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31. 发明申请

US20060264651A1 Method for hydrocyanating an olefinically unsaturated compound 审中-公开
标题翻译：氢化氰化烯属不饱和化合物的方法
公开(公告)号：US20060264651A1
公开(公告)日：2006-11-23
申请号：US10548536
申请日：2004-02-24
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miguel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Peter Babier
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miguel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Peter Babier
IPC分类号： C07C253/10
CPC分类号： C07C253/10 , C07C253/34 , C07C255/04
摘要： A process for hydrocyanating an olefinically unsaturated nitrile in the presence of an Ni(0)-containing catalyst, which comprises carrying out the reaction in the presence of a hydrocarbon which leads under certain pressure, concentration and temperature conditions to the formation of at least two liquid phases of the overall system, of which one phase has a higher proportion of the Ni(0)-containing catalyst, based on the total weight of this phase, than the other phase or other phases.
摘要翻译：一种在含有Ni（0）的催化剂存在下对烯属不饱和腈进行氢氰化的方法，其包括在一定压力，浓度和温度条件下导致的烃的存在下进行反应以形成至少两种与其他相或其他相相比，整个系统的液相，其中一相具有比该相的总重量更高的含Ni（0）的催化剂的比例。

32. 发明申请

US20060164911A1 Mixing device 失效
标题翻译：混合装置
公开(公告)号：US20060164911A1
公开(公告)日：2006-07-27
申请号：US10530930
申请日：2003-10-14
申请人： Hartmut Nikolai , Ernst-Jurgen Grittmann
发明人： Hartmut Nikolai , Ernst-Jurgen Grittmann
IPC分类号： B29B7/42 , B29B7/58
CPC分类号： B29C47/60 , B29B7/421 , B29C47/0009
摘要： A device comprising a shaft (1), a front ring (2), which is non-positively and positively connected to this shaft, an end ring (3), which is non-positively and positively connected to the shaft at a distance A from the front ring, and a loose mixing ring (4), which is freely rotatable and located between the front ring and the end ring, wherein the front ring and the end ring in each case have at least one channel (2k) or (3k), respectively, which runs axially parallel, at an angle in relation to the axis of the shaft or helically, and has in each case at least two regions (2b1 and 2b2) or (3b1 and 3b2) of different outside diameters, of which the region with the smaller outside diameter (2b2) or (3b2) is respectively located on the side facing the mixing ring, and the mixing ring has a first region (4b1) in which its inside diameter is large enough for it to be able to overlap with the region of smaller diameter of the front ring (2b2), has an adjoining region (4b2) in which the mixing ring has on its inner side at least one channel (4k) which runs axially parallel, at an angle in relation to the axis of the shaft or helically thereto, and also an adjoining third region (4b3), in which its inside diameter is large enough for it to be able to overlap with the region of smaller diameter of the end ring (3b2) and the mixing ring is so long that, in its respective end positions, the other of the two rings (2) or (3) respectively is partially overlapped by the mixing ring.
摘要翻译：一种装置，包括轴（1），前端环（2），其不间断地和主动地连接到该轴上;端环（3），其以一定距离A不间断地和主动地连接到轴以及松散的混合环（4），其可自由旋转并位于前环和端环之间，其中前环和端环在每种情况下具有至少一个通道（2k）或（3k），其分别轴向平行地以相对于轴的轴线或螺旋形的方式成角度地延伸，并且在每种情况下具有至少两个区域（2ba和2b）其中外径较小的区域（2b <2>），或（3b） SUB 3）或（3 b 2 2 N）分别位于面向混合环的一侧，并且混合环具有第一区域（4 b <1 >），其中其内径足够大以使其能够与其重叠所述前环的较小直径的区域（2 b 2 2）具有邻接区域（4b），其中所述混合环的内侧具有至少一个通道（4k），其以相对于轴的轴线或螺旋形的方式以一定角度轴向平行地延伸，以及相邻的第三区域（4 b 3 N 3），其中其内径为足够大以使其能够与端环（3 b 2 2）的较小直径的区域重叠，并且混合环如此长，使得在其各自的端部位置中，另一个两个环（2）或（3）分别与混合环部分重叠。

33. 发明申请

US20060122436A1 Method for producing aldehydes from alkanes 审中-公开
标题翻译：从烷烃生产醛的方法
公开(公告)号：US20060122436A1
公开(公告)日：2006-06-08
申请号：US10533959
申请日：2003-11-03
申请人： Götz-Peter Schindler , Rocco Paciello , Klaus Harth
发明人： Götz-Peter Schindler , Rocco Paciello , Klaus Harth
IPC分类号： C07C45/50
CPC分类号： C07C45/72 , C07C5/42 , C07C29/141 , C07C45/50 , Y02P20/125 , C07C31/125 , C07C47/02 , C07C11/06 , C07C11/08
摘要： Process for preparing saturated aliphatic Cn-aldehydes and Cn-1-alkanes, where n is from 4 to 20, which comprises a) providing a feed gas stream comprising one or more Cn-1-alkanes, b) subjecting the Cn-1-alkanes to a catalytic dehydrogenation to give a product gas stream comprising unreacted Cn-1-alkanes, one or more Cn-1-alkenes and secondary constituents, c) at least partly hydroformylating the Cn-1-alkenes in the presence of the Cn-1-alkanes and possibly the secondary constituents by means of carbon monoxide and hydrogen in the presence of a hydroformylation catalyst to give the Cn-aldehydes, d) separating the product mixture obtained to give a stream comprising the Cn-aldehydes and a stream comprising Cn-1-alkanes and possibly secondary constituents, e) recirculating at least part of the gas stream comprising the Cn-1-alkanes and possibly the secondary constituents as recycle gas stream to the catalytic alkane dehydrogenation (step b)).
摘要翻译：制备饱和脂肪族C n - 醛和C n-1-N烷烃的方法，其中n为4至20，其包括a）提供包含一种或更多的C 1〜n烷烃，b）使C 1 -C 12烷烃进行催化脱氢，得到包含未反应的C n的产物气流 -1个 - 烷烃，一个或多个C n-1 - 烯烃和第二组分，c）至少部分地将C 1 -C 6 - 亚烷基在加氢甲酰化催化剂存在下，通过一氧化碳和氢气存在C n-1 - 烷烃并且可能存在第二成分，得到C 1 -C 6烷基，d）将得到的产物混合物分离得到包含C 1 -C 4烷基的物流和包含C 1〜N 2烷烃的物流，并且可能是二级成分，e）循环气流的至少一部分包含C n-1 - 烷烃，并且可能是二级的 y成分作为催化烷烃脱氢的再循环气流（步骤b））。

34. 发明申请

US20090078087A1 PROCESS FOR THE ACID DIGESTION OF METAL-CONTAINING COMPOUNDS 审中-公开
标题翻译：含金属化合物的酸性处理方法
公开(公告)号：US20090078087A1
公开(公告)日：2009-03-26
申请号：US12281217
申请日：2007-02-28
申请人： Thomas Heidenfelder , Helmut Witteler , Bernd Laubusch , Hans-Peter Seelmann-Eggebert
发明人： Thomas Heidenfelder , Helmut Witteler , Bernd Laubusch , Hans-Peter Seelmann-Eggebert
IPC分类号： C22B15/00 , C09K3/00
CPC分类号： C22B15/0071 , C22B3/0031 , C22B3/08 , C22B3/165 , C22B7/007 , C22B19/22 , C22B59/00 , Y02P10/234 , Y02P10/236
摘要： Aqueous leachant compositions and processes for using the same comprising: (a) providing a metal-containing compound; and (b) subjecting the metal-containing compound to an acid digestion comprising contacting the metal-containing compound with an aqueous leachant; wherein the aqueous leachant comprises a mixture selected from the group consisting of: (i) sulfuric acid and one or more alkanesulfonic acids having alkane moieties selected from the group consisting of propyl, ethyl and methyl groups, at a weight ratio of alkanesulfonic acid to sulfuric acid of 1:1000 to 1:1; (ii) sulfuric acid and one or more salts of alkanesulfonic acids having alkane moieties selected from the group consisting of propyl, ethyl and methyl groups, at a weight ratio of salt of alkanesulfonic acid to sulfuric acid of 1:9 to 1:99.
摘要翻译：含水浸出剂组合物及其使用方法包括：（a）提供含金属的化合物; 和（b）使含金属化合物进行酸消化，包括使含金属化合物与含水浸出剂接触; 其中所述含水浸出剂包含选自以下的混合物：（i）硫酸和一种或多种烷烃磺酸，其烷烃部分选自丙基，乙基和甲基，烷基磺酸与硫酸的重量比酸为1：1000至1：1; （ii）硫酸和一种或多种烷烃磺酸盐，其烷烃部分选自丙基，乙基和甲基，烷基磺酸与硫酸的重量比为1:9至1:99。

35. 发明申请

US20080064594A1 Titanium Dioxide Mixtures for Producing Catalysts 失效
标题翻译：用于生产催化剂的二氧化钛混合物
公开(公告)号：US20080064594A1
公开(公告)日：2008-03-13
申请号：US11719422
申请日：2005-04-11
申请人： Samuel Neto , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B01J21/00
CPC分类号： B01J21/063 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J35/1014 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/53 , B01J2523/55 , B01J2523/15 , B01J2523/47 , B01J2523/51
摘要： Catalytic titanium dioxide mixtures comprising: a first anatase titanium dioxide having a BET surface area greater than 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti of from 5 to 20 μmol/m2; and a second anatase titanium dioxide having a BET surface area less than or equal to 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 0.6 to 7 μmol/m2, processes for preparing catalysts containing the same, catalysts containing active compositions including such titanium dioxide mixtures on support materials, and catalyst systems using the same.
摘要翻译：催化二氧化钛混合物，其包含：具有大于15m 2 / g的BET表面积的第一锐钛矿二氧化钛和将Ti 4+还原成Ti的氢吸收为5至20mumol / m 2; 和具有小于或等于15m 2 / g的BET表面积的第二锐钛矿二氧化钛和用于还原Ti 4+的氢吸收 0.6〜7μmol/ m 2以上的3+以下，制备含有该催化剂的催化剂的方法，含有活性组合物的催化剂，包括载体材料上的这种二氧化钛混合物，以及使用相同。

36. 发明申请

US20070270614A1 Method for Controlling the Reactor Admission Temperature During the Production of Methylamine 有权
标题翻译：控制甲胺生产过程中反应器进口温度的方法
公开(公告)号：US20070270614A1
公开(公告)日：2007-11-22
申请号：US10573185
申请日：2004-09-24
申请人： Werner Reutemann , Rolf Wambsganss , Frank Poplow , Theodor Weber , Karl-Heinz Ross , Manfred Julius
发明人： Werner Reutemann , Rolf Wambsganss , Frank Poplow , Theodor Weber , Karl-Heinz Ross , Manfred Julius
IPC分类号： C07C209/14
CPC分类号： C07C209/16 , C07C211/04
摘要： The invention relates to a process for preparing methylamines by gas-phase reaction of methanol and ammonia as starting materials at a pressure in the range from 15 to 30 bar in the presence of heterogeneous catalyst. The starting materials are vaporized in one or more heat exchangers (1, 2, 3), superheated to produce a feed gas stream and subsequently fed into a reactor (4), with the mixing of the starting materials being able to be carried out in the feed stream to one of the heat exchangers (1, 2, 3) or at any desired position in a heat exchanger (1, 2, 3). A product gas stream comprising monomethylamine, dimethylamine and trimethylamine and also reaction by-products is taken off from the reactor (4). To control the reactor inlet temperature of the starting materials to a temperature in the range from 360° C. to 370° C., all or some of the feed gas stream or the product gas stream is passed through an adjustable valve (5) in order to vary the pressure and thus the condensation temperature.
摘要翻译：本发明涉及通过甲醇和氨作为起始原料在非均相催化剂存在下在15至30巴的压力下气相反应制备甲胺的方法。起始材料在一个或多个热交换器（1,2,3）中蒸发，过热以产生进料气流，并随后进料到反应器（4）中，原料的混合能够进行到一个热交换器（1,2,3）或在热交换器（1,2,3）中的任何期望位置的进料流。从反应器（4）中取出包含一甲胺，二甲胺和三甲胺以及反应副产物的产物气流。为了将原料的反应器入口温度控制在360℃至370℃的温度范围内，所有或一些进料气流或产物气流通过可调节阀（5），其中以改变压力，从而改变冷凝温度。

37. 发明申请

US20070202060A1 Retinoid-Containing Preparations 审中-公开
标题翻译：含维甲酸的制剂
公开(公告)号：US20070202060A1
公开(公告)日：2007-08-30
申请号：US10586776
申请日：2005-01-14
申请人： Arne Ptock , Axel Jentzsch
发明人： Arne Ptock , Axel Jentzsch
IPC分类号： A61K8/49 , A61K31/355 , A61K31/07
CPC分类号： A61K8/671 , A61K8/676 , A61K8/678 , A61K2800/522 , A61Q1/02 , A61Q17/04 , A61Q19/00 , A61Q19/08
摘要： Preparations comprising a. at least one retinoid, b. at least one water-soluble antioxidant, c. at least one oil-soluble antioxidant and d. 0.01 to 10% by weight of at least one UV filter, wherein, in the preparations, per part by weight of retinoid, at least 1 part by weight of one or more water-soluble antioxidants and 0.1 to 100 parts by weight of one or more oil-soluble antioxidants are present, where the content of one or more water-soluble antioxidants is in the range from 0.05 to 0.8% by weight, based on the total amount of the preparations.
摘要翻译：准备工作包括a。至少一种类视黄醇，b。至少一种水溶性抗氧化剂，c。至少一种油溶性抗氧化剂和d。 0.01至10重量％的至少一种UV过滤器，其中在制剂中，每重量份类视黄醇，至少1重量份的一种或多种水溶性抗氧化剂和0.1至100重量份的一种或多种存在更多的油溶性抗氧化剂，其中基于制剂的总量，一种或多种水溶性抗氧化剂的含量在0.05至0.8重量％的范围内。

38. 发明申请

US20070149793A1 Heterogeneous ruthenium catalyst, nucleus-hydrogenated diglycidyl ether of bisphenols a and f, and method for the production thereof 审中-公开
标题翻译：非均相钌催化剂，双酚a和f的核氢化二缩水甘油醚及其制备方法
公开(公告)号：US20070149793A1
公开(公告)日：2007-06-28
申请号：US10583539
申请日：2004-12-08
申请人： Jan-Dirk Arndt , Frederik Laar , Michael Becker , Stephan Herwig
发明人： Jan-Dirk Arndt , Frederik Laar , Michael Becker , Stephan Herwig
IPC分类号： C07D405/02
CPC分类号： C07D303/28 , B01J21/08 , B01J23/462 , B01J23/58 , B01J33/00 , B01J35/002 , B01J35/006 , B01J35/008 , B01J35/1014 , B01J35/1019 , B01J35/1023 , B01J35/1047 , B01J35/1061 , B01J37/14 , C07D303/30 , C08G59/24
摘要： A heterogeneous ruthenium catalyst comprising silicon dioxide as support material, in which the percentage ratio of the Q2 and Q3 structures Q2/Q3 in the silicon dioxide determined by means of solid-state 29Si-NMR is less than 25, a process for preparing a bisglycidyl ether of the formula I where R is CH3 or H, by ring hydrogenation of the corresponding aromatic bisglycidyl ether of the formula II in which the abovementioned heterogeneous ruthenium catalyst is used, and a bisglycidyl ether of the formula I which can be prepared using the abovementioned process.
摘要翻译：包含二氧化硅作为载体材料的异相钌催化剂，其中Q 2和Q 3结构的百分比Q 2 / Q 2，通过固相法测定的二氧化硅中的“3”> 3 <3>小于25，制备式I的双缩水甘油醚的方法，其中R为CH 通过使用其中使用上述非均相钌催化剂的式II的相应的芳族二缩水甘油醚和可以使用上述方法制备的式I的双缩水甘油醚进行环氢化来制备。

39. 发明申请

US20070123726A1 Method for producing phosphonium salts 有权
标题翻译：鏻盐的制备方法
公开(公告)号：US20070123726A1
公开(公告)日：2007-05-31
申请号：US10582912
申请日：2004-12-14
申请人： Laszlo Szarvas , Klemens Massonne , Harald Laas , Kai Exner , Detlev Glas
发明人： Laszlo Szarvas , Klemens Massonne , Harald Laas , Kai Exner , Detlev Glas
IPC分类号： C07F9/02
CPC分类号： C07F9/5428 , C07F9/5442
摘要： The present invention relates to a process for preparing quaternary phosphonium salts by reacting a ternary phosphine with an optionally substituted, saturated or monounsaturated or polyunsaturated electrophile having from 3 to 25 carbon atoms in ternary solvent mixtures.
摘要翻译：本发明涉及通过使三元膦与在三元溶剂混合物中具有3至25个碳原子的任选取代的饱和或不饱和或多不饱和亲电体反应来制备季鏻盐的方法。

40. 发明申请

US20070100097A1 Method for the anionic polymerisation of oxiranes 审中-公开
标题翻译：环氧乙烷的阴离子聚合方法
公开(公告)号：US20070100097A1
公开(公告)日：2007-05-03
申请号：US10557838
申请日：2004-05-10
申请人： Philippe Desbois , Alain Deffieux , Stephane Carlotti , Cyrille Billouard
发明人： Philippe Desbois , Alain Deffieux , Stephane Carlotti , Cyrille Billouard
IPC分类号： C08F4/46
CPC分类号： C08G65/12
摘要： Process for preparing homopolymers of oxiranes, or for preparing copolymers of oxiranes and comonomers, via anionic polymerization in the presence of an alkali metal compound and of an organylaluminum compound, which comprises avoiding any use of crown ethers or of cryptands during the polymerization.
摘要翻译：在碱金属化合物和有机铝化合物的存在下通过阴离子聚合制备环氧乙烯的均聚物或制备环氧乙烷和共聚单体的共聚物的方法，其包括在聚合过程中避免使用冠醚或穴状物。

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