2011-11-14
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： NAKANO TAKASHI , SHIROTA NAOKO
IPC分类号： B05D7/24 , B05D7/14 , C09D5/08 , C09D123/08 , C09D127/18 , C09D157/00
摘要： PROBLEM TO BE SOLVED: To provide a method of coating a metal plate to obtain a coated metal plate excellent in weather resistance, chemical resistance and rust-proof properties and a coated metal plate excellent in weather resistance, chemical resistance and rust-proof properties obtained by using the method.SOLUTION: The coating method of the metal plate includes processes of: preparing a coating composition which contains a fluorine-containing copolymer containing a repeating unit based on ethylene and a repeating unit based on tetrafluoroethylene and a solvent capable of dissolving the fluorine-containing copolymer at a temperature equal to or lower than a melting point of the fluorine-containing copolymer in a method including dissolving treatment of dissolving the fluorine-containing copolymer in the solvent at the temperature equal to or lower than the melting point of the fluorine-containing copolymer; and applying the coating composition to the surface of the metal plate. The metal plate coated with a resin layer including the fluorine-containing copolymer is obtained by using the coating method.
摘要翻译：要解决的问题：提供一种涂覆金属板以获得耐候性，耐化学性和防锈性优异的涂覆金属板和耐候性，耐化学性和防锈性优异的涂覆金属板的方法，通过使用该方法获得的证明性能。解决方案：金属板的涂布方法包括以下工艺：制备包含含有基于乙烯的重复单元的含氟共聚物和基于四氟乙烯的重复单元的涂料组合物和能够溶解氟 - 含氟共聚物在含氟共聚物的熔点以下的温度下，在含氟共聚物的熔点以下的温度下，将含氟共聚物溶解在溶剂中进行溶解处理的方法，含有共聚物; 以及将所述涂料组合物施加到所述金属板的表面。通过使用涂布法得到涂布有含氟共聚物的树脂层的金属板。版权所有（C）2013，JPO＆INPIT

49. 发明专利

JP2012031167A Diene compound-containing fluorine, polymerizable liquid crystal composition, optically anisotropic material, and optical element 审中-公开
标题翻译：二烯化合物氟化物，可聚合液晶组合物，光学非均质材料和光学元件
公开(公告)号：JP2012031167A
公开(公告)日：2012-02-16
申请号：JP2011151668
申请日：2011-07-08
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： KAIDA YURIKO , YAMAMOTO YUJI , OGUCHI RYOHEI , MORISAWA YOSHITOMI , NAKANO TAKASHI , FUKUDA MIYAKO , TAWARA SHINYA , KONISHI TEPPEI , OKADA SATOSHI
IPC分类号： C07C69/753 , C08F36/20 , C09K19/38 , C09K19/54 , G02F1/13363 , G02F1/1337
摘要： PROBLEM TO BE SOLVED: To provide a new optically anisotropic material having a high refractive index anisotropy and optical resistance to blue laser, and suppressed in film thickness unevenness and orientation distortion; and also to provide an optical element and a new liquid crystal compound for obtaining these products.SOLUTION: The new optically anisotropic material is represented by the following formula. The polymerizable liquid crystal compound containing the compound is prepared, and then by polymerizing the compound, the optically anisotropic and the optical element are obtained. In the formula of CF=CFCXYCH(CZ-O-W-(CH)-R-(CH)-(O)-W-(E)-W-(E)-(E)-E-R)CHCH=CH, Ris a single bond, 1C-12C alkylene group or the like; Ris 1C-8C alkyl group; Eis 1,4 phenylene group; E, Eand Eare each independently 1,4-phenylene group, trans-1,4-cyclohexylene group, or trans-2,6-decahydrophenylene group; and CZ is a methylene group or the like.
摘要翻译：要解决的问题：提供具有高折射率各向异性和对蓝色激光的光电阻的新的光学各向异性材料，并且抑制了膜厚度不均匀性和取向变形; 并且还提供用于获得这些产品的光学元件和新的液晶化合物。
解决方案：新的光学各向异性材料由下式表示。制备含有该化合物的可聚合液晶化合物，然后通过聚合化合物，获得光学各向异性和光学元件。在CF 2 = CFCXYCH（CZ-OW 1 - （CH 2 < / SB>） m -R 1 - （CH 2 ）< SB POS =“POST”> n - （O） i -W 2 - （E 1 ） h -W 3 - （E 2 ） j - （E 3 ） k 2 = > 2 -R 2 ）CH 2 CH = CH 2 ，R 1 是单键，1C-12C亚烷基等; R 2 是1C-8C烷基; E 1 是1,4-亚苯基; E 2 ，E 3 和E 4 亚苯基，反-1,4-亚环己基或反-2,6-癸氢亚苯基; CZ是亚甲基等。版权所有（C）2012，JPO＆INPIT

50. 发明专利

JP2011225674A Coating composition for surface application used for blade of wind-power generator, and blade of wind-power generator and process for production thereof 审中-公开
标题翻译：用于风力发电机叶片的表面涂层涂层组合物，风力发电机叶片及其生产方法
公开(公告)号：JP2011225674A
公开(公告)日：2011-11-10
申请号：JP2010095211
申请日：2010-04-16
申请人： Asahi Glass Co Ltd , 旭硝子株式会社
发明人： NAKANO TAKASHI , SHIROTA NAOKO
IPC分类号： C09D153/00 , C09D7/12 , C09D123/08 , C09D127/18 , F03D11/00
CPC分类号： Y02P70/523
摘要： PROBLEM TO BE SOLVED: To provide a coating composition for surface application used for a blade of the wind-power generator which can form a coating film excellent in workability, scratch resistance, and weather resistance on the blade surface of the wind-power generator, and a blade and a process for production thereof.SOLUTION: The coating composition for surface application used for a blade of a wind-power generator contains a fluororesin. The blade of the wind-power generator having a coating film formed on the blade substrate surface from the coating composition for surface application used for the blade of the wind-power generator is also provided. The process for production of the blade is also provided.
摘要翻译：要解决的问题：提供一种用于风力发电机叶片的表面涂布用组合物，其能够形成在风力发电机的叶片表面上的加工性，耐划伤性和耐候性优异的涂膜，发电机，叶片及其制造方法。解决方案：用于风力发电机叶片的用于表面应用的涂料组合物含有氟树脂。还提供了具有从用于风力发电机的叶片的表面涂布用涂料组合物形成在叶片基板表面上的涂膜的风力发电机的叶片。还提供了用于生产叶片的方法。版权所有（C）2012，JPO＆INPIT

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