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31. 发明授权

US5420085A Methods of making composite aluminum nitride ceramic articles having embedded filler 失效
标题翻译：制备具有嵌入填料的复合氮化铝陶瓷制品的方法
公开(公告)号：US5420085A
公开(公告)日：1995-05-30
申请号：US7387
申请日：1993-01-21
申请人： Marc S. Newkirk , Harry R. Zwicker , Andrew W. Urquhart , Harold D. Lesher , Terry D. Claar , Michael K. Aghajanian , John P. Biel, Jr.
发明人： Marc S. Newkirk , Harry R. Zwicker , Andrew W. Urquhart , Harold D. Lesher , Terry D. Claar , Michael K. Aghajanian , John P. Biel, Jr.
IPC分类号： C04B35/65 , C04B35/76 , C04B35/80 , C04B41/50 , C04B41/87 , C04B35/58
CPC分类号： C04B41/5025 , C04B35/652 , C04B35/76 , C04B35/80 , C04B41/87
摘要： A method of making self-supporting ceramic composite structures having filler embedded therein includes infiltrating a permeable mass of filler with polycrystalline material comprising an oxidation reaction product obtained by oxidation of a parent metal such as aluminum and optionally, containing therein non-oxidized constituents of the parent metal. The structure is formed by placing a parent metal adjacent to a permeable filler and heating the assembly to melt the parent metal and provide a molten body of parent metal which is contacted with a suitable vapor-phase oxidant. Within a certain temperature region and optionally, aided by one or more dopants in or on the parent metal, molten parent metal will migrate through previously formed oxidation reaction product into contact with the oxidant, causing the oxidation reaction product to grow so as to embed the adjacent filler and provide the composite structure. In a preferred embodiment, a parent metal comprising aluminum is oxidized by a vapor-phase oxidant comprising nitrogen to form a ceramic matrix comprising an aluminum nitride oxidation reaction product. In a particularly preferred embodiment, one or more protective coatings are applied to the filler prior to formation of the aluminum nitride oxidation reaction product matrix.
摘要翻译：制造具有嵌入其中的填料的自支撑陶瓷复合结构的方法包括用多晶材料渗透可渗透的填料，所述多晶材料包含通过氧化母体金属如铝而获得的氧化反应产物，并且任选地含有其中的非氧化成分母金属。通过将母体金属放置在可渗透填料附近并加热该组件以熔化母体金属并提供与合适的气相氧化剂接触的母体金属的熔融体来形成结构。在一定温度范围内，任选地，由母体金属中或母体金属上的一种或多种掺杂剂辅助，熔融母体金属将迁移通过预先形成的氧化反应产物与氧化剂接触，使氧化反应产物生长，从而嵌入相邻填料并提供复合结构。在优选的实施方案中，包含铝的母体金属被包含氮的气相氧化剂氧化以形成包含氮化铝氧化反应产物的陶瓷基体。在特别优选的实施方案中，在形成氮化铝氧化反应产物基质之前，将一种或多种保护性涂料施加到填料上。

32. 发明授权

US5277989A Metal matrix composite which utilizes a barrier 失效
标题翻译：使用屏障的金属基复合材料
公开(公告)号：US5277989A
公开(公告)日：1994-01-11
申请号：US934823
申请日：1992-08-24
申请人： Michael K. Aghajanian , Terry D. Claar
发明人： Michael K. Aghajanian , Terry D. Claar
IPC分类号： C04B35/65 , C04B41/51 , C04B41/88 , C22C1/10 , C22C29/16
CPC分类号： C04B35/652 , C04B41/5155 , C04B41/88 , C22C1/1036 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486 , Y10T428/12576 , Y10T428/12583 , Y10T428/12736 , Y10T428/30
摘要： A net shaped ceramic-reinforced aluminum matrix composite is formed by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contacting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
摘要翻译：网状陶瓷增强铝基复合材料通过形成具有限定的具有阻挡层的表面边界的陶瓷材料的可渗透物质形成，并且在熔融的铝 - 镁合金与可渗透物质的陶瓷材料的存在下，约10至100％的氮气（体积），平衡非氧化气体，例如氢或氩。在这些条件下，熔融合金在正常大气压力下自发渗透到陶瓷块中直至达到屏障。合金的固体可以放置在与具有阻挡层的陶瓷材料的可渗透层合物附近，并且进入熔融状态，优选至少约700℃，以便通过渗透形成网状铝基复合材料。除了镁之外，辅助合金元素可以与铝一起使用。所得到的复合产品可能在铝基体中含有不连续的氮化铝相。

33. 发明授权

US5141819A Metal matrix composite with a barrier 失效
标题翻译：带屏障的金属基复合材料
公开(公告)号：US5141819A
公开(公告)日：1992-08-25
申请号：US657286
申请日：1991-02-19
申请人： Michael K. Aghajanian , Terry D. Claar
发明人： Michael K. Aghajanian , Terry D. Claar
IPC分类号： C04B35/65 , C04B41/51 , C04B41/88 , C22C1/10
CPC分类号： C04B41/88 , C04B35/652 , C04B41/5155 , C22C1/1036 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486 , Y10T428/12576 , Y10T428/12583 , Y10T428/12736
摘要： A net shaped ceramic-reinforced aluminum matrix composite is formed by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contracting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
摘要翻译：网状陶瓷增强铝基复合材料通过形成具有限定的具有阻挡层的表面边界的陶瓷材料的可渗透物质形成，并且在气体存在下将熔融的铝 - 镁合金与陶瓷材料的渗透物料接合，约10至100％的氮气（体积），平衡非氧化气体，例如氢或氩。在这些条件下，熔融合金在正常大气压力下自发渗透到陶瓷块中直至达到屏障。可以将合金的固体放置在具有阻挡层的陶瓷材料的可渗透层的附近，并且进入熔融状态，优选至少约700℃，以便通过渗透形成网状铝基复合材料。除了镁之外，辅助合金元素可以与铝一起使用。所得到的复合产品可能在铝基体中含有不连续的氮化铝相。

34. 发明授权

US5104029A Method of bonding a ceramic composite body to a second body and articles produced thereby 失效
标题翻译：将陶瓷复合体与第二体相结合的方法及其生产的制品
公开(公告)号：US5104029A
公开(公告)日：1992-04-14
申请号：US551290
申请日：1990-07-12
申请人： Terry D. Claar
发明人： Terry D. Claar
IPC分类号： C04B35/58 , C04B35/65 , C04B37/00 , C04B41/50 , C04B41/51
CPC分类号： C04B41/51 , C04B35/5607 , C04B35/5805 , C04B35/58071 , C04B35/58078 , C04B35/652 , C04B35/653 , C04B37/001 , C04B41/5053 , C04B2237/36 , C04B2237/363 , C04B2237/403 , Y10T428/249969 , Y10T428/24997 , Y10T428/24999 , Y10T428/252 , Y10T428/256 , Y10T428/257
摘要： This invention relates generally to a novel method of manufacturing a composite body and to novel products made thereby. More particularly, the invention relates to a method of producing a self-supporting composite body comprising one or more boron-containing compounds, e.g., a boride or a boride and carbide, by reactive infiltration of molten parent metal into a bed or mass containing boron carbide, and, optionally, one or more inert fillers and permitting residual or excess parent metal to remain bonded to the formed self-supporting composite body. The residual or excess metal is used to form a bond between the formed composite body and another body (e.g., a metal body, a ceramic body, or another composite body). In addition, this invention related to alternative methods of disposing metal on at least one surface of the above-described composite bodies (such as sputtering, CVD, etc.) to permit the composite bodies to be bonded to another body.
摘要翻译：本发明一般涉及一种制造复合体的新方法及其制成的新颖产品。更具体地说，本发明涉及通过将熔融母体金属反应性浸入含硼的床或物质中来生产包含一种或多种含硼化合物（例如硼化物或硼化物和碳化物）的自支撑复合体的方法碳化物和任选的一种或多种惰性填料，并允许残留或过量的母体金属保持结合到形成的自支撑复合体上。剩余或多余的金属用于在所形成的复合体与另一体（例如，金属体，陶瓷体或其它复合体）之间形成结合。此外，本发明涉及在上述复合体的至少一个表面（例如溅射，CVD等）上设置金属以允许复合体结合到另一个主体的替代方法。

35. 发明授权

US4883497A Formation of thin walled ceramic solid oxide fuel cells 失效
标题翻译：薄壁陶瓷固体氧化物燃料电池的形成
公开(公告)号：US4883497A
公开(公告)日：1989-11-28
申请号：US174146
申请日：1988-03-28
申请人： Terry D. Claar , Donald E. Busch , John J. Picciolo
发明人： Terry D. Claar , Donald E. Busch , John J. Picciolo
IPC分类号： H01M8/24
CPC分类号： H01M8/2435 , Y10T29/49115
摘要： To reduce thermal stress and improve bonding in a high temperature monolithic solid oxide fuel cell (SOFC), intermediate layers are provided between the SOFC's electrodes and electrolyte which are of different compositions. The intermediate layers are comprised of a blend of some of the materials used in the electrode and electrolyte compositions. Particle size is controlled to reduce problems involving differential shrinkage rates of the various layers when the entire structure is fired at a single temperature, while pore formers are provided in the electrolyte layers to be removed during firing for the formation of desired pores in the electrode layers. Each layer includes a binder in the form of a thermosetting acrylic which during initial processing is cured to provide a self-supporting structure with the ceramic components in the green state. A self-supporting corrugated structure is thus formed prior to firing, which the organic components of the binder and plasticizer removed during firing to provide a high strength, high temperature resistant ceramic structure of low weight and density.
摘要翻译：为了降低热应力并改善高温整体式固体氧化物燃料电池（SOFC）中的结合，在SOFC的电极和组成不同的电解质之间提供了中间层。中间层由电极和电解质组合物中使用的一些材料的共混物组成。控制粒径以减少在单个温度下烧结整个结构时各种层的不同收缩率的问题，同时在焙烧期间在电解质层中提供成孔剂以在电极层中形成所需孔的电解质层中形成孔。每层包括热固性丙烯酸形式的粘合剂，其在初始加工期间固化以提供具有处于绿色状态的陶瓷组分的自支撑结构。因此，在烧制之前形成自支撑的波纹状结构，其中烧结期间粘合剂和增塑剂的有机组分除去以提供低重量和密度的高强度，耐高温陶瓷结构。

36. 发明授权

US4579788A High temperature fuel cell wet seal 失效
标题翻译：高温燃料电池湿封
公开(公告)号：US4579788A
公开(公告)日：1986-04-01
申请号：US543130
申请日：1983-10-18
申请人： Leonard G. Marianowski , Terry D. Claar
发明人： Leonard G. Marianowski , Terry D. Claar
IPC分类号： H01M8/02 , H01M8/14 , H01M2/08
CPC分类号： H01M8/0271 , H01M8/142 , H01M2008/147 , H01M2300/0051 , Y02E60/526
摘要： High temperature fuel cell wet seal strips around the periphery of a separator plate fabricated utilizing powder metallurgy technique. The material composition of said wet seal may be variably graded to afford ease of bonding of said wet seal with the separator plate on one side and provide corrosion inhibition on the other side in communication with an electrolyte. Similar wet seals may be formed from a single metal powder with surface treatment of the surface adjacent the electrolyte to provide resistance to corrosion by the electrolyte.
摘要翻译：使用粉末冶金技术制造的隔板周围的高温燃料电池湿密封条。所述湿式密封件的材料组成可以可变地分级，以便容易地将所述湿式密封件与隔板在一侧上粘接，并且在与电解质连通的另一侧提供腐蚀抑制。类似的湿密封件可以由单一的金属粉末形成，其表面处理邻近电解质的表面以提供对电解质腐蚀的抵抗力。

37. 发明授权

US5614308A Macrocomposite bodies 失效
标题翻译：大复合体
公开(公告)号：US5614308A
公开(公告)日：1997-03-25
申请号：US352983
申请日：1994-12-09
申请人： Terry D. Claar
发明人： Terry D. Claar
IPC分类号： C04B35/58 , C04B35/65 , C04B37/00 , C04B41/50 , C04B41/51 , B32B15/04
CPC分类号： C04B41/51 , C04B35/5607 , C04B35/5805 , C04B35/58071 , C04B35/58078 , C04B35/652 , C04B35/653 , C04B37/001 , C04B41/5053 , C04B2237/36 , C04B2237/363 , C04B2237/403 , Y10T428/249969 , Y10T428/24997 , Y10T428/24999 , Y10T428/252 , Y10T428/256 , Y10T428/257
摘要： This invention relates generally to a novel method of manufacturing a composite body and to novel products made thereby. More particularly, the invention relates to a method of producing a self-supporting composite body comprising one or more boron-containing compounds, e.g., a boride or a boride and carbide, by reactive infiltration of molten parent metal into a bed or mass containing boron carbide, and, optionally, one or more inert fillers and permitting residual or excess parent metal to remain bonded to the formed self-supporting composite body. The residual or excess metal is used to form a bond between the formed composite body and another body (e.g., a metal body, a ceramic body, or another composite body). In addition, this invention related to alternative methods of disposing metal on at least one surface of the above-described composite bodies (such as sputtering, CVD, etc.) to permit the composite bodies to be bonded to another body.
摘要翻译：本发明一般涉及一种制造复合体的新方法及其制成的新颖产品。更具体地说，本发明涉及通过将熔融母体金属反应性浸入含硼的床或物质中来生产包含一种或多种含硼化合物（例如硼化物或硼化物和碳化物）的自支撑复合体的方法碳化物和任选的一种或多种惰性填料，并允许残留或过量的母体金属保持结合到形成的自支撑复合体上。剩余或多余的金属用于在所形成的复合体与另一体（例如，金属体，陶瓷体或其它复合体）之间形成结合。此外，本发明涉及在上述复合体的至少一个表面（例如溅射，CVD等）上设置金属以允许复合体结合到另一个主体的替代方法。

38. 发明授权

US5439744A Composite bodies and methods for making same 失效
标题翻译：复合体及其制作方法
公开(公告)号：US5439744A
公开(公告)日：1995-08-08
申请号：US979853
申请日：1993-02-25
申请人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
发明人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
IPC分类号： C04B35/65 , C04B41/50 , C23C10/08 , C04B35/58
CPC分类号： C04B41/5053 , C04B35/652 , C23C10/08 , Y10T428/30 , Y10T428/31678
摘要： This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal (e.g., a parent metal vapor) is induced to react with at least one solid oxidant-containing material to result in the directed growth of a reaction product which is formed from a reaction between the parent metal and the solid oxidant-containing material. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.
摘要翻译： PCT No.PCT / US91 / 04762 Sec。 371日期：1993年2月25日 102（e）日期1993年2月25日PCT 1991年6月25日提交PCT本发明一般涉及一种用于生产自支撑体的新型定向金属氧化方法。在本发明的一些更具体的方面中，诱导母体金属（例如母体金属蒸汽）与至少一种含固体氧化剂的材料反应，导致反应产物的直接生长，所述反应产物由母体金属和含固体氧化剂的材料之间的反应。本发明的方法可以用于形成具有基本上均匀的组合物，分级组合物和大复合体的本体。

39. 发明授权

US5277933A Method for forming a self-supporting body using vapor-phase parent metals and solid oxidants 失效
标题翻译：使用气相母体金属和固体氧化剂形成自支撑体的方法
公开(公告)号：US5277933A
公开(公告)日：1994-01-11
申请号：US812775
申请日：1991-12-23
申请人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
发明人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
IPC分类号： C04B35/65 , C04B41/50 , C04B41/87 , C04B41/88 , C23C10/06 , C23C10/08 , C23C10/16 , C23C16/00
CPC分类号： C04B41/87 , C04B35/652 , C04B41/5053 , C04B41/5057 , C23C10/08 , C23C10/16
摘要： This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal (e.g., a parent metal vapor) is induced to react with at least one solid oxidant-containing material to result in the directed growth of a reaction product which is formed from a reaction between the parent metal and the solid oxidant-containing material. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.
摘要翻译：本发明一般涉及用于生产自支撑体的新颖的定向金属氧化方法。在本发明的一些更具体的方面中，诱导母体金属（例如母体金属蒸汽）与至少一种含固体氧化剂的材料反应，导致反应产物的直接生长，所述反应产物由母体金属和含固体氧化剂的材料之间的反应。本发明的方法可以用于形成具有基本上均匀的组合物，分级组合物和大复合体的本体。

40. 发明授权

US5250324A Method for forming a surface coating using powdered solid oxidants and parent metals 失效
标题翻译：使用粉状固体氧化剂和母体金属形成表面涂层的方法
公开(公告)号：US5250324A
公开(公告)日：1993-10-05
申请号：US881277
申请日：1992-05-11
申请人： Terry D. Claar
发明人： Terry D. Claar
IPC分类号： C04B41/50 , C04B41/87 , C23C10/30 , C23C24/08 , B05D3/02 , C04B35/58
CPC分类号： C04B41/87 , C04B41/5053 , C23C10/30 , C23C24/08
摘要： This invention relates generally to a reaction which occurs on the surface of a substrate body. Particularly, at least one solid oxidant is contacted with at least one parent metal to result in a reaction therebetween and the formation of a reaction product on the surface of a substrate body.
摘要翻译：本发明一般涉及发生在基体表面上的反应。特别地，至少一种固体氧化剂与至少一种母体金属接触，导致其间的反应和在基体表面上形成反应产物。

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