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    • 22. 发明授权
    • Powder of a vinylpyrrolidone polymer and a process for production thereof
    • 乙烯基吡咯烷酮聚合物的粉末及其制备方法
    • US07910672B2
    • 2011-03-22
    • US11666883
    • 2005-11-02
    • Kazuhiro OkamuraNorihiro WakaoKeiji WatanabeKeiichi Fujise
    • Kazuhiro OkamuraNorihiro WakaoKeiji WatanabeKeiichi Fujise
    • C08F26/10
    • C08F226/10C08J3/12C08J2339/00C09D139/06C09J139/06
    • The present invention is a powder of a vinylpyrrolidone polymer having a K value of smaller than 50, characterized in that a content of particles having a particle diameter of 106 μm or smaller is 10% by mass or less and a content of particles having a particle diameter of greater than 1,000 μm is 5% by mass or lower. A process for production of a powder of a vinylpyrrolidone polymer according to the present invention is characterized in that a vinylpyrrolidone polymer having a K value of smaller than 50 is formed into a solution having a concentration from 30% to 70% by mass, and the solution is dried by using a hot surface adhesion-type dryer, followed by pulverization so that a content of particles having a particle diameter of 106 μm or smaller is 10% by mass or lower and a content of particles having a particle diameter of greater than 1,000 μm is 5% by mass or lower.Thus, there is provided a powder of a vinylpyrrolidone polymer, which has excellent solubility in spite of having a low K value determined by a Fikentscher method and can be made into solution with favorable handleability without dust rising, and a process for production of the same.
    • 本发明是K值小于50的乙烯基吡咯烷酮聚合物的粉末,其特征在于,粒径为10μm以下的粒子的含量为10质量%以下,具有粒子的粒子的含量 大于1000μm的直径为5质量%以下。 本发明的乙烯基吡咯烷酮聚合物粉末的制造方法的特征在于,将K值小于50的乙烯基吡咯烷酮聚合物形成浓度为30〜70质量%的溶液, 溶液通过使用热表面粘附型干燥器进行干燥,然后粉碎,使得粒径为10μm以下的颗粒的含量为10质量%以下,粒径为 1,000μm为5质量%以下。 因此,提供了一种乙烯基吡咯烷酮聚合物的粉末,尽管具有通过Fikentscher方法测定的低K值而具有优异的溶解性,并且可以制成具有良好可操作性而没有粉尘升高的溶液及其制备方法 。