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31. 发明授权

US5124233A Photoresist compositions 失效
标题翻译：光电组合物
公开(公告)号：US5124233A
公开(公告)日：1992-06-23
申请号：US202765
申请日：1988-06-03
申请人： Kurt Meier , Ewald Losert
发明人： Kurt Meier , Ewald Losert
IPC分类号： C08G59/50 , C08G59/40 , C08G59/70 , G03C1/72 , G03F7/004 , G03F7/038 , G03F7/039 , H05K3/06
CPC分类号： G03F7/004
摘要： Positive-working photoresist compositions containing(a) an epoxide resin which can be hardened by heat,(b) a latent urea or imidazole hardener for the component (a) and(c) an iron-arene complex of the formula (I)[R.sup.1 (Fe.sup.II R.sup.2).sub.n ].sub.m.sup.+n [X].sub.n.sup.-m(I) in which n is 1 or 2, m is 1, 2, 3, 4 or 5, X is a non-nucleophilic anion, R.sup.1 is a .pi.-arene and R.sup.2 is an anion of a .pi.-arene, are described.These compositions are distinguished by good properties towards heat and chemicals and require short exposure times.
摘要翻译：含有（a）可通过加热硬化的环氧树脂的正性光致抗蚀剂组合物，（b）组分（a）和（c）式（I）的铁 - 芳烃络合物的潜在脲或咪唑硬化剂[ R1（FeIIR2）n] m + n [X] nm（I）其中n为1或2，m为1,2,3,4或5，X为非亲核阴离子，R1为伯 - 芳并且描述了R 2是伯 - 芳的阴离子。这些组合物的特征在于对热和化学品具有良好的性能并且需要短的曝光时间。

32. 发明授权

US5082952A Process for the preparation of metallocene complexes 失效
标题翻译：制备金属络合物的方法
公开(公告)号：US5082952A
公开(公告)日：1992-01-21
申请号：US867113
申请日：1986-05-27
申请人： Kurt Meier
发明人： Kurt Meier
IPC分类号： C07F15/02
CPC分类号： C07F15/02
摘要： The invention relates to a process for the preparation of .pi.-arene-iron complexes of the general formula I[R.sup.1 (R.sup.2 Fe.sup.II).sub.a ].sub.b.sup.+a (LQ.sub.m).sup.-b (I)whereina is 1 or 2,b is an integer from 1 to 3,m is an integer corresponding to the valency of L+b,L is a divalent to heptavalent metal or non-metal,Q is a halogen atom,R.sup.1 is a .pi.-arene, an O- or S-heteroarene or a pyrrole or an indole andR.sup.2 is a cyclopentadienyl anion or an indenyl anion.The .pi.-arene-iron complexes of formula I are obtained by ligand exchange at elevated temperatures from .pi.-arene-iron complexes of formula II[R.sup.3 (R.sup.2 Fe.sup.II).sub.a ].sub.b.sup.+a (LQ.sub.m).sub.a.sup.-b (II)wherein R.sup.3 is a condensed .pi.-arene which differs from R.sup.1. The .pi.-arene-iron complexes of formula I are suitable as photoinitiators for curable compositions containing cationically polymerizable organic materials.
摘要翻译：本发明涉及一种制备通式I [R1（R2FeII）a] b + a（LQm）-b（I）的仲 - 铁络合物的方法，其中a为1或2，b为整数 1〜3，m为对应于L + b的化合价的整数，L为二价至七价金属或非金属，Q为卤素原子，R1为仲芳基，O-或S-杂芳环或吡咯或吲哚，R2为环戊二烯阴离子或茚基阴离子。式I的络合铁络合物通过配体交换在通式II的二芳基 - 铁络合物[R3（R2FeII）a] b + a（LQm）ab（II））中通过配体交换获得，其中R3是稠合 pi-arne与R1不同。式I的络合铁络合物适用作含有阳离子聚合有机材料的可固化组合物的光引发剂。

33. 发明授权

US5073438A Process for the preparation of laminates 失效
标题翻译：制备层压板的方法
公开(公告)号：US5073438A
公开(公告)日：1991-12-17
申请号：US572731
申请日：1990-08-23
申请人： Kurt Meier , Theobald Haug , Wolfgang Scharf
发明人： Kurt Meier , Theobald Haug , Wolfgang Scharf
IPC分类号： C08J5/24 , C08G59/68 , H05K1/03
CPC分类号： C08G59/68 , H05K1/0326 , Y10T442/3577 , Y10T442/3585 , Y10T442/3691
摘要： A laminate prepared by combining at least two layers wherein at least one of which is made of a fibrous material, an epoxy resin having on average at least two 1,2-epoxide groups per molecule or a mixture of these epoxy resins and a ferrocene derivative of the formula [R.sup.1 (Fe.sup.II R.sup.2).sub.a ].sup.ab+ ab.[X].sup.-, wherein a and b independently of one another are 1 or 2, R.sup.1 is a .pi.-arene, R.sup.2 is a .pi.-arene or an indenyl- or cyclopentadienyl anion, X.sup..crclbar. is an anion [LQ.sub.m ].sup..crclbar. or an anion of a partly fluorinated or perfluorinated aliphatic or aromatic sulfonic acid, L is P, As or Sb, Q is fluorine or some of the Q substituents may also be hydroxyl groups, and m corresponds to a value which exceeds the valence of L by unity, subjecting the layers to compression molding at such a temperature and pressure that a liquid resin matrix is present at the beginning of this step and an initial fall in the viscosity is produced so that entrained gases can escape from the layers and crosslinking the laminated layers to obtain a rapid rise in viscosity such that the resin which flows out does not bind the compression mold.

34. 发明授权

US5020850A Roof and frame assembly for a motor vehicle and method of forming same 失效
标题翻译：用于机动车辆的车顶和车架组件及其形成方法
公开(公告)号：US5020850A
公开(公告)日：1991-06-04
申请号：US410893
申请日：1989-09-22
申请人： Horst Bienert , August Hirschberger , Bernd Schleicher , Richard Igel , Kurt Meier
发明人： Horst Bienert , August Hirschberger , Bernd Schleicher , Richard Igel , Kurt Meier
IPC分类号： B60J7/057
CPC分类号： B60J7/057 , Y10T74/18808 , Y10T74/18832 , Y10T74/2045
摘要： A sliding type vehicle roof is provided having guide tubes for pressure-resistant drive cables that are positioned, in the zone of contact area between the drive cables and a drive device, in a sheathing part that is formed about the guide tubes and acts as a holding device for the guide tubes. In the sheathing part, there is provided at least one recess to accommodate a drive pinion of the drive device, and a central opening in the base of the recess for accurately locating the drive pinion. Further, the sheathing part functions as a support for the drive device, that is suitably attached to the sheathing part with the aid of screws, and a defined seat can be provided on the sheathing part to receive the top housing part of the drive device. The sheathing part with the drive thereon can be attached to the frame, which can be set into a roof opening of a vehicle roof.
摘要翻译：一种滑动型车顶设置有用于耐压驱动电缆的引导管，该引导管在驱动电缆和驱动装置之间的接触区域中定位在围绕引导管形成的护套部分中，并且用作用于导管的保持装置。在护套部分中，设置有至少一个凹部以容纳驱动装置的驱动小齿轮，以及凹部的基部中的中心开口，用于精确地定位驱动小齿轮。此外，护套部件用作驱动装置的支撑件，借助于螺钉适当地附接到护套部分，并且可以在护套部分上设置限定的座以容纳驱动装置的顶部壳体部分。其上具有驱动器的护套部分可以附接到框架，框架可以设置在车顶的屋顶开口中。

35. 发明授权

US5011755A Photoinitiator mixtures containing a titanocene and a 3-ketocoumarin 失效
标题翻译：含有二茂钛和3-酮香豆素的光引发剂混合物
公开(公告)号：US5011755A
公开(公告)日：1991-04-30
申请号：US473135
申请日：1990-01-30
申请人： Ottmar Rohde , Armin Schaffner , Martin Riediker , Kurt Meier
发明人： Ottmar Rohde , Armin Schaffner , Martin Riediker , Kurt Meier
IPC分类号： C08F2/50 , C08F290/00 , C08F299/02 , C08G73/10 , G03F7/028 , G03F7/029
CPC分类号： G03F7/029 , C08F2/50 , Y10S430/107 , Y10S430/12 , Y10S430/125 , Y10S430/148 , Y10S502/522
摘要： The present invention relates to compositions comprising(a) a titanocene photoinitiator of the formula I ##STR1## (b) a 3-ketocoumarin of the formula II ##STR2## in which both R.sup.1, R.sup.2 and R.sup.3 are as defined in claim 1, R.sup.4 is a radical of the formula V ##STR3## R.sup.5 is C.sub.1 -C.sub.20 alkyl, cycloalkyl having 5-7 ring carbon atoms, phenyl or naphthyl which are unsubstituted or substituted by one to three C.sub.1 -C.sub.6 alkyl groups, C.sub.1 -C.sub.6 alkoxy groups or halogen atoms or by one diphenylamino or C.sub.1 -C.sub.6 dialkylamino group, or is C.sub.7 -C.sub.9 aralkyl, a radical --(CH.dbd.CH).sub.a --C.sub.6 H.sub.5 or a radical of the formula V, a is 1 or 2, preferably 1, and R.sup.10, R.sup.11, R.sup.12, R.sup.13 and R.sup.14 independently of one another are hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 alkoxy, phenyl, tolyl, xylyl or benzyl, and R.sup.11 can additionally also be a group --NR.sup.15 R.sup.16 or --OR.sup.15, wherein R.sup.15 and R.sup.16 independently of one another are hydrogen or C.sub.1 -C.sub.6 alkyl, it also being possible for two or three of the radicals R.sup.10, R.sup.11, R.sup.12 and R.sup.13 together with the ring carbon atoms, to which they are attached, to form a fused ring having 5 or 6 ring atoms or a fused ring system having 5-membered or 6-membered rings. The photoinitiator mixtures can be used in combination with ethylenically unsaturated monomers, preferably with photopolymerizable precursors of thermally stable polymers. These mixtures can be processed especially on substrates having surfaces which are strongly scattering or strongly reflecting, to give relief structures with high resolution.
摘要翻译：本发明涉及组合物，其包含（a）式I的二茂钛光引发剂（I）（b）式II的3-酮香豆素（II），其中R1，R2和R3均为权利要求1中定义的R 4是式V的基团（V）R 5是C 1 -C 20烷基，具有5-7个环碳原子的环烷基，未被取代或被一至三个C 1 -C 6烷基取代的苯基或萘基 C 1 -C 6烷氧基或卤素原子或一个二苯基氨基或C 1 -C 6二烷基氨基，或者是C 7 -C 9芳烷基，基团 - （CH = CH）a -C 6 H 5或式V基团，a是1或2，优选 1和R 10，R 11，R 12，R 13和R 14彼此独立地是氢，C 1 -C 6烷基，C 1 -C 6烷氧基，苯基，甲苯基，二甲苯基或苄基，R 11还可以是基团-NR 15 R 16或-OR 15，其中 R 15和R 16彼此独立地是氢或C 1 -C 6烷基，基团R 10，R 11，R 12和R 13中的两个或三个与环碳原子一起也可以它们相连，形成具有5或6个环原子的稠环或具有5元环或6元环的稠环体系。光引发剂混合物可以与烯属不饱和单体组合使用，优选与热稳定聚合物的可光聚合前体一起使用。这些混合物可以特别在具有强散射或强烈反射的表面的基底上进行加工，以提供高分辨率的浮雕结构。

36. 发明授权

US4868288A Process for preparing metallocene complexes 失效
标题翻译：金属茂配合物的制备方法
公开(公告)号：US4868288A
公开(公告)日：1989-09-19
申请号：US257152
申请日：1988-09-30
申请人： Kurt Meier
发明人： Kurt Meier
IPC分类号： C08F4/00 , C08F2/00 , C08F4/42 , C08F4/60 , C08G59/68 , C08G85/00 , C08L61/00 , G03F7/029
CPC分类号： C08G85/00 , C08L61/00 , G03F7/029
摘要： The invention relates to a process for the preparation of compounds of formula Ia[R.sup.1 FeR.sup.2' ].sup..sym..sub.q [LQ.sub.m ].sup.q.crclbar.(Ia),wherein R.sup.1 is a .pi.-arene, R.sup.2' is an anion of a .pi.-arene, L is a divalent to heptavalent metal or non-metal, Q is a halogen atom, q is an integer from 1 to 3 and m is an integer corresponding to the valency of L+q, said process comprises reacting an uncharged .pi.-complex of the formula IIIa[(R.sup.2').sub.2 Fe] (IIIa)with a .pi.arene R.sup.1 is in the presence of Al and a Lewis-acid followed by treatment with an acid or a salt of an acid of the anion [LQ.sub.m ].sup.q-, the improvement consisting essentially of using TiCl.sub.4 as a Lewis-acid.
摘要翻译：本发明涉及制备式Ia化合物的方法[R1FeR2']（+）q [LQm] q（ - ）（Ia），其中R1是一个仲芳基，R2'是一个π- 芳烃，L是二价至七价金属或非金属，Q是卤素原子，q是1至3的整数，m是对应于L + q的化合价的整数，所述方法包括使不带电的π- 式IIIa [（R 2'）2 Fe]（IIIa）与吡咯烷酮R1的络合物在Al和路易斯酸的存在下，然后用酸或阴离子的酸[LQm]的盐处理， q-，改进主要是使用TiCl 4作为路易斯酸。

37. 发明授权

US4624912A Thermally transferable layers of radiation sensitive epoxy resins used to prepare protective coatings and relief images 失效
标题翻译：用于制备保护性涂层和浮雕图像的耐辐射敏感性环氧树脂层
公开(公告)号：US4624912A
公开(公告)日：1986-11-25
申请号：US698952
申请日：1985-02-06
申请人： Hans Zweifel , Sigrid Bauer , Kurt Meier
发明人： Hans Zweifel , Sigrid Bauer , Kurt Meier
IPC分类号： G03C5/00 , C08G59/68 , C08J3/28 , C08J7/04 , G03C1/00 , G03F7/038 , G03F7/11 , H05K3/00 , G03C11/12 , B44C1/165 , G03C5/16
CPC分类号： C08G59/68 , G03F7/0385 , H05K3/0079
摘要： A process for the production of a protective layer or a relief image on a substrate, wherein a radiation-sensitive layer, consisting of a solid film-forming epoxy resin containing a photoinitiator, which can be activated by radiation, for the polyaddition reaction, is transferred from a support to a substrate, then exposed directly or under a photomask and hardened by the action of heat, after which, if appropriate, the unexposed parts are developed with a solvent. The process is suitable, for example, for the production of printed circuits, solder resist masks and offset printing plates.
摘要翻译：用于在基板上制造保护层或浮雕图像的方法，其中由用于加聚反应可以通过辐射活化的含有光引发剂的固体成膜环氧树脂组成的辐射敏感层为从支撑体转移到基底，然后直接或在光掩模下曝光并通过热作用而硬化，之后如果合适，将未曝光部分用溶剂显影。该方法例如适用于生产印刷电路，阻焊掩模和胶版印刷版。

38. 发明授权

US4484992A Process for the production of hydrogen by means of heterogeneous photoredox catalysis 失效
标题翻译：通过异源光催化氧化生产氢气的方法
公开(公告)号：US4484992A
公开(公告)日：1984-11-27
申请号：US342615
申请日：1982-01-25
申请人： Niklaus Buhler , Jean F. Reber , Kurt Meier , Milos Rusek
发明人： Niklaus Buhler , Jean F. Reber , Kurt Meier , Milos Rusek
IPC分类号： B01J19/12 , B01J23/00 , B01J27/00 , B01J27/02 , B01J27/04 , B01J27/057 , B01J35/02 , C01B3/04 , C07B61/00
CPC分类号： C01B3/042 , B01J27/02 , B01J27/04 , B01J27/0573 , Y02E60/364
摘要： A process is described for the selective production of hydrogen by means of heterogeneous photoredox catalysis, in which mixtures of water and alkali metal sulfites or sulfides, alkaline earth metal sulfites or sulfides or ammonium sulfites or sulfides are reacted under the action of light in a suspension of a cadmium sulfide, cadmium sulfoselenide or titanium dioxide/semiconductor powder which is at least partially coated with Cu, Cr, Ni, Co or a noble metal or mixtures thereof. The catalysts which can be employed in this process (coated semiconductor powders) are in some cases novel.
摘要翻译：描述了通过异源光氧化物催化选择性生产氢的方法，其中水和碱金属亚硫酸盐或硫化物，碱土金属亚硫酸盐或硫化物或亚硫酸铵或硫化物的混合物在光的作用下在悬浮液中反应至少部分涂覆有Cu，Cr，Ni，Co或贵金属的硫化镉，硫化镉或二氧化钛/半导体粉末或其混合物。在这种方法中可以使用的催化剂（涂覆的半导体粉末）在某些情况下是新颖的。

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