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31. 发明授权

US4617144A Organoleptic uses of tertiary hydroxyl carboxaldehydes 失效
标题翻译：感官使用叔羟基羧醛
公开(公告)号：US4617144A
公开(公告)日：1986-10-14
申请号：US768807
申请日：1985-08-23
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C45/49 , C07C47/27 , C07C47/36 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/49 , C07C47/27 , C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers solid or liquid anionic, cationic, noninic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基甲醛：其中当m不为0时，线* * * * *和 - - - - - 和/或+ + + + +代表共价碳 - 碳键 ; 并且当m = 0时，线+ + + + + * * * * *和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个完成具有代表碳 - 碳键的线+ + + + + * * * * *和 - - - - 的双环的所需的碳原子。当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z完全是环烷基环部分，其中线* * * *和+ + + +代表碳 - 碳键，并且线 - - - - - 不表示键; 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物固体或液体阴离子，阳离子，无定形或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜等）的香气）。

32. 发明授权

US4608196A Preparing tertiary hydroxyl carboxaldehyde containing perfume compositions 失效
标题翻译：制备含羟基甲醛的香料组合物
公开(公告)号：US4608196A
公开(公告)日：1986-08-26
申请号：US768840
申请日：1985-08-23
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C45/49 , C07C47/27 , C07C47/36 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/49 , C07C47/27 , C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基甲醛：其中当m不为0时，线* * * * *和 - - - - - 和/或+ + + + +代表共价碳 - 碳键 ; 并且当m = 0时，线+ + + + + * * * * *和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个完成具有代表碳 - 碳键的线+ + + + + * * * * *和 - - - - 的双环的所需的碳原子。当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z完全是环烷基环部分，其中线* * * *和+ + + +代表碳 - 碳键，并且线 - - - - - 不表示键; 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物固体或液体阴离子，阳离子，无定形或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜等）的香气）。

33. 发明授权

US4601835A Hydroxyalkoxy norbornyl ethers, process for preparing same and organoleptic uses thereof 失效
标题翻译：羟基烷氧基降冰片基醚，其制备方法和感官用途
公开(公告)号：US4601835A
公开(公告)日：1986-07-22
申请号：US742276
申请日：1985-06-07
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , A61K7/46 , C11D3/50
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described are the hydroxyalkoxy norbornyl ethers or mixtures of same having the structure: ##STR1## wherein one of R.sub.1 or R.sub.2 is methyl and the other of R.sub.1 or R.sub.2 is hydrogen and wherein one of the dashed lines represents a carbon-carbon bond and the other of the dashed lines represents no bond as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of at least one of said hydroxyalkoxy norbornyl ethers.
摘要翻译：描述了具有以下结构的羟基烷氧基降冰片基醚或其混合物：其中R 1或R 2中的一个是甲基，R 1或R 2中的另一个是氢，并且其中一个虚线表示碳 - 碳键，而另一个的虚线表示没有粘合，以及通过向其中加入增加或增加至少一种所述羟基烷氧基降冰片基醚的香气来增强或增强包括香料，古龙水和香料制品在内的可消耗材料的香气的方法。

34. 发明授权

US4556746A 4(p-Cumenyloxy)-3-methyl-1-butanol 失效
标题翻译： 4（对 - 间甲氧基）-3-甲基-1-丁醇
公开(公告)号：US4556746A
公开(公告)日：1985-12-03
申请号：US709915
申请日：1985-03-08
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C43/205
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene; C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture of carbon monoxide and hydrogen by means of an oxo reaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.
摘要翻译：描述了根据通用结构定义的醚甲醇：其中X 1表示选自以下的部分：其中Y 1表示C 4或C 5亚烷基; C4或C5亚链烯基或C4或C5亚炔基; 通过首先使烯丙基醚与一氧化碳和氢气的混合物通过氧代反应反应制备这种醚甲醇的方法，以产生醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。还描述了具有以下结构之一的两个醚甲醛：＆lt; IMAGE＆gt;和＆lt; IMAGE＆gt;用于通过使羰基合成的烯丙基醚与一氧化碳和氢的混合物通过氧代 - 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

35. 发明授权

US4532364A Ether carboxaldehydes 失效
公开(公告)号：US4532364A
公开(公告)日：1985-07-30
申请号：US533915
申请日：1983-09-19
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C45/50 , C07C47/225
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , Y10S514/974
摘要： Described are ether carboxaldehydes defined according to the generic structure: ##STR1## wherein X represents aryl, alkaryl, hydroxyalkyl, alkenyl, cycloalkenyl, lower alkyl or bicycloalkyl; wherein Y represents C.sub.1 -C.sub.3 lower alkylene; wherein Z completes an alkyl substituted C.sub.6 cycloalkyl ring or represents no moiety; wherein R represents hydrogen or methyl; wherein m represents 0 or 1; wherein n represents 0 or 1; wherein p represents 0 or 1 and wherein q represents 0 or 1 with the provisos that when m is 1, Z completes the alkyl substituted or unsubstituted C.sub.6 cycloalkyl ring; that p is 1 when q is 0; and that when p is 0, q is 1, processes for producing same by reacting allyl ethers defined according to the structure: ##STR2## wherein x, y, z, m, n and r are as defined above with a mixture of carbon monoxide and hydrogen by means of an oxo reaction products produced according to said oxo reaction which are mixtures which contain the above-mentioned ether carboxaldehydes as well as methods for augmenting or enhancing the aroma or taste of consumable materials, including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto aroma or taste augmenting or enhancing quantities of the thus produced ether carboxaldehydes or ether carboxaldehyde-containing mixtures.Also described are perfume compositions, colognes, perfumed articles (including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, deodorant compositions, bleaching compositions and perfumed polymers), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles containing the products thus produced.

36. 发明授权

US4510080A Organoleptic uses of hydrocarbyloxy alkanals 失效
标题翻译：烃氧基链烷醇的感官用途
公开(公告)号：US4510080A
公开(公告)日：1985-04-09
申请号：US535930
申请日：1983-09-26
申请人： Richard M. Boden , William L. Schreiber , Futoshi Fujioka , Patrick Chant , Lambert Dekker
发明人： Richard M. Boden , William L. Schreiber , Futoshi Fujioka , Patrick Chant , Lambert Dekker
IPC分类号： C07C45/49 , C07C47/198 , C11B9/00 , C11D17/00
CPC分类号： C11B9/0061 , C07C45/49 , C07C47/198 , C11B9/0015 , C11B9/0046
摘要： Described are hydrocarbyloxy alkanals defined according to the generic structure: ##STR1## wherein R.sub.1 represents one of the moieties: ##STR2## and R.sub.2 represents hydrogen or methyl prepared according to the process of first reacting an allyl alcohol defined according to the structure: ##STR3## with a hydrocarbon or hydrocarbyl halide defined according to the structure: ##STR4## having an electrophilic center wherein R.sub.1 ' is saturated or unsaturated hydrocarbyl and X represents halogen or hydrogen with the provisos that:R.sub.1 ' is saturated hydrocarbyl when X is halogen andR.sub.1 ' is unsaturated hydrocarbyl when X is hydrogen.Also described are organoleptic uses of such hydrocarbyloxy alkanals in the field of perfumery, colognes and perfumed articles, (e.g. perfumed plastics, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or drier-added fabric softener articles).
摘要翻译：描述的是根据通用结构定义的烃氧基链烷烃：其中R 1表示下列部分之一：其中R 1表示氢或甲基，根据以下步骤制备：根据具有根据以下结构定义的烃或烃基卤化物的结构：具有亲电中心的R1'-X，其中R1'是饱和或不饱和烃基，X表示卤素或氢，条件是：R1'饱和当X是氢时R 1是烃基，而当X是氢时，R 1'是不饱和烃基。还描述了在香料，古龙水和加香制品领域（例如加香塑料，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物或干燥剂添加的织物柔软剂制品）领域中的这种烃氧基链烷酸的感官用途。

37. 发明授权

US4491537A Tertiary hydroxyl carboxaldehydes and organoleptic use thereof 失效
标题翻译：叔羟基羧醛及其感官用途
公开(公告)号：US4491537A
公开(公告)日：1985-01-01
申请号：US511965
申请日：1983-07-08
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C45/49 , C07C47/27 , C07C47/36 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/49 , C07C47/27 , C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines* * * * *and-- -- -- -- -- --and/or+ + + + +represent covalent carbon-carbon bonds when m does not=0; and wherein the lines+ + + + +* * * * *and-- -- -- -- -- --do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines+ + + + +* * * * *and-- -- -- -- -- --representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line-- -- -- -- -- --represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines* * * * *and+ + + + +represent carbon-carbon bonds and with the line-- -- -- -- -- --representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR2## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基甲醛：其中当m不为0时，线* * * * *和 - - - - - 和/或+ + + + +代表共价碳 - 碳键 ; 并且当m = 0时，线+ + + + + * * * * *和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个完成具有代表碳 - 碳键的线+ + + + + * * * * *和 - - - - 的双环的所需的碳原子。当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z完全是环烷基环部分，其中线* * * *和+ + + +代表碳 - 碳键，并且线 - - - - - 不表示键; 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜和喜欢）。

38. 发明授权

US4782192A Tricyclic alcohols, ethers and esters, process for preparing same and use thereof in augmenting or enhancing the organoleptic properties of consumable materials 失效
标题翻译：三环醇，醚和酯，其制备方法及其在增加或增强消耗材料的感官特性方面的用途
公开(公告)号：US4782192A
公开(公告)日：1988-11-01
申请号：US391568
申请日：1982-06-24
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C43/18 , C07C45/67 , C07C49/453 , C07C43/02
CPC分类号： C07C49/453 , A23L27/203 , C07C403/02 , C07C45/67 , C07C2101/16
摘要： Described are organoleptic compounds having the generic structure: ##STR1## wherein R.sub.1 represents hydrogen, methyl or acetyl and wherein R.sub.2, R.sub.3, R.sub.4 and R.sub.5 represent the same or different hydrogen, methyl or ethyl.
摘要翻译：描述了具有以下通用结构的感官化合物：其中R 1表示氢，甲基或乙酰基，并且其中R 2，R 3，R 4和R 5表示相同或不同的氢，甲基或乙基。

39. 发明授权

US4439354A Tricyclic alcohols, ethers and esters, process for preparing same and use thereof in augmenting or enhancing the organoleptic properites of consumable materials 失效
标题翻译：三环醇，醚和酯，其制备方法及其在增强或增强消耗材料感官特性中的用途
公开(公告)号：US4439354A
公开(公告)日：1984-03-27
申请号：US311291
申请日：1981-10-13
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C31/137 , C07C43/18 , C07C45/00 , C07C45/67 , C07C49/453
CPC分类号： C07C49/453 , A23L27/203 , C07C403/02 , C07C45/00 , C07C45/67 , C07C2101/16
摘要： Described are compounds having the generic structure: ##STR1## wherein R.sub.1 represents hydrogen, methyl or acetyl and wherein R.sub.2, R.sub.3, R.sub.4 and R.sub.5 represent the same or different hydrogen, methyl or ethyl; a process for preparing same using compounds designed according to the generic structure: ##STR2## and organoleptic uses thereof in perfumes, colognes and perfumed articles.
摘要翻译：描述了具有以下通用结构的化合物：其中R 1表示氢，甲基或乙酰基，并且其中R 2，R 3，R 4和R 5表示相同或不同的氢，甲基或乙基; 使用根据通用结构设计的化合物的方法制备方法：＆lt; IMAGE＆gt;和其在香水，古龙水和香料制品中的感官用途。

40. 发明授权

US4411830A Bridged tricyclic alcohol, process for preparing same and perfumery use thereof 失效
标题翻译：桥接三环醇，其制备方法和香料用途
公开(公告)号：US4411830A
公开(公告)日：1983-10-25
申请号：US396258
申请日：1982-07-08
申请人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
发明人： Kenneth K. Light , Joseph A. McGhie , Futoshi Fujioka , Takao Yoshida
IPC分类号： A23L27/20 , C07C45/67 , C07C49/453 , C11B9/00 , A61K7/46
CPC分类号： C07C49/453 , A23L27/203 , C07C45/67
摘要： Described are the compounds covered by the generic structure: ##STR1## wherein "R" represents hydrogen or lithium. The compound having the structure: ##STR2## is useful in augmenting or enhancing the patchouli aroma of a perfume, cologne or perfumed article, such as a solid or liquid anionic, cationic, nonionic or zwitterionic detergent. The compound having the structure: ##STR3## is an intermediate for preparing the compound having the structure: ##STR4## according to the process defined by the reaction: ##STR5## .
摘要翻译：描述了通用结构覆盖的化合物：其中“R”表示氢或锂。具有以下结构的化合物：可用于增强或增强香料，古龙水或香水制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂的广藿香香气。具有以下结构的化合物：是根据由反应定义的方法制备具有以下结构的化合物的中间体：。

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