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31. 发明授权

US4330665A Process for the preparation of aromatic polycarbonates 失效
标题翻译：制备芳族聚碳酸酯的方法
公开(公告)号：US4330665A
公开(公告)日：1982-05-18
申请号：US256227
申请日：1981-04-21
申请人： Heinrich Krimm , Hans-Josef Buysch , Hans Rudolph
发明人： Heinrich Krimm , Hans-Josef Buysch , Hans Rudolph
IPC分类号： C08G63/00 , C08G64/20 , C08G64/30 , C08G63/62
CPC分类号： C08G64/307
摘要： The invention is directed to a process for the preparation of polycarbonates of Mw 20,000 to 180,000 by transesterification of diphenols and carbonic acid dialkyl esters in the presence of organo-tin-IV compounds and a monophenol.
摘要翻译：本发明涉及通过在有机锡 - Ⅳ-IV化合物和单酚存在下二元酚和碳酸二烷基酯的酯交换制备Mw为20,000至180,000的聚碳酸酯的方法。

32. 发明授权

US4054597A Thiodiglycol polycarbonates 失效
标题翻译：硫二甘醇聚碳酸酯
公开(公告)号：US4054597A
公开(公告)日：1977-10-18
申请号：US687437
申请日：1976-05-17
申请人： Heinrich Krimm , Hans-Josef Buysch , Hermann Schnell
发明人： Heinrich Krimm , Hans-Josef Buysch , Hermann Schnell
IPC分类号： C08G18/46 , C08G64/02 , C07C149/14 , C08G63/62
CPC分类号： C08G64/025 , C08G18/4676
摘要： The present invention relates to an interfacial process for the production of polycarbonates having terminal, aliphatically bonded hydroxyl groups by reacting predominantly dihydric alcohols with phosgene or chlorocarbonic acid esters of predominantly dihydric alcohols and/or phenols using alkali liquors as HCl-binding agents and in the presence of inert solvents, the process according to the invention being distinguished by the fact that concentrated, aqueous alkali liquors are used as the HCl-binding agents and thiodiglycol, optionally mixed with additional monohydric and polyhydric alcohols, is used as the dihydric alcohol. The present invention further relates to the new polycarbonates produced according to the novel process and to the use of these new polycarbonates for the production of polyurethane plastics.
摘要翻译：本发明涉及通过使用碱金属作为HCl结合剂，主要使二元醇与主要为二元醇和/或酚的光气或氯代碳酸酯主要反应的具有末端脂族键合羟基的聚碳酸酯的界面方法，惰性溶剂的存在，根据本发明的方法的区别在于使用浓缩的碱水溶液作为HCl结合剂，并且任选与另外的一元醇和多元醇混合的硫二甘醇用作二元醇。本发明还涉及根据新方法生产的新的聚碳酸酯以及这些新的聚碳酸酯用于生产聚氨酯塑料的用途。

33. 发明授权

US3979462A Condensation resins of phenols and .alpha.,.alpha.'-dihydroxy-diisopropyl benzenes 失效
标题翻译：苯酚的缩合树脂和{60，{60 {40-二羟基 - 二异丙基苯
公开(公告)号：US3979462A
公开(公告)日：1976-09-07
申请号：US636921
申请日：1975-12-02
申请人： Heinrich Krimm , Hans-Josef Buysch , Dieter Freitag
发明人： Heinrich Krimm , Hans-Josef Buysch , Dieter Freitag
IPC分类号： C07C37/16 , C08G8/12 , C08G61/02 , C07C39/12
CPC分类号： C08G61/02 , C07C37/16 , C08G8/12
摘要： A process for the production of light colored condensation resins, wherein phenols are reacted with .alpha.,.alpha.'-dihydroxy-diisopropyl benzenes in the presence of acids of phosphorus at temperatures of between 70.degree. and 270.degree.C.
摘要翻译：一种生产浅色缩合树脂的方法，其中在70℃至270℃的温度下，在磷酸存在下，苯酚与α，α'-二羟基 - 二异丙基苯反应。

34. 发明授权

US06350920B1 Method for preparing polyether polyols 失效
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US06350920B1
公开(公告)日：2002-02-26
申请号：US09485507
申请日：2000-03-20
申请人： Hans-Josef Buysch , Manfred Dietrich , Pramod Gupta , Pieter Ooms
发明人： Hans-Josef Buysch , Manfred Dietrich , Pramod Gupta , Pieter Ooms
IPC分类号： C07C4311
CPC分类号： B01J31/0202 , B01J31/068 , C08G65/2648 , C08G65/2651 , C08G65/30
摘要： Polyether polyols can be prepared by reacting polyols with epoxides in the presence of basic catalysts, by treating the polyether polyols containing the basic catalysts with OH-functional solid compounds of metals of groups III to VIII of the periodic system of the elements (Mendeleyev), the compounds being insoluble in the polyether polyols and having BET surface areas of from 10 to 1000 m2/g, isolating the solid inorganic compounds laden with the basic catalysts from the polyether polyol and using them in the reaction of polyols with epoxides, or bringing the isolated inorganic compounds laden with the basic catalysts into contact with the polyols that are to be used in the reaction with epoxides, separating those polyols from the inorganic compounds and delivering them to the reaction with epoxides.
摘要翻译：聚醚多元醇可以通过在碱性催化剂的存在下使多元醇与环氧化物反应来制备，通过用含有元素（Mendeleyev）的周期体系的III-VIII族金属的OH-官能固体化合物处理含有碱性催化剂的聚醚多元醇，所述化合物不溶于所述聚醚多元醇并具有10至1000m 2 / g的BET表面积，从所述聚醚多元醇中分离含有碱性催化剂的固体无机化合物，并将其用于多元醇与环氧化物的反应，或将分离的无机化合物与碱性催化剂接触，与用于与环氧化物的反应中使用的多元醇接触，将这些多元醇与无机化合物分离并将其输送到与环氧化物反应。

35. 发明授权

US06211417B1 Process for preparing bis-(4-hydroxyaryl) alkanes 失效
标题翻译：制备双（4-羟基芳基）烷烃的方法
公开(公告)号：US06211417B1
公开(公告)日：2001-04-03
申请号：US09341506
申请日：1999-07-12
申请人： Gerd Fengler , Hans-Josef Buysch , Frieder Heydenreich , Rob Eek , Gerhard Fennhoff
发明人： Gerd Fengler , Hans-Josef Buysch , Frieder Heydenreich , Rob Eek , Gerhard Fennhoff
IPC分类号： C07C3916
CPC分类号： C07C37/20 , C07C39/16
摘要： The present invention relates to a process for the production of bis-(4-hydroxyaryl)-alkanes by a heterogeneously catalyzed reaction of aromatic hydroxy compounds with ketones in at least two reactors connected in series, which, as the reaction progresses, are operated at higher temperatures, wherein the total quantity of ketone is divided between the individual reactors in such a manner that the higher is the temperature of the particular reactor, the smaller is the proportion per reactor, the highest possible reactor loading is maintained and the temperatures and temperature gradients are kept as low as possible.
摘要翻译：本发明涉及通过芳族羟基化合物与至少两个串联连接的反应器中的酮的不均匀催化反应生产双 - （4-羟基芳基） - 烷烃的方法，其随着反应进行而在较高的温度，其中酮的总量在单个反应器之间分开，使得特定反应器的温度越高，每个反应器的比例越小，保持最高可能的反应器负载和温度和温度梯度保持尽可能低。

36. 再颁专利

USRE36432E Process for the purification of polycarbonate and polyester carbonate solutions 失效
标题翻译：聚碳酸酯和聚酯碳酸酯溶液的净化方法
公开(公告)号：USRE36432E
公开(公告)日：1999-12-07
申请号：US856830
申请日：1997-05-15
申请人： Gerhard Fennhoff , Pieter Ooms , Hans-Josef Buysch , Ralf Pakull
发明人： Gerhard Fennhoff , Pieter Ooms , Hans-Josef Buysch , Ralf Pakull
IPC分类号： C08G63/64 , C08G63/88 , C08G63/90 , C08G64/40 , C08F6/00
CPC分类号： C08G63/90 , C08G64/406
摘要： A process for purifying aromatic carbonate polymers, including polycarbonates and polyestercarbonates, is disclosed. Accordingly, a carbonate polymer is an organic solvent is rendered virtually free of low molecular weight components by agitation with aluminosilicate or by passing through layers of such aluminosilicate. The aluminosilicate is subsequently separated off and the carbonate polymer is isolated in known methods.
摘要翻译：公开了一种净化芳族碳酸酯聚合物，包括聚碳酸酯和聚酯碳酸酯的方法。因此，碳酸酯聚合物是有机溶剂通过用硅铝酸盐搅拌或通过这种硅铝酸盐层而实际上不含低分子量组分。随后分离出硅铝酸盐，并以已知方法分离碳酸酯聚合物。

37. 发明授权

US5965472A Recovery of catalyst systems from diaryl carbonate-containing reaction solutions by suspension crystallization 失效
标题翻译：通过悬浮结晶从含碳酸二芳基酯的反应溶液中回收催化剂体系
公开(公告)号：US5965472A
公开(公告)日：1999-10-12
申请号：US829929
申请日：1997-04-01
申请人： Hans-Josef Buysch , Carsten Hesse , Johann Rechner , Hans-Peter Wirges
发明人： Hans-Josef Buysch , Carsten Hesse , Johann Rechner , Hans-Peter Wirges
IPC分类号： B01D9/02 , B01J38/00 , C07B61/00 , C07C68/00 , C07C68/08 , C07C69/96 , B01J38/52 , B01J20/34 , B01J38/50
CPC分类号： C07C68/08 , C07C68/005
摘要： Catalyst systems with a content of a platinum-group-metal catalyst, a co-catalyst, a quaternary salt and a base for the oxidative carbonylation of aromatic hydroxy compounds to the corresponding diaryl carbonates are according to the invention obtained as a mother liquor by suspension crystallization and can be returned into the carbonylation reaction or worked up to valuable materials. The crystallizate, which consists predominantly of diaryl carbonate and the parent aromatic hydroxy compound, is worked up to pure diaryl carbonate and pure hydroxy compound.
摘要翻译：根据本发明，通过悬浮液作为母液获得具有铂族金属催化剂，助催化剂，季盐和用于将芳族羟基化合物氧化羰基化成相应的碳酸二芳基酯的碱的催化剂体系结晶并可以回到羰基化反应或加工成有价值的材料。主要由碳酸二芳酯和母体芳族羟基化合物组成的结晶物被加工成纯碳酸二芳酯和纯羟基化合物。

38. 发明授权

US5962365A Process for the manufacture of aromatic amines by gas-phase hydrogenation and catalyst useful thereof 失效
标题翻译：通过气相氢化制备芳香胺的方法及其有用的催化剂
公开(公告)号：US5962365A
公开(公告)日：1999-10-05
申请号：US878592
申请日：1997-06-19
申请人： Reinhard Langer , Hans-Josef Buysch , Ursula Pentling
发明人： Reinhard Langer , Hans-Josef Buysch , Ursula Pentling
IPC分类号： B01J21/18 , B01J23/62 , C07B61/00 , C07C209/36 , C07C211/45 , C07C211/46 , C07C211/47 , C07C211/50 , B01J23/00 , B01J23/42 , C07C5/10
CPC分类号： C07C209/36 , B01J23/628
摘要： Aromatic amines are produced by catalytic hydrogenation of nitroaromatic compounds in the gas phase. The catalyst includes palladium and lead on graphite or on a graphite-containing coke support. From 30 to 6000 equivalents of hydrogen for each equivalent of nitro groups are contacted with the catalyst during this process.
摘要翻译：芳族胺通过在气相中的硝基芳族化合物的催化氢化产生。催化剂包括钯和铅在石墨上或含石墨的焦炭载体上。在此过程中，每当量硝基的30至6000当量氢与催化剂接触。

39. 发明授权

US5900501A Process for the continuous production of aryl carbonates 失效
标题翻译：连续生产碳酸芳基酯的方法
公开(公告)号：US5900501A
公开(公告)日：1999-05-04
申请号：US799299
申请日：1997-02-13
申请人： Pieter Ooms , Hans-Josef Buysch , Steffen Kuhling , Gottfried Zaby
发明人： Pieter Ooms , Hans-Josef Buysch , Steffen Kuhling , Gottfried Zaby
IPC分类号： C07C67/54 , C07B61/00 , C07C68/02 , C07C69/96
CPC分类号： C07C68/02
摘要： The present invention relates to a process for the continuous production of carbonates having aromatic ester groups by the reaction of aromatic hydroxy compounds with phosgene in the presence of heterogeneous catalysts, phosgene still present being removed from the stream of waste gas by returning the waste gas to an additional reactor.
摘要翻译：本发明涉及通过芳族羟基化合物与光气在多相催化剂的存在下连续生产具有芳族酯基的碳酸酯的方法，通过将废气返回到废气流中，仍然存在的光气从废气流中除去一个额外的反应器。

40. 发明授权

US5856516A Process for the preparation of carbazole 失效
标题翻译：制备咔唑的方法
公开(公告)号：US5856516A
公开(公告)日：1999-01-05
申请号：US911961
申请日：1997-08-15
申请人： Hans-Josef Buysch , Reinhard Langer , Ulrich Notheis , Alexander Klausener
发明人： Hans-Josef Buysch , Reinhard Langer , Ulrich Notheis , Alexander Klausener
IPC分类号： B01J23/46 , C07B61/00 , C07D209/86
CPC分类号： C07D209/86
摘要： Carbazole can be prepared by dehydrogenation of compounds of the formula ##STR1## or by aminating dehydrogenation of compounds of the formula ##STR2## at 300.degree. to 600.degree. C. in the presence of hydrogen over an iridium catalyst or an iridium-containing catalyst.
摘要翻译：咔唑可以通过式（Ⅰ）化合物（II）（III）化合物的脱氢或通过酰胺化式（IV）化合物（IVa）的脱氢来制备。（VIII）（VII）（VIII）（VIII）（IX）在（IX）中，在氢存在下，在300〜600℃下铱催化剂或含铱催化剂。

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