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31. 发明授权

US5616443A Substrate having a mutable colored composition thereon 失效
标题翻译：底物上具有可变色的组合物
公开(公告)号：US5616443A
公开(公告)日：1997-04-01
申请号：US456784
申请日：1995-06-01
申请人： Ronald S. Nohr , John G. MacDonald , Vincent D. McGinniss , Robert S. Whitmore, Jr.
发明人： Ronald S. Nohr , John G. MacDonald , Vincent D. McGinniss , Robert S. Whitmore, Jr.
IPC分类号： B41M3/14 , B41M5/26 , B41M5/28 , B41M5/40 , B41M5/46 , B43M11/08 , C07C65/38 , C07C69/76 , C08B37/00 , C08B37/16 , C09B67/42 , C09D11/00 , C09D11/16 , G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097 , G06K1/12 , G06K19/06 , G09C5/00
CPC分类号： B41M5/46 , B41M3/14 , B41M5/26 , B41M5/284 , B43M11/08 , C07C65/38 , C07C69/76 , C08B37/0012 , C08B37/0015 , C09B67/0071 , C09D11/17 , C09D11/30 , C09D11/36 , G03G9/08 , G03G9/0825 , G03G9/08777 , G03G9/0906 , G03G9/0926 , G03G9/09708 , G03G9/09733 , G03G9/09741 , G03G9/0975 , G03G9/09758 , G03G9/09775 , G03G9/09791 , G06K1/121 , G06K19/06046 , Y10S428/916 , Y10T428/31504 , Y10T428/31678
摘要： A solid colored composition which includes a colorant and an ultraviolet radiation transorber. The colorant, in the presence of the ultraviolet radiation transorber, is adapted, upon exposure of the transorber to ultraviolet radiation, to be mutable. The ultraviolet radiation transorber is adapted to absorb ultravioiet radiation and interact with the colorant to effect the irreversible mutation of the colorant. By way of example, the solid colored composition can be a toner adapted to be utilized in an electrophotographic process. The toner includes the colorant and ultraviolet radiation transorber as just described, and a carrier. The carrier can be a polymer, and the toner may contain a charge carrier. The ultraviolet radiation in general will have wavelengths of from about 100 to about 375 nanometers. Especially useful incoherent pulsed ultraviolet radiation is produced by a dielectric barrier discharge excimer lamp.
摘要翻译：包括着色剂和紫外线辐射传感器的固色组合物。在存在紫外线辐射体的情况下，着色剂在辐射器暴露于紫外线辐射时适应为可变的。紫外线辐射传感器适于吸收紫外线辐射并与着色剂相互作用以实现着色剂的不可逆突变。作为实例，固体着色组合物可以是适于在电子照相方法中使用的调色剂。调色剂包括如上所述的着色剂和紫外线辐射传感器，以及载体。载体可以是聚合物，并且调色剂可以含有电荷载体。紫外线辐射通常具有约100至约375纳米的波长。特别有用的非相干脉冲紫外线辐射是由介电阻挡放电准分子灯产生的。

32. 发明授权

US5540984A Coated polymeric fabric having durable wettability and reduced adsorption of protein 失效
公开(公告)号：US5540984A
公开(公告)日：1996-07-30
申请号：US407727
申请日：1995-03-20
申请人： Roger B. Quincy, III , Ronald S. Nohr , John G. MacDonald , Elizabeth D. Gadsby , Dennis S. Everhart
发明人： Roger B. Quincy, III , Ronald S. Nohr , John G. MacDonald , Elizabeth D. Gadsby , Dennis S. Everhart
IPC分类号： A61F13/511 , A61F5/44 , A61F13/15 , A61F13/20 , A61F13/49 , A61L15/48 , B32B27/32 , C09D183/12 , D06M15/643 , D06M15/647 , B32B27/00 , B32B9/00
CPC分类号： D06M15/647 , A61L15/48 , C09D183/12 , Y10S428/903 , Y10T442/2484 , Y10T442/2492 , Y10T442/2549 , Y10T442/291
摘要： A method of durably rendering a polymeric fabric, e.g., a polyolefin fabric, wettable and resistant to protein adsorption. The method involves providing a polymeric fabric having a surface, applying to the surface of the polymeric fabric a composition which includes water and a surfactant adapted to durably render the polymeric fabric resistant to protein adsorption, and drying the polymeric fabric. The surfactant has a solubility in water at 20.degree. C. no greater than about 5 percent by weight, based on the weight of the water, and is present on the polymeric fabric in an amount of the surfactant sufficient to reduce the adsorption of the protein by the fabric. The coated fabric not only exhibits durable reduced adsorption of protein but also has durable wettability by aqueous liquids. The coated fabric is especially suited for incorporation in such disposable absorbent articles as diapers, feminine care products, such as sanitary napkins and tampons, incontinent care products, training pants, wipes, and the like.

33. 发明授权

US5494855A Thermoplastic compositions and nonwoven webs prepared therefrom 失效
公开(公告)号：US5494855A
公开(公告)日：1996-02-27
申请号：US346664
申请日：1994-11-30
申请人： Ronald S. Nohr , John G. MacDonald
发明人： Ronald S. Nohr , John G. MacDonald
IPC分类号： D01F6/46 , D04H1/42 , B32B27/14
CPC分类号： D01F6/46 , D04H1/4291 , Y10T428/24826 , Y10T442/68 , Y10T442/681 , Y10T442/696
摘要： A melt-extrudable thermoplastic composition is provided which includes a thermoplastic polyolefin and an additive system made up of a first component and a second component, in which (A) the first component is a defined polysiloxane polyether having a molecular weight of from about 350 to about 18,000 and which is present in an amount of from about 0.1 to about 3 percent by weight, based on the amount of thermoplastic polyolefin; and (B) the second component is a hydrophobic fumed silica, in which the weight ratio of the first component to the second component is in the range of from about 20 to about 300. Such composition yields, upon melt-extrusion, either nonwoven webs having significantly increased tensile strengths when compared to nonwoven webs prepared from the thermoplastic polyolefin alone, or wettable webs requiring an amount of first component which is significantly less than that required in the absence of the second component.

34. 发明授权

US5455108A Coated polymeric fabric having reduced adsorption of protein 失效
标题翻译：涂层的聚合物织物具有减少的蛋白质吸附
公开(公告)号：US5455108A
公开(公告)日：1995-10-03
申请号：US175654
申请日：1993-12-30
申请人： Roger B. Quincy, III , Ronald S. Nohr , John G. MacDonald , Dennis S. Everhart
发明人： Roger B. Quincy, III , Ronald S. Nohr , John G. MacDonald , Dennis S. Everhart
IPC分类号： A61L15/48 , D06M10/02 , D06M10/10 , D06M15/647 , D06N3/00 , D06N3/04 , D06N3/12 , B05D3/06 , B05D5/08 , B32B33/00
CPC分类号： D06M15/647 , A61L15/48 , D06M10/025 , D06M10/10 , D06N3/0084 , D06N3/045 , D06N3/128 , D06M2101/18 , Y10T428/31663 , Y10T442/2549 , Y10T442/291
摘要： A method of reducing the adsorption of protein by a polymeric fabric; e.g., a polyolefin fabric, which involves providing a polymeric fabric having a surface, applying to the surface of the polymeric fabric a composition including water and a surfactant adapted to reduce the adsorption of protein by the polymeric fabric, and treating the fabric to which a surfactant has been applied by air corona discharge at a corona energy density of from about 10 to about 280 kilojoules per square meter. The surfactant is present on the fabric in an amount sufficient to reduce the adsorption of protein by the fabric. The coated fabric is especially suited for incorporation in such disposable absorbent articles as diapers; feminine care products, such as sanitary napkins and tampons; incontinent care products; training pants; and wipes.
摘要翻译：降低聚合物织物对蛋白质吸附的方法; 例如，聚烯烃织物，其涉及提供具有表面的聚合物织物，向聚合物织物的表面施加包含水和表面活性剂的组合物，该组合物适于减少聚合物织物对蛋白质的吸附，以及将织物通过空气电晕放电以约10至约280千焦/平方米的电晕能量密度施加表面活性剂。表面活性剂以足以减少织物对蛋白质吸附的量存在于织物上。涂布的织物特别适合于并入诸如尿布的一次性吸收制品中; 女性护理产品，如卫生巾和卫生棉条; 失禁护理产品; 训练裤子和擦拭。

35. 发明授权

US5336707A Surface segregation through the use of a block copolymer 失效
标题翻译：通过使用嵌段共聚物进行表面偏析
公开(公告)号：US5336707A
公开(公告)日：1994-08-09
申请号：US972678
申请日：1992-11-06
申请人： Ronald S. Nohr , John G. MacDonald
发明人： Ronald S. Nohr , John G. MacDonald
IPC分类号： C08L53/00 , A61L15/24 , C08K5/5419 , D04H1/54 , C08K5/54 , C08L83/12
CPC分类号： D04H1/54 , A61L15/24 , C08K5/5419
摘要： A surface-segregatable, melt-extrudable thermoplastic composition is provided which includes (A) a thermoplastic polypropylene-polyethylene block copolymer in which the polyethylene blocks constitute from about 1 to about 10 percent by weight of the copolymer and (B) a defined trisiloxane polyether additive having a molecular weight of from about 350 to about 1,400, which additive is present in an amount of from about 0.1 to about 5 percent by weight, based on the amount of thermoplastic block copolymer. The use of the block copolymer unexpectedly permits the use of significantly reduced amounts of additive while still providing nonwoven webs which are immediately wettable and which do not become significantly less wettable over time.
摘要翻译：提供了表面可分离的可熔融挤出的热塑性组合物，其包括（A）热塑性聚丙烯 - 聚乙烯嵌段共聚物，其中聚乙烯嵌段占共聚物的约1至约10重量％，（B）限定的三硅氧烷聚醚基于热塑性嵌段共聚物的量，分子量为约350至约1400的添加剂，该添加剂的存在量为约0.1至约5重量％。嵌段共聚物的使用意外地允许使用显着减少量的添加剂，同时仍然提供可立即润湿的非织造纤维网，并且随着时间的推移不会变得显着更少的润湿性。

36. 发明授权

US5283023A Method of imparting delayed wettability to a nonwoven web 失效
标题翻译：赋予非织造纤维网延迟润湿性的方法
公开(公告)号：US5283023A
公开(公告)日：1994-02-01
申请号：US818030
申请日：1992-01-03
申请人： Ronald S. Nohr , John G. MacDonald
发明人： Ronald S. Nohr , John G. MacDonald
IPC分类号： D01F1/10 , D01F6/04 , D01F6/06 , D04H1/42
CPC分类号： D01F1/10 , D01F6/04 , D01F6/06 , D04H1/4291
摘要： A method of forming a nonwoven web having delayed wettability, in that the web is not wettable by water upon its formation but becomes wettable within from about three hours to about 30 days thereafter without any post-formation treatment, which method involves the steps of (1) melting a mixture consisting of a thermoplastic polyolefin, and additive, and a retardant coadditive; (2) forming fibers by extruding the resulting melt through under defined conditions of shear and throughput; (3) drawing the fibers; and (4) collecting the fibers on a moving foraminous surface as a web of entangled fibers. The additive is a defined polysiloxane polyether having a molecular weight of from about 700 to about 1,300 and a polydispersity of from about 1.3 to about 3.0. The additive is present in an amount of from about 1.8 to about 3.0 percent by weight, based on the amount of thermoplastic polyolefin. The retardant coadditive is a high surface area particulate inorganic or organic material which is insoluble in the polymer at both ambient and melt-extrusion temperatures, is present in an amount of from about 0.1 to about 1 percent, based on the weight of the thermoplastic composition, has a surface area of from about 50 to about 500 m.sup.2, and is capable of being at least partially coated by the additive.
摘要翻译：一种形成具有延迟润湿性的非织造纤维网的方法，其特征在于，所述网状物在其形成时不被水润湿，但在其后约3小时至约30天内可润湿，而不进行任何后期处理，该方法包括以下步骤： 1）熔化由热塑性聚烯烃和添加剂组成的混合物和阻燃剂共添加剂; （2）通过在限定的剪切和生产条件下挤出所得熔体来形成纤维; （3）拉丝纤维; 和（4）将纤维收集在移动的多孔表面上作为缠结纤维网。添加剂是分子量为约700至约1,300且多分散性为约1.3至约3.0的限定的聚硅氧烷聚醚。基于热塑性聚烯烃的量，添加剂的存在量为约1.8至约3.0重量％。阻燃剂共添加剂是在环境温度和熔融挤出温度下不溶于聚合物的高表面积颗粒状无机或有机材料，其含量为基于热塑性组合物重量的约0.1％至约1％具有约50至约500m 2的表面积，并且能够至少部分地被添加剂涂覆。

37. 发明授权

US4923914A Surface-segregatable, melt-extrudable thermoplastic composition 失效
公开(公告)号：US4923914A
公开(公告)日：1990-05-08
申请号：US181359
申请日：1988-04-14
申请人： Ronald S. Nohr , J. Gavin MacDonald
发明人： Ronald S. Nohr , J. Gavin MacDonald
IPC分类号： A61L15/22 , C08J5/18 , C08K5/00 , C08K5/54 , C08K5/5419 , C08L23/02 , C08L83/04 , C08L101/00 , D01F1/10 , D04H1/56
CPC分类号： C08L101/00 , A61L15/225 , C08J5/18 , C08K5/0008 , C08K5/54 , C08K5/5419 , C08L23/02 , C08L83/04 , D01F1/10 , D04H1/56 , C08G77/045 , C08G77/14 , C08G77/18 , C08G77/26
摘要： A surface-segregatable, melt-extrudable thermoplastic composition suitable for processing by melt extrusion to form a fiber or film having a differential, increasing concentration of an additive from the center of the fiber or film to the surface thereof, which differential, increasing concentration imparts to the surface of the fiber or film at least one desired characteristic which otherwise would not be present, which composition includes at least one thermoplastic polymer and at least one defined additive. During formation of the fiber or film, the additive rapidly segregates in a controllable manner toward the newly-formed surface of the fiber or film, thereby resulting in a controllable differential concentration of the polymeric material, which concentration increases with increasing distance from the center of the fiber or film to its surface. The weight ratio of the polymer to the additive is in the range of from about 1 to about 1,000. The preferred polymer is a polyolefin such as polyethylene and polypropylene.The thermoplastic composition is useful in the preparation of fibers or films which have at least one surface characteristic which is different from that of the polymer component of the thermoplastic composition. The thermoplastic composition is particularly useful in the formation of nonwoven webs which are used in the construction of such disposable absorbent products as diapers, feminine care products, incontinence products, and the like.

38. 发明授权

US4920168A Stabilized siloxane-containing melt-extrudable thermoplastic compositions 失效
标题翻译：稳定的含硅氧烷的可熔融挤出的热塑性组合物
公开(公告)号：US4920168A
公开(公告)日：1990-04-24
申请号：US181352
申请日：1988-04-14
申请人： Ronald S. Nohr , J. Gavin MacDonald
发明人： Ronald S. Nohr , J. Gavin MacDonald
IPC分类号： A61L15/22 , C08K5/00 , C08K5/5419 , C08L23/02 , C08L101/00
CPC分类号： A61L15/225 , C08K5/0008 , C08K5/5419 , C08L101/00 , C08L23/02
摘要： A stabilized surface-segregatable, melt-extrudable thermoplastic composition suitable for processing by melt extrusion to form a fiber or film having a differential, increasing concentration of a siloxane-containing primary additive from the center of the fiber or film to the surface thereof, which differential, increasing concentration imparts hydrophilicity to the surface of the fiber or film, which composition includes at least one thermoplastic polymer, at least one siloxane-containing primary additive, and at least one siloxane-containing stabilizing additive. During formation of the fiber or film, the primary additive rapidly segregates in a controllable manner toward the newly-formed surface of the fiber or film, thereby resulting in a controllable differential concentration of the primary additive, which concentration increases with increasing distance from the center of the fiber or film to its surface. The weight ratio of the polymer to the additive is in the range of from about 1 to about 1,000. The preferred polymer is a polyolefin such as polyethylene and polypropylene. The stabilizing additive prevents or minimizes degradation of additive and/or polymer during the melt-extrusion process.The stabilized thermoplastic composition is useful in the preparation of fibers or films which have hydrophilic surfaces. The thermoplastic composition is particularly useful in the formation of nonwoven webs which are used in the construction of such disposable absorbent products as diapers, feminine care products, incontinence products, and the like.
摘要翻译：一种稳定的表面可分离的可熔融挤出的热塑性组合物，适用于通过熔体挤出加工以形成纤维或薄膜，所述纤维或薄膜从纤维或薄膜的中心到其表面具有不同的，含硅氧烷的初级添加剂的浓度增加，不同的增加浓度赋予纤维或薄膜表面亲水性，该组合物包括至少一种热塑性聚合物，至少一种含硅氧烷的初级添加剂和至少一种含硅氧烷的稳定添加剂。在形成纤维或薄膜期间，主要添加剂以可控的方式快速地偏离到新形成的纤维或薄膜的表面，从而导致主要添加剂的可控差分浓度，该浓度随着与中心距离的增加而增加的纤维或薄膜到其表面。聚合物与添加剂的重量比在约1至约1,000的范围内。优选的聚合物是聚烯烃，例如聚乙烯和聚丙烯。稳定添加剂防止或最小化熔融挤出过程中添加剂和/或聚合物的降解。稳定的热塑性组合物可用于制备具有亲水表面的纤维或薄膜。热塑性组合物特别可用于形成用于构造诸如尿布，女性护理产品，失禁产品等的一次性吸收产品的非织造纤维网。

39. 发明授权

US06399769B1 Method of making sulfanatophenyl substituted porphines 失效
标题翻译：制备磺胺苯基取代的卟吩的方法
公开(公告)号：US06399769B1
公开(公告)日：2002-06-04
申请号：US09210229
申请日：1998-12-11
申请人： Ronald S. Nohr , J. Gavin MacDonald
发明人： Ronald S. Nohr , J. Gavin MacDonald
IPC分类号： C07D48722
CPC分类号： C09B47/00 , C09B67/0033
摘要： The present invention relates to improved methods of making Cu-meso-tetra-(4-sulfanatophenyl)-porphine (designated p-CuTPPS4). The improved processes allow the production of p-CuTPPS4 at lower cost and higher yields compared to conventional methods of making p-CuTPPS4. The present invention further relates to methods of making Cu-meso-tetra-(2-sulfanatophenyl)-porphine (designated o-CuTPPS4) and the use of o-CuTPPS4 as a colorant stabilizer for a variety of colorants, especially magenta colorants. The o-CuTPPS4, according to the present invention, provides a more stable and more “blue” colorant stabilizer compared to known colorant stabilizers, such as Cu-meso-tetra-(p-phenylcarboxylic acid)-porphine.
摘要翻译：本发明涉及制备Cu-内消旋 - 四 - （4-磺基苯基） - 卟吩（称为p-CuTPPS4）的改进方法。与常规的制备p-CuTPPS4的方法相比，改进的方法允许以更低的成本和更高的产率生产p-CuTPPS4。本发明还涉及制备Cu-内消旋 - 四 - （2-磺基苯基） - 卟吩（称为o-CuTPPS4）的方法，以及使用o-CuTPPS4作为各种着色剂，特别是品红色着色剂的着色剂稳定剂。根据本发明的o-CuTPPS4与已知的着色剂稳定剂例如Cu-内消旋 - 四 - （对苯基羧酸） - 卟吩相比，提供了更稳定和更“蓝色”的着色剂稳定剂。

40. 发明授权

US5641822A Surface-segregatable compositions and nonwoven webs prepared therefrom 失效
公开(公告)号：US5641822A
公开(公告)日：1997-06-24
申请号：US422743
申请日：1995-04-14
申请人： Ronald S. Nohr , J. Gavin MacDonald
发明人： Ronald S. Nohr , J. Gavin MacDonald
IPC分类号： C08K5/5419 , D01F1/10 , D01F6/04 , D04H1/42 , D04H1/56 , D04H3/14 , D04H3/16 , C08K5/24 , C08L53/00
CPC分类号： D04H1/56 , C08K5/5419 , D01F1/10 , D01F6/04 , D04H1/4291 , D04H3/14 , D04H3/16
摘要： A surface-segregatable, melt-extrudable thermoplastic composition is provided which includes at least one thermoplastic polyolefin and at least one additive having the general formula, ##STR1## in which: (A) R.sub.1 -R.sub.9 are independently selected monovalent C.sub.1 -C.sub.3 alkyl groups;(B) R.sub.10 is hydrogen or a monovalent C.sub.1 -C.sub.3 alkyl group;(C) m represents an integer of from 1 to about 4;(D) n represents an integer of from 0 to about 3;(E) the sum of m and n is in the range of from 1 to about 4;(F) p represents an integer of from 0 to about 5;(G) x represents an integer of from 1 to about 10;(H) y represents an integer of from 0 to about 5;(I) the ratio of x to y is equal to or greater than 2;(J) the additive has a molecular weight of from about 350 to about 1,400; and(K) the additive is present in an amount of from about 0.5 to about 5 percent by weight, based on the amount of thermoplastic polyolefin.Melt-extrusion of the foregoing composition results in a wettable nonwoven web which remains wettable for at least two years at ambient temperature. A method of making such a wettable nonwoven web also is provided.

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