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    • 43. 发明授权
    • Method of producing a plasma-resistant thermal oxide coating
    • 制造耐等离子体热氧化物涂层的方法
    • US08758858B2
    • 2014-06-24
    • US13374980
    • 2012-01-25
    • Jennifer Y. SunLi XuKenneth S. CollinsThomas GravesRen-Guan DuanSenh Thach
    • Jennifer Y. SunLi XuKenneth S. CollinsThomas GravesRen-Guan DuanSenh Thach
    • B05D3/02
    • C23C16/4404H01J37/32467H01J37/32477
    • A method of creating a plasma-resistant thermal oxide coating on a surface of an article, where the article is comprised of a metal or metal alloy which is typically selected from the group consisting of yttrium, neodymium, samarium, terbium, dysprosium, erbium, ytterbium, scandium, hafnium, niobium or combinations thereof. The oxide coating is formed using a time-temperature profile which includes an initial rapid heating rage, followed by a gradual decrease in heating rate, to produce an oxide coating structure which is columnar in nature. The grain size of the crystals which make up the oxide coating is larger at the surface of the oxide coating than at the interface between the oxide coating and the metal or metal alloy substrate, and the oxide coating is in compression at the interface between the oxide coating and the metal or metal alloy substrate.
    • 一种在制品的表面上产生耐等离子体热氧化物涂层的方法,其中制品由金属或金属合金组成,金属或金属合金通常选自钇,钕,钐,铽,镝,铒, 镱,钪,铪,铌或其组合。 使用时间 - 温度曲线形成氧化物涂层,其包括初始的快速加热,然后逐渐降低加热速率,以产生本质上为柱状的氧化物涂层结构。 构成氧化物涂层的晶体的晶粒尺寸在氧化物涂层的表面比在氧化物涂层和金属或金属合金衬底之间的界面处大,并且氧化物涂层在氧化物之间的界面处被压缩 涂层和金属或金属合金基材。