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41. 发明公开

EP1303347A1 VERFAHREN UND VORRICHTUNG ZUR AUTOMATISIERTEN HERSTELLUNG UND CHARAKTERISIERUNG VON FLÜSSIGEN MEHRKOMPONENTENSYSTEMEN 有权
标题翻译：方法和装置液体多组分系统自动化生产及表征
公开(公告)号：EP1303347A1
公开(公告)日：2003-04-23
申请号：EP01960514.6
申请日：2001-07-18
申请人： BASF AKTIENGESELLSCHAFT
发明人： BECKER, Dietmar , BECK, Georg , BENTZ, Stefan , BEST, Wolfgang , ERK, Peter , ETZRODT, Günter , KÖNEMANN, Martin , RIEGER, Reinhold , UNTERFORSTHUBER, Klaus
IPC分类号： B01F13/10 , B01F15/04
CPC分类号： B01F13/1055 , B01F11/02 , B01F15/00207 , B01F15/00214 , B01F15/0441 , B01F2215/005 , G01N21/25 , G01N21/83 , G01N35/0099 , G01N35/028 , G01N35/10 , G01N2035/00188 , G01N2035/00217 , G01N2035/00752
摘要： The invention relates to a method for carrying out the automated preparation and characterization of liquid multi-constituent systems comprised of at least two, preferably at least three, constituents. The inventive method involves the automated preparation of a mixture by combining at least two, preferably at least three, constituents in a vessel, whereby at least one constituent is dosed into the vessel in an automated manner. The method also involves the automated homogenization of the mixture followed by an automated measuring and evaluation. The device for implementing said method comprises at least one dosing station (5), a closing station (7), a homogenizing station (9), a measuring station (13) for determining formulation properties, and an evaluation unit.

42. 发明公开

EP1597232A1 NEUE KRISTALLINE MODIFIKATION DES ANHYDRATES VON BOSCALID 有权转让
标题翻译：作者无水啶酰菌胺新的结晶改良
公开(公告)号：EP1597232A1
公开(公告)日：2005-11-23
申请号：EP04705809.4
申请日：2004-01-28
申请人： BASF Aktiengesellschaft
发明人： MAYER, Winfried , ZIEGLER, Hans , SCHNEIDER, Karl-Heinrich , KRÖHL, Thomas , MAYER, Horst , ERK, Peter , COX, Gerhard , STIERL, Reinhard
IPC分类号： C07D213/82 , A01N43/40
CPC分类号： C07D213/82 , A01N43/40
摘要： The invention relates to monoclinic 2-chloro-N-(4'-chlorobiphenyl-2-yl)-nicotinamide of formula (I), which melts at a temperature of between 147 and 148 °C, and to a method for producing the same.

43. 发明授权

EP1516018B1 VERFAHREN ZUR UEBERFUEHRUNG VON PERYLEN-3,4:9, 10-TETRACARBONSAEUREDIIMIDEN IN EINE FUER DIE ANWENDUNG ALS FLUORESZENZFARBMITTEL GEEIGNETE FORM 有权
标题翻译： VERFAHREN ZUR UEBERFUEHRUNG VON PERYLEN-3,4：9，10-TETRACARBONSAEEDIIMIDEN IN EINE FUER DIE ANWENDUNG ALS FLUORESZENZFARBMITTEL GEEIGNETE FORM
公开(公告)号：EP1516018B1
公开(公告)日：2005-11-23
申请号：EP03735563.3
申请日：2003-06-06
申请人： BASF Aktiengesellschaft
发明人： ERK, Peter , SCHÄFER, Simone , BÖHM, Arno , BLASCHKA, Peter , ARMS, Harald , HELFER, Willi
IPC分类号： C09B5/62
CPC分类号： C09B67/0014 , C09B67/0025
摘要： Disclosed is a method for converting perylen-3,4:9,10-tetracarboxylic acid diimides of general formula I in which R and R represent unbranched, branched, or cyclical C1-C8-alkyl, into a form that is suitable for use as a fluorescent dye by a) solving or suspending the perylen-3,4:9,10-tetracarboxylic acid diimides in an organic or inorganic solvent, the molecules of which have a molecular volume of = 230 ANGSTROM , at 0 to 250 DEG C; b1) cooling the solution obtained in step a) to or below the crystallization temperature and at the same time optionally removing excess solvent until crystals start forming in case an organic solvent is used or adding water or diluted aqueous solutions of the solvent until crystals start forming in case an inorganic solvent is used, and maintaining said solution at said temperature for further crystallization; or b2) cooling the suspension obtained in step a) to or below the crystallization temperature if the temperature in step a) was above the crystallization temperature and maintaining the suspension at said temperature for further crystallization; c) isolating the solvate crystals formed in step b); and d) then removing the solvent from the solvate crystals. Also disclosed are novel crystalline forms of perylen-3,4:9,10-tetracarboxylic acid diimides.
摘要翻译：公开了用于将通式I的苝-3,4：9,10-四甲酸二酰亚胺（其中R 1和R 2代表无支链，支链或环状C 1 -C 8烷基）转化成其适合用作荧光染料：a）将苝-3,4：9,10-四甲酸二酰亚胺溶解或悬浮在有机或无机溶剂中，其分子的分子量为230Å<3 在0至250℃下; b1）将步骤a）中获得的溶液冷却至结晶温度或低于结晶温度，并且同时任选地除去过量的溶剂直至在使用有机溶剂的情况下开始形成晶体或者加入水或稀释的溶剂水溶液直至晶体开始形成在使用无机溶剂的情况下，并且将所述溶液保持在所述温度以进一步结晶; 或b2）如果步骤a）中的温度高于结晶温度并将悬浮液保持在所述温度以进一步结晶，则将步骤a）中获得的悬浮液冷却至或低于结晶温度; c）分离步骤b）中形成的溶剂合物晶体; 和d）然后从溶剂合物晶体中除去溶剂。还公开了苝-3,4：9,10-四甲酸二酰亚胺的新颖结晶形式。

44. 发明授权

EP1373272B1 TERT.-ALKYLPHENOXYSUBSTITUIERTE POLYCYCLISCHE VERBINDUNGEN 有权
标题翻译：叔丁基苯氧基缩水甘油聚环酯VERBINDUNGEN
公开(公告)号：EP1373272B1
公开(公告)日：2005-06-29
申请号：EP02735166.7
申请日：2002-03-20
申请人： BASF AKTIENGESELLSCHAFT
发明人： BÖHM, Arno , HELFER, Willi , BECK, Georg , KRIEGER, Matthias , ERK, Peter
IPC分类号： C07D487/06 , C07D209/56 , C07D241/38 , C07D487/22 , C09B69/10
CPC分类号： C07D241/38 , C07D209/56 , C07D211/08 , C07D471/06 , C07D487/06 , C08K5/0041 , C09B3/44 , C09B5/62 , C09B47/18 , C09B69/00 , C09D5/36 , C09D11/037
摘要： Tert. alkylphenoxy substituted polycyclic compounds of general formula (I), in which the variables have the following meanings: P = a conjugated polycyclic group, optionally aryl substituted, stable to base and acid and not containing residues from the group -CO-NH-CO-, -COOH and -CO-O-CO-; R = C1-C8 alkyl, the carbon chain of which may be interrupted by one or several groups of -O-, -S-, -NR1-, -CO- and/or -SO¿2?- and which may be mono- or serially-substituted by C1-C6 alkoxy or a 5- to 7-membered heterocyclic group, bonded by means of a nitrogen atom, which can contain further heteroatoms and can be aromatic, C5-C8 cycloalkyl, the carbon skeleton of which may be interrupted by one or several groups of -O-, -S-, -NR?1¿-, -CO- and/or -SO¿2?- and may optionally be substituted with C1-C6 alkyl; R?1¿ = H or C¿1?-C6 alkyl; Hal = chlorine and/or bromine; m = a number from 0 to 15; n = a number from 1 to 16, whereby the sum m + n ≤ 16, production and use thereof.
摘要翻译：叔。（I）的烷基苯氧基取代的多环化合物，其中变量具有以下含义：P =共轭多环基团，任选被芳基取代，对碱和酸稳定并且不含来自基团-CO-NH-CO- ，-COOH和-CO-O-CO-; R = C 1 -C 8烷基，其碳链可以被-O - ， - S - ， - NR 1 - ， - CO-和/或-SO 2 - 的一个或几个基团间隔，并且可以是单 - 或通过可含有其他杂原子且可为芳族的氮原子键合的C1-C6烷氧基或5至7元杂环基连续取代的C 5 -C 8环烷基，其碳骨架可以是被-O - ， - S-，-NR 1 - ， - CO-和/或-SO 2 - 的一个或几个基团中断，并且可以任选地被C 1 -C 6烷基取代; R 1 = H或C 1 -C 6烷基; Hal =氯和/或溴; m =从0到15的数字; n =从1到16的数字，由此总和m +n≤16，其生产和使用。

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