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31. 发明专利

JPH09147783A METHOD AND DEVICE FOR MEASURING CONFIGURATION OF SAMPLE 失效
公开(公告)号：JPH09147783A
公开(公告)日：1997-06-06
申请号：JP30255395
申请日：1995-11-21
申请人： KAWASAKI STEEL CO
发明人： SAKAI MINORU , JINNO GIICHI , SHIMOMURA JUNICHI
IPC分类号： G01B15/00 , G01B15/08 , H01J37/256
摘要： PROBLEM TO BE SOLVED: To quantitatively measure the configuration of a sample by irradiating a sample with electrons, and detecting within a predetermined solid angle backscattered electrons produced from the sample surface for quantitative measurements of the sample configuration and for analysis of its composition. SOLUTION: When a sample is irradiated with S an electron beam EB from an electron gun 10, backscattered electrons BSE, secondary electrons SE, and characteristic X rays XR, emitted from the surface of the sample S, are detected respectively by a backscattered electron detector 1, a secondary electron detector 4, and a characteristic X-ray detector 5. The detector 1 is arranged immediately above the sample S in axial symmetry with respect to the electron beam EB in order to detect the electrons BSE within a predetermined solid angle, and has its detecting part divided into numerous parts. The electrons BSE detected by the detector 1 are amplified by a backscattered electron amplifier 6, are synchronized by an observation-CRT signal synchronizing device 7 with the scanning of the electron beam EB, and displayed on an observation CRT 8 simultaneously with images of the secondary electrons SE and the characteristic X-rays XR.

32. 发明专利

JPH0813192A RUSTPROOF STEEL SHEET EXCELLENT IN CORROSION RESISTANCE AND WORKABILITY AND ITS PRODUCTION 失效
公开(公告)号：JPH0813192A
公开(公告)日：1996-01-16
申请号：JP14976794
申请日：1994-06-30
申请人： KAWASAKI STEEL CO
发明人： MATSUSHIMA TOMOHIRO , GOTOU CHIZUKO , SHIMOMURA JUNICHI
IPC分类号： C25D3/56 , C25D5/26 , C25D5/50
摘要： PURPOSE:To produce a rustproof steel sheet excellent in corrosion resistance and workability by preparing a steel sheet having a Zn-Cr alloy plated layer contg. a specified amt. of Cr and substantially constituted of a single phase of a monoclinic system crystal phase having specified lattice constant. CONSTITUTION:A Zn-Cr alloy electroplated steel sheet having Zn-Cr electroplating in which the content of Cr is regulated to 3 to 40wt.% is subjected to heat treatment at 130 to

33. 发明专利

JPH0645270A METHOD FOR HEAT-TREATING SEMICONDUCTOR SUBSTRATE 失效
公开(公告)号：JPH0645270A
公开(公告)日：1994-02-18
申请号：JP21665892
申请日：1992-07-23
申请人： KAWASAKI STEEL CO
发明人： SHIMOMURA JUNICHI , OKIMOTO NOBUYUKI
IPC分类号： H01L21/265 , H01L21/324
摘要： PURPOSE:To reduce a lattice defect of the part where ions are implanted by suitably heat treating after ion implantion. CONSTITUTION:After ions of As, P, B, BF2, etc., are implanted in a semiconductor substrate, a first heat treatment is conducted at 600 to 800 deg.C, and then a second heat treatment is executed at 800 less than 1000 deg.C. It is desirable to execute the second treatment for 500sec or longer. The first treatment is conducted by lamping, and the second treatment can be executed for 500sec or longer. Further, the first and second treatments may be conducted in a lamp- annealing furnace.

34. 发明专利

JPH05186205A HEXAGONAL BORON NITRIDE POWDER AND ITS PRODUCTION 失效
公开(公告)号：JPH05186205A
公开(公告)日：1993-07-27
申请号：JP1951792
申请日：1992-01-08
申请人： KAWASAKI STEEL CO
发明人： SHIMOMURA JUNICHI , FUNABASHI TOSHIHIKO , KOITABASHI HISAMITSU
IPC分类号： A61K8/30 , A61K8/19 , A61Q1/02 , C01B21/064
摘要： PURPOSE:To provide hexagonal boron nitride powder with sustaining effect thereof, suitable esp. for cosmetics of excellent spreadability. CONSTITUTION:The objective hexagonal boron nitride powder whose flat-shaped powder side represents the respective six kinds of crystal faces equivalent to (100) plane and (110) plane in the crystal description for hexagonal system. The powder can be obtained by (A) heat-treating crude hexagonal boron nitride powder with a nitrogen-contg. compound as raw material at 1500-1900 deg.C in an inert gas atmosphere followed by further heat treatment at 1900-2200 deg.C in an inert gas atmosphere; or (B) heat-treating crude hexagonal boron nitride powder with a nitrogen-contg. compound as raw material at 1500-1900 deg.C in an inert gas atmosphere followed by removing the contained water-soluble components by washing with water and then further heat-treating at 1900-2200 deg.C in an inert gas atmosphere.

35. 发明专利

JPH03250607A CORROSIVE RESISTANT RARE EARTH-TRANSITION METAL MAGNET AND ITS MANUFACTURE 失效
公开(公告)号：JPH03250607A
公开(公告)日：1991-11-08
申请号：JP26963590
申请日：1990-10-09
申请人： KAWASAKI STEEL CO
发明人： OZAKI YUKIKO , SHIMOTOMAI MICHIO , FUKUDA YASUTAKA , FUJITA AKIRA , KITANO YOKO , SHIMOMURA JUNICHI
IPC分类号： C22C33/02 , C22C1/04 , C22C19/00 , C22C19/07 , C22C38/00 , H01F1/053 , H01F1/057 , H01F41/02
摘要： PURPOSE:To cause the title magnet to have both high magnetic characteristics and high corrosion resistance by mixing and pressing a powder mainly composed of an intermetallic compound having a specific RE2TM14B composition and one or more kinds of powder having, as a main phase, RE-TM interfamily compound or RE-TM-B intermetallic compound lower in the melting point than the first powder and thereafter by sintering the obtained product. CONSTITUTION:A mixed powder of a permanent magnet alloy, which consists of RE not less than 10% and not more than 25% including one or two sorts or materials selected from Y, Sc and lanthanoids, B of not less then 2% and not more than 20% and the rest TM and its constitution is in the phase od RE2TM14B composition having Nd2Fe14B structure, and a powder mainly composed of RE-TM intermetallic compound phase or RE-TM eutectic structure and/or RE-TM-B intermetallic compound phase lower in the melting point than the first phase is subjected to compression molding and sintered thereafter. For further improvement of corrosion resistance, it is effective that a grain boundary phase is electrochemically nobler than a main phase. Therefore, it is preferable to make the ratio of Ni and/or Co in TM in the RE-TM and RE-TM-B low melting point phase higher than that in the RE2TM14B phase.

36. 发明专利

JPS5844736B2 失效
公开(公告)号：JPS5844736B2
公开(公告)日：1983-10-05
申请号：JP15353179
申请日：1979-11-29
申请人： KAWASAKI STEEL CO
发明人： SHIMOMURA JUNICHI , NOHARA KYOHIKO , ONO HIROSHI , OOHASHI NOBUO
IPC分类号： C22C38/00 , C22C38/50

37. 发明专利

JPH10130778A FINE GRAIN DISPERSED TYPE STEEL FOR LARGE HEAT INPUT WELDING 失效
公开(公告)号：JPH10130778A
公开(公告)日：1998-05-19
申请号：JP29061196
申请日：1996-10-31
申请人： KAWASAKI STEEL CO
发明人： OTA HIROKI , SHIMOMURA JUNICHI
IPC分类号： C22C38/00 , C22C38/04 , C22C38/58
摘要： PROBLEM TO BE SOLVED: To improve toughness in a large heat input weld zone by dispersing fine TiMnO3 grains in a steel having respectively specified Si and B contents and forming fine transgranular ferrite even in a heat affected zone at large heat input welding SOLUTION: The steel has a composition consisting of, by mass, 0.02-0.15% C, 0.10-0.40% Si, 0.50-1.80% Mn, =2 kinds selected from 0.05-5.0% Ni, 0.05-1.0% Cu, 0.05-1.0% Cr, and 0.05-1.0% Mo and either or both of 0.02-0.10% Nb and 0.02-0.10% V are incorporated into the steel composition. It is preferable that the TiMnO3 grains are mixed with a metal powder, such as Fe powder, and formed into a green compact and this green compact is then added to a molten steel just before tapping or just before solidification and dispersed.

38. 发明专利

JPH09134693A PRETREATMENT METHOD OF NONCONDUCTIVE SAMPLE FOR OBSERVATION WITH ELECTRON MICROSCOPE, PRETREATING DEVICE AND ELECTRON MICROSCOPE 失效
公开(公告)号：JPH09134693A
公开(公告)日：1997-05-20
申请号：JP29010395
申请日：1995-11-08
申请人： KAWASAKI STEEL CO
发明人： SAKAI MINORU , KIKUCHI ASAO , SHIMOMURA JUNICHI
IPC分类号： G01N1/28 , H01J37/20 , H01J37/28
摘要： PROBLEM TO BE SOLVED: To prevent charge-up and pollution of a sample surface, and attain observation of a microscope by high accelerating voltage by performing pretreatment to preform a specific pattern on the sample surface when a shape of a nonconductive sample is observed by using an electron microscope. SOLUTION: For example, a nonconductive sample (such as silica) 2 is arranged on a sample stand 4 of a sample pretreating device 1, and is fixed by sample stand fixing jigs 5 and 6, and next, a prescribed lattice interval is set by using a lattice manufacturing machine 7, and pretreatment is performed to form a lattice pattern 3 preferably composed of a conductive substance (such as Au) having a low melting point and a small specific resistance value on a surface of a sample 4. For example, meshes which are used in a transmission type electron microscope and are made of metal (such as Cu) are arranged on an observing surface of the sample, and a shape is observed. Therefore, a clear electron microscope image of the sample can be obtained.

39. 发明专利

JPH07193073A MANUFACTURE OF SILICON WAFER 失效
公开(公告)号：JPH07193073A
公开(公告)日：1995-07-28
申请号：JP34702693
申请日：1993-12-27
申请人： KAWASAKI STEEL CO
发明人： ISHIKAWA SHIN , GOTOU CHIZUKO , SHIMOMURA JUNICHI
IPC分类号： C30B33/02 , H01L21/324
摘要： PURPOSE:To form crystal defects which fix contaminant element effectively by a method wherein, after a heat treatment by which defects in an element activating region are eliminated and, further, the density of crystal defects caused by oxygen deposition is made to be within a specific range, Cu is added to have a specific concentration. CONSTITUTION:A silicon wafer is subjected to a heat treatment by which defects in the element activating region of the silicon wafer are eliminated and, further, the density of crystal defects caused by oxygen deposition is made to be not less than 10 cm and not larger than 10 cm Further, Cu is added to the silicon wafer so as to have a concentration not less than 10 atoms.cm and not larger than 2X10 atoms.cm . By this method, Cu captured by the crystal defects in the silicon wafer is deposited and, further, a secondary crystal defects caused by the deposition of Cu are formed. With this constitution, the capability of gettering of contaminant element can be improved.

40. 发明专利

JPH01168856A METHOD FOR CASE-HARDENING STEEL 失效
公开(公告)号：JPH01168856A
公开(公告)日：1989-07-04
申请号：JP32594587
申请日：1987-12-23
申请人： AGENCY IND SCIENCE TECHN , KAWASAKI STEEL CO
发明人： SATO MAMORU , FUJII KANEYOSHI , KIUCHI MASATO , WANAKA HIROKI , KIMURA TATSUMI , SHIMOMURA JUNICHI , OHORI MANABU , UEDA SHUZO
IPC分类号： C23C14/06 , C23C14/24
摘要： PURPOSE:To form a TiN film having excellent adhesive property and wear resistance by specifying the accelerating voltage for nitrogen ion, current density, Ti vapor-deposition rate, total nitrogen ion input, and Ti vapor-deposition amt. at the time of forming the hard TiN layer on the steel product such as a rolling roll, a bearing, and a metallic mold by ion implantation and vacuum deposition. CONSTITUTION:When the rolling roll, bearing, metallic mold, etc., requiring wear resistance is case-hardened, a hard TiN layer is formed on the surface of the steel member to be treated by an ion mixing process wherein ion implantation and vacuum deposition are simultaneously or alternately carried out. The accelarating voltage for nitrogen ion in this case is controlled to 10-40kV, the current density of nitrogen ion to 0.5-2.0mA/cm , the Ti vapor deposition rate to >5Angstrom /sec, the total nitrogen input to >10 ion/cm , and the Ti vapor- deposition amt. to >5X10 ion/cm . A TiN film having excellent adhesive strength and water resistance is formed on the surface of the steel member to be treated.

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