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    • 35. 发明授权
    • Ceramic tape formulations with green tape stability
    • 陶瓷胶带配方,绿带稳定
    • US5766528A
    • 1998-06-16
    • US800489
    • 1997-02-14
    • Wei-Fang SuDeborah P. Partlow
    • Wei-Fang SuDeborah P. Partlow
    • C04B35/634C04B35/622
    • C04B35/63472C04B35/634
    • A method for producing ceramic tape used to fabricate electronic devices while eliminating continued shrinkage of the unfired tape. Chemical agents are added to a mixture of ceramic powder and binder to manipulate the crosslinking of the binder. A first approach involves promoting the crosslinking reaction to completion quickly. The second approach involves preventing the crosslinking reaction during the tape slurry mixing and casting processes. A solvent is used to accelerate the crosslinking of the binder in which the solvent may include one or more of acetone, acetylacetone, toluene and ethanol. Preferably, the solvent is a combination of acetone and acetylacetone. A polyhydroxy compound, such as glycerine, may be added to accelerate the crosslinking reaction of the binder. The boron in the tape may alternatively be rendered inoperative as a crossing agent for the binder by pre-reacting the boron with the Lewis base prior to contact with the binder. The preferred Lewis base is an organic amine, such as piperidine.
    • 一种制造用于制造电子装置的陶瓷带的方法,同时消除未烧结带的持续收缩。 将化学试剂加入到陶瓷粉末和粘合剂的混合物中以操纵粘合剂的交联。 第一种方法是促进交联反应迅速完成。 第二种方法涉及在胶带浆料混合和流延过程中防止交联反应。 使用溶剂来加速粘合剂的交联,其中溶剂可以包括丙酮,乙酰丙酮,甲苯和乙醇中的一种或多种。 优选地,溶剂是丙酮和乙酰丙酮的组合。 可以加入多羟基化合物如甘油以加速粘合剂的交联反应。 胶带中的硼可以替代地作为粘合剂的交叉剂不起作用,在与粘合剂接触之前使硼与路易斯碱预反应。 优选的路易斯碱是有机胺,例如哌啶。