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41. 发明申请

WO2011139591A2 PROCESS FOR DEHYDROHALOGENATION OF HALOGENATED ALKANES 审中-公开
标题翻译：脱氢烷基脱氢酶的方法
公开(公告)号：WO2011139591A2
公开(公告)日：2011-11-10
申请号：PCT/US2011/033522
申请日：2011-04-22
申请人： HONEYWELL INTERNATIONAL INC. , COOK, George R. , KOPKALLI, Haluk , COTTRELL, Stephen A. , CHIU, Yuon , SCHEIDLE, Peter , MERKEL, Daniel C.
发明人： COOK, George R. , KOPKALLI, Haluk , COTTRELL, Stephen A. , CHIU, Yuon , SCHEIDLE, Peter , MERKEL, Daniel C.
IPC分类号： C07C17/23 , C07C21/18
CPC分类号： C07C17/23 , C07C17/25 , C07C21/18
摘要： A process for the manufacture of halogenated olefins in semi-batch mode by dehydrohalogenation of halogenated alkanes in the presence of an aqueous base such as KOH which simultaneously neutralizes the resulting hydrogen halide. During the process, aqueous base is continuously added to the haloalkane which results in better yields, lower by-product formation and safer/more controllable operation.
摘要翻译：一种通过卤化烷烃在碱性水溶液（如KOH）的存在下脱卤化氢同时中和所得卤化氢，以半间歇模式制造卤代烯烃的方法。在此过程中，将水性碱连续加入到卤代烷烃中，产生更好的产率，更低的副产物形成和更安全/更可控的操作。

42. 发明申请

WO2011126620A2 SEPARATION OF CLOSE BOILING COMPOUNDS BY ADDITION OF A THIRD COMPOUND 审中-公开
标题翻译：通过添加第三种化合物分离接近沸点的化合物
公开(公告)号：WO2011126620A2
公开(公告)日：2011-10-13
申请号：PCT/US2011/026447
申请日：2011-02-28
申请人： HONEYWELL INTERNATIONAL INC. , MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh S. , PHAM, Hang T. , SINGH, Rajiv R.
发明人： MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh S. , PHAM, Hang T. , SINGH, Rajiv R.
IPC分类号： C07C17/386 , C07C19/10 , C07C21/18 , B01D3/36
CPC分类号： B01D3/36 , C07C17/386 , C07C19/10 , C07C21/18
摘要： The invention provides a method for separating halocarbons. In particular, a method for separating 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb) from 2-chloro-3,3,3-trifluoropropene (HCFC-1233xf) by adding a third component and then separating via conventional distillation. More particularly the invention pertains to a method for separating HCFC-244bb from HCFC-1233xf which are useful as intermediates in the production of 2,3,3,3-tetrafluoropropene (HFO-1234yf).
摘要翻译：本发明提供一种分离卤代烃的方法。特别是通过添加第三成分分离2-氯-3,3,3-三氟丙烯（HCFC-1233xf）而分离出2-氯-1,1,1,2-四氟丙烷（HCFC-244bb）的方法，通过常规蒸馏。更具体地说，本发明涉及从HCFC-1233xf中分离HCFC-244bb的方法，其可用作制备2,3,3,3-四氟丙烯（HFO-1234yf）中的中间体。

43. 发明申请

WO2011103035A2 INTEGRATED PROCESS AND METHODS OF PRODUCING (E)-1-CHLORO-3,3,3-TRIFLUOROPROPENE 审中-公开
标题翻译：（E）-1-氯-3,3,3-三氟丙烯的一体化方法和生产方法
公开(公告)号：WO2011103035A2
公开(公告)日：2011-08-25
申请号：PCT/US2011024483
申请日：2011-02-11
申请人： HONEYWELL INT INC , TUNG HSUEH S , JOHNSON ROBERT , POKROVSKI KONSTANTIN , MERKEL DANIEL C
发明人： TUNG HSUEH S , JOHNSON ROBERT , POKROVSKI KONSTANTIN , MERKEL DANIEL C
IPC分类号： C07C17/10 , B01J27/135 , C07C21/18
CPC分类号： B01J19/245 , B01J23/26 , B01J37/26 , B01J2219/00006 , B01J2219/24 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C17/358 , C07C17/383 , Y02P20/125 , Y02P20/582 , C07C21/18
摘要： The present invention relates to methods, process, and integrated systems for economically producing (E)-1-chloro-3,3,3-trifluoropropene via vapor phase and/or liquid processes.
摘要翻译：本发明涉及经由气相和/或液体方法经济地生产（E）-1-氯-3,3,3-三氟丙烯的方法，工艺和集成系统。

44. 发明申请

WO2011068649A2 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 审中-公开
标题翻译：生产氟化有机化合物的方法
公开(公告)号：WO2011068649A2
公开(公告)日：2011-06-09
申请号：PCT/US2010/056291
申请日：2010-11-11
申请人： HONEYWELL INTERNATIONAL INC. , MERKEL, Daniel, C. , JOHNSON, Robert, C. , TUNG, Hsueh Sung
发明人： MERKEL, Daniel, C. , JOHNSON, Robert, C. , TUNG, Hsueh Sung
IPC分类号： C07C17/10 , C07C17/25 , C07C19/10 , B01J27/08 , B01J23/26
CPC分类号： C07C17/013 , C07C17/087 , C07C19/10
摘要： Provided is a process for making 2-chloro-1,1,1,2-tetrafluoropropane. The process has the step of hydrofluorinating 2-chloro-3,3,3-trifluoropropene in the presence of a catalyst selected from the group consisting of SbCl 3 , SbCl 5 , SbF 5 , TiCl 4 , SnCl 4 , Cr 2 O 3 , and fluorinated Cr 2 O 3 .
摘要翻译：提供了制备2-氯-1,1,1,2-四氟丙烷的方法。该方法具有在选自SbCl 3，SbCl 5，SbF 5，TiCl 4，SnCl 4，Cr 2 O 3和氟化Cr 2 O 3的催化剂存在下氢化2-氯-3,3,3-三氟丙烯的步骤。

45. 发明申请

WO2010051340A3 AZEOTROPE-LIKE COMPOSITIONS OF 1,1,1,2,3-PENTACHLOROPROPANE AND HYDROGEN FLUORIDE 审中-公开
标题翻译： 1,1,1,2,3-戊二醇和氢氟酸的类似物组合物
公开(公告)号：WO2010051340A3
公开(公告)日：2010-07-22
申请号：PCT/US2009062481
申请日：2009-10-29
申请人： HONEYWELL INT INC , TUNG HSUEH S , PHAM HANG T , SINGH RAJIV R , MERKEL DANIEL C
发明人： TUNG HSUEH S , PHAM HANG T , SINGH RAJIV R , MERKEL DANIEL C
IPC分类号： C07C19/01 , C11D7/50 , C23G5/028
CPC分类号： C23G5/02806 , C01B7/191 , C07C17/206 , C07C17/25 , C07C19/01 , C09K3/30 , C11D7/5045 , C23G5/028 , C07C21/18
摘要： An azeotrope-like composition consisting essentially of 1,1,1,2,3-pentachloropropane and hydrogen fluoride is provided, as well as methods that involve such an azeotrope-like composition.
摘要翻译：提供了基本上由1,1,1,2,3-五氯丙烷和氟化氢组成的类共沸组合物，以及涉及这种类共沸组合物的方法。

46. 发明申请

WO2007079431A8 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 审中-公开
标题翻译：生产氟化有机化合物的方法
公开(公告)号：WO2007079431A8
公开(公告)日：2008-08-21
申请号：PCT/US2007000056
申请日：2007-01-03
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , MUKHOPADHYAY SUDIP , VAN DER PUY MICHAEL , MA JING JI , BORTZ CHERYL , LIGHT BARBARA , PHILLIPS STEVEN D , DUBEY RAJESH , MERKEL DANIEL C
发明人： TUNG HSUEH SUNG , MUKHOPADHYAY SUDIP , VAN DER PUY MICHAEL , MA JING JI , BORTZ CHERYL , LIGHT BARBARA , PHILLIPS STEVEN D , DUBEY RAJESH , MERKEL DANIEL C
IPC分类号： C07C17/087 , C07C21/19 , C09K5/00
CPC分类号： C07C19/10 , C07C17/04 , C07C17/06 , C07C17/087 , C07C17/206 , C07C17/21 , C07C17/25 , C07C21/18 , C07C19/01 , C07C21/073
摘要： Disclosed are processes for the production of fluorinated olefins, preferably adapted to commercialization of CF 3 CF=CH 2 (1234yf). Three steps may be used in preferred embodiments in which a feedstock such as CCI 2 =CCICH 2 CI (which may be purchased or synthesized from 1,2,3- trichloropropane) is fluorinated (preferably with HF in gas-phase in the presence of a catalyst) to synthesize a compound such as CFaCCl=CH2, preferably in a 80-96% selectivity. The CF 3 CCl=CH 2 is preferably converted to CF 3 CFClCH 3 (244-isomer) using a SbCl 5 as the catalyst which is then transformed selectively to 1234yf, preferably in a gas-phase catalytic reaction using activated carbon as the catalyst. For the first step, a mixture Of Cr2O3 and FeCl 3 /C is preferably used as the catalyst to achieve high selectivity to CF 3 CCl=CH 2 (96%). In the second step, SbCl 5 /C is preferably used as the selective catalyst for transforming 1233xf to 244-isomer, CF 3 CFClCH 3 . The intermediates are preferably isolated and purified by distillation and used in the next step without further purification, preferably to a purity level of greater than about 95%.
摘要翻译：公开了用于生产氟化烯烃的方法，优选适于CF 3 CH 2 CH 2（1234yf）的商业化。优选实施方案中可以使用三个步骤，其中诸如CCI 2 = CCICH 2 Cl（其可以从1,2,3-三氯丙烷购买或合成）被氟化（优选在催化剂存在下在气相中用HF）合成化合物如CFaClCl = CH 2，优选为80-96％的选择性。 CF 3 3 CCl = CH 2 2优选使用以下化合物转化为CF 3 CFClCH 3（244-异构体） SbCl 5作为催化剂，然后将其选择性地转化为1234yf，优选在使用活性炭作为催化剂的气相催化反应中进行。对于第一步，优选使用Cr 2 O 3和FeCl 3/3的混合物作为催化剂，以实现对CF 3 CCl = CH 2 / （96％）。在第二步中，优选使用SbCl 5 / C作为将1233xf转化为244-异构体CF 3 CFClCH 3的选择性催化剂。中间体优选通过蒸馏分离和纯化，并且用于下一步骤而不进一步纯化，优选纯度高于约95％。

47. 发明申请

WO2007079435A2 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 审中-公开
标题翻译：生产氟化有机化合物的方法
公开(公告)号：WO2007079435A2
公开(公告)日：2007-07-12
申请号：PCT/US2007/000064
申请日：2007-01-03
申请人： HONEYWELL INTERNATIONAL INC. , TUNG, Hsueh Sung , MUKHOPADHYAY, Sudip , VAN DER PUY, Michael , MA, Jing Ji , MERKEL, Daniel, C. , BORTZ, Cheryl , LIGHT, Barbara , PHILLIPS, Steven, D. , FLEMING, Kim, M. , FERGUSON, Susan
发明人： TUNG, Hsueh Sung , MUKHOPADHYAY, Sudip , VAN DER PUY, Michael , MA, Jing Ji , MERKEL, Daniel, C. , BORTZ, Cheryl , LIGHT, Barbara , PHILLIPS, Steven, D. , FLEMING, Kim, M. , FERGUSON, Susan
CPC分类号： C07C17/10 , C07C17/00 , C07C17/087 , C07C17/206 , C07C17/25 , C07C17/383 , C07C19/10 , C07C19/01 , C07C19/08 , C07C21/18
摘要： Disclosed is a process for producing fluorinated organic compounds, including hydrofluoropropenes, which preferably comprises converting at least one compound of Formula (I): C(X)3CF2C(X)3 (I) to at least one compound of Formula (II) CF3CF=CHZ (II) where each X and Z is independently H, F, Cl, I or Br, said process preferably not including any substantial amount of oxygen-containing catalyst in certain embodiments. Preferably Z is H.
摘要翻译：公开了一种制备氟化有机化合物的方法，包括氢氟丙烯，其优选包括将至少一种式（I）化合物：C（X）3CF 2 C（X）3（I）转化为至少一种式（II）化合物CF 3 CF = CHZ（II）其中每个X和Z独立地为H，F，Cl，I或Br，在某些实施方案中，所述方法优选不包括任何显着量的含氧催化剂。 Z优选为

48. 发明申请

WO2007056127A1 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 审中-公开
标题翻译：生产氟化有机化合物的方法
公开(公告)号：WO2007056127A1
公开(公告)日：2007-05-18
申请号：PCT/US2006/042935
申请日：2006-11-03
申请人： HONEYWELL INTERNATIONAL INC. , MUKHOPADHYAY, Sudip , NAIR, Haridasan , TUNG, Hsueh Sung , VAN DER PUY, Michael , JOHNSON, Robert , MERKEL, Daniel, C.
发明人： MUKHOPADHYAY, Sudip , NAIR, Haridasan , TUNG, Hsueh Sung , VAN DER PUY, Michael , JOHNSON, Robert , MERKEL, Daniel, C.
IPC分类号： C07C17/266 , C07C17/269 , C07C21/18
CPC分类号： C07C21/18 , C07C17/266 , C07C17/269
摘要： Disclosed is a process for the preparation of fluorinated C3 olefins comprising contacting a compound of the Formula (I): C(R 1 a R 2 b R 3 c ), with a compound of Formula (II) C(R 1 a R 2 b R 3 c )C n (R 1 a R 2 b R 3 c ): wherein R 1 a , R 2 b, and R 3 c are independently a hydrogen atom or a halogen selected from the group consisting of fluorine; chlorine, bromine and iodine, provided that the compound of formula (I) has at least three halogen substituents and that said at three halogen substituents comprise at least one fluorine; a, b and c are independently= 0, 1, 2 or 3 and (a+b+c) = 2 or 3; and n is 0 or 1, under conditions effective to produce at least one C3 fluoroolefin.
摘要翻译：公开了一种制备氟化C3烯烃的方法，包括使式（I）的化合物：C（R 1）

49. 发明申请

WO2005097716A1 METHOD OF MAKING DIFLUOROMETHANE, 1,1,1-TRIFLUOROETHANE AND 1,2-DIFLUOROETHANE 审中-公开
标题翻译：制备二氟甲磺酸的方法，1,1,1-三氟乙基和1,2-二氟乙基
公开(公告)号：WO2005097716A1
公开(公告)日：2005-10-20
申请号：PCT/US2005/011125
申请日：2005-03-31
申请人： HONEYWELL INTERNATIONAL INC. , MERKEL, Daniel, C. , SHANKLAND, Ian , TUNG, Hsuehsung
发明人： MERKEL, Daniel, C. , SHANKLAND, Ian , TUNG, Hsuehsung
IPC分类号： C07C17/20
CPC分类号： B01J27/125 , B01J21/18 , B01J27/08 , B01J27/135 , B01J37/26 , C07C17/206 , C07C17/208 , C07C17/21 , C07C19/08 , Y02P20/582
摘要： A process for the production of difluoromethane (HFC-32), 1,1,1-trifluoroethane (HFC-143a) and 1,1-difluoroethane (HFC-152a). In the process the following steps are employed: (a) providing a reaction vessel, (b) providing in the reaction vessel activated carbon impregnated with a strong Lewis acid fluorination catalyst selected from halides of As, Sb, Al, TI, In, V, Nb, Ta, Ti, Zr and Hf, (c) activating the catalyst by passing through the activated carbon impregnated with a strong Lewis acid fluorination catalyst anhydrous hydrogen fluoride gas and chlorine gas, (d) contacting, in vapor state in the reaction vessel containing the activated catalyst, hydrogen fluoride and one or more halogenated hydrocarbons selected from chlorofluoromethane, dichloromethane, 1,1,1-trichloroethane, vinyl chloride, 1,1-dichloroethylene, 1.2-dichloroethylene, 1,2-dichloroethane, and 1,1-dichloroethane for a time and at a temperature to produce a product stream comprising hydrofluorocarbon product(s) corresponding to the chlorinated hydrocarbon reactant(s), and one or more of hydrogen chloride, unreactacted chlorinated hydrocarbon reactant(s), under-fluorinated intermediates, and unreacted hydrogen fluoride, and (e) separating the hydrofluorocarbon product(s) from the product stream.
摘要翻译：制备二氟甲烷（HFC-32），1,1,1-三氟乙烷（HFC-143a）和1,1-二氟乙烷（HFC-152a）的方法。在该过程中，采用以下步骤：（a）提供反应容器，（b）在反应容器中提供用强路易斯酸氟化催化剂浸渍的活性炭，该催化剂选自As，Sb，Al，TI，In，V ，Nb，Ta，Ti，Zr和Hf，（c）通过浸渍有强力路易斯酸氟化催化剂的无水氟化氢气体和氯气的活性炭活化催化剂，（d）在反应中以气态接触含有活化催化剂的容器，氟化氢和选自氯氟甲烷，二氯甲烷，1,1,1-三氯乙烷，氯乙烯，1,1-二氯乙烯，1,2-二氯乙烯，1,2-二氯乙烷和1,1-二氯乙烷的一种或多种卤代烃，在一个温度下产生包含对应于氯代烃反应物的氢氟烃产物的产物流，以及一种或多种氯化氢，未反应的氯化氢化碳氢化合物 n反应物，非氟化中间体和未反应的氟化氢，和（e）从产物流中分离氢氟烃产物。

50. 发明申请

WO2005012212A2 PROCESS FOR THE MANUFACTURE OF 1,3,3,3 TETRAFLUOROPROPENE 审中-公开
标题翻译：制备1,3,3,3-四氢呋喃的方法
公开(公告)号：WO2005012212A2
公开(公告)日：2005-02-10
申请号：PCT/US2004023160
申请日：2004-07-21
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , MERKEL DANIEL C , JOHNSON ROBERT C
发明人： TUNG HSUEH SUNG , MERKEL DANIEL C , JOHNSON ROBERT C
IPC分类号： B01J21/18 , B01J27/10 , C07C17/04 , C07C17/20 , C07C17/25 , C07C19/08 , C07C21/18 , C07C17/00
CPC分类号： B01J27/10 , B01J21/18 , C07C17/04 , C07C17/206 , C07C17/25 , C07C19/08 , C07C21/18 , C07C19/10
摘要： The invention provides an economic process for the manufacture of 1,3,3,3tetrafluoropropene (HFC-1234ze) by a two stage process. A hydr6fluorination of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) into 1-chloro.-1,3,3,3 tetrafluoropropane (HCFC-244fa) and 1,1,1,3,3-pent afluoropropane (HFC 245fa) is conducted, followed by the dehydrochlorination of (HCFC-244)fa and dehydrofluorination of (HFC-245)fa into (HFC-1234)ze.
摘要翻译：本发明提供了通过两阶段方法制造1,3,3,3-四氟丙烯（HFC-1234ze）的经济方法。将1-氯-3,3,3-三氟丙烯（HCFC-1233zd）氟化为1-氯-1,3,3,3四氟丙烷（HCFC-244fa）和1,1,1,3,3-戊烯（HFC 245fa），然后将（HCFC-244）fa的脱氯化氢和（HFC-245）fa的脱氟化氢分解成（HFC-1234）ze。

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