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21. 发明公开

EP1196374A1 PROCESS OF PREPARING A HIGH-ENERGY SOFTENING AGENT 有权
标题翻译：方法一种生产能量富增塑剂
公开(公告)号：EP1196374A1
公开(公告)日：2002-04-17
申请号：EP99956364.6
申请日：1999-10-14
申请人： Dyno Nobel ASA
发明人： SKJOLD, Erlend , JOHANSEN, yvind, Hammer , GJERSOE, Richard , HALVORSEN, Terje , BERG, Alf , GRANBY, Trine , CHRISTENSEN, Mona
IPC分类号： C07C243/02 , C07C241/00 , C06B25/34
CPC分类号： C07C241/00 , C06B25/34 , C06B45/105 , C07C213/06 , C07C243/02 , C07C219/16
摘要： The present invention relates to a continuous process of preparing N-alkyl-nitratoethylamines and a production plant for carrying out a continuous process of preparing such N-alkyl-nitratoethylamines.

22. 发明公开

EP1119544A1 ENERGETIC NITRAMINE-LINKED AZOLES AND HYDROXYLAMMONIUM SALTS AS OXIDIZERS, INITIATORS AND GAS GENERATORS 审中-公开
标题翻译：高能NITRA MINE具体种唑类和羟的作为氧化剂，引发剂和充气器
公开(公告)号：EP1119544A1
公开(公告)日：2001-08-01
申请号：EP99951844.2
申请日：1999-10-07
申请人： SRI INTERNATIONAL
发明人： BOTTARO, Jeffrey, C. , SCHMITT, Robert, J. , PETRIE, Mark, A. , PENWELL, Paul, E.
IPC分类号： C07C243/02 , C07D249/10 , C06B25/34 , A61K31/13 , A61K31/41
CPC分类号： C07D257/04 , C06B25/34 , C07C243/02 , C07D249/10
摘要： Novel compounds are provided having the structural formula R[-N(NO2)-L-R1]n wherein R, L, R1 and n are defined herein. The compounds are useful in a variety of contexts, but are primarily to be used as high energy oxidizing agents in explosive compositions, propellant formulations, gas-generating compositions and the like. The compounds are also useful as pharmaceutical agents. Compositions containing the compounds are also provided, including energetic compositions, as are methods for using the novel compounds and compositions.

23. 发明授权

US06670506B2 Method for producing dinitro-diaza-alkanes and interediate products thereof 失效
标题翻译：二硝基二烷 - 烷烃及其中间产物的制备方法
公开(公告)号：US06670506B2
公开(公告)日：2003-12-30
申请号：US09959631
申请日：2001-11-01
申请人： Thomas Knott
发明人： Thomas Knott
IPC分类号： C07C24100
CPC分类号： C07C243/02 , C07C231/02 , C07C241/00 , C07C233/56
摘要： A method of synthesis of dinitro-diaza-alkanes and intermediate products thereto from alkylamines and esters, whereby a dialkyl ester of a dicarboxylic acid is reacted with an alkylamine in an aqueous medium to form the corresponding dialkyldiamide of the dicarboxylic acid; the resulting dialkyldiamide is nitrated by means of conventional nitration agents to form the corresponding dialkyldinitroamide of the dicarboxylic acid and; the resulting dialkyldinitroamide is reacted with methylamine and/or ethylamine in an aquous medium to yield a corresponding alkylnitroamine and the dimethyldiamide and/or diethyldiamide of the dicarboxylic acid, and the alkylnitroamine is isolated from that, and the isolated alkylnitroamine is condensed in a known manner to form the dinitro-diaza-alkanes.
摘要翻译：从烷基胺和酯合成二硝基二氮烷 - 烷烃及其中间产物的方法，其中二羧酸的二烷基酯与水性介质中的烷基胺反应形成二羧酸的相应二烷基二酰胺;得到的二烷基二酰胺为通过常规硝化剂硝化以形成二羧酸的相应的二烷基二硝基酰胺;并且将所得的二烷基二硝基酰胺与水性介质中的甲胺和/或乙胺反应，得到相应的烷基硝胺，二羧酸的二甲基二酰胺和/或二乙基二酰胺，并从其中分离烷基硝胺，分离的烷基硝胺以已知的方式冷凝以形成二硝基二氮烷 - 烷烃。

24. 发明申请

US20010044544A1 Energetic nitramine-linked azoles and related compounds as oxidizers, initiators and gas generators 失效
标题翻译：活性硝胺连接的唑类和相关化合物作为氧化剂，引发剂和气体发生器
公开(公告)号：US20010044544A1
公开(公告)日：2001-11-22
申请号：US09877319
申请日：2001-06-07
发明人： Jeffrey C. Bottaro , Robert J. Schmitt , Mark A. Petrie , Paul E. Penwell
IPC分类号： C07D203/04 , C07D211/26 , C07D207/10
CPC分类号： C07D257/04 , C06B25/34 , C07C243/02 , C07D249/10
摘要： Novel compounds are provided having the structural formula RnullnullN(NO2)nullLnullR1nulln wherein R, L, R1 and n are defined herein. The compounds are useful in a variety of contexts, but are primarily to be used as high energy oxidizing agents in explosive compositions, propellant formulations, gas-generating compositions and the like. The compounds are also useful as pharmaceutical agents. Compositions containing the compounds are also provided, including energetic compositions, as are methods for using the novel compounds and compositions.
摘要翻译：提供具有结构式R [-N（NO 2）-L-R 1] n的新化合物，其中R，L，R 1和n如本文所定义。这些化合物可用于各种情况，但主要用作爆炸组合物中的高能氧化剂，推进剂制剂，产气组合物等。这些化合物也可用作药剂。还提供了含有化合物的组合物，包括能量组合物，以及使用新化合物和组合物的方法。

25. 发明授权

US06262301B1 Process of preparing a high-energy softening agent 有权
标题翻译：制备高能软化剂的方法
公开(公告)号：US06262301B1
公开(公告)日：2001-07-17
申请号：US09524013
申请日：2000-03-13
申请人： Erlend Skjold , Øyvind Hammer Johansen , Richard Gjersøe , Terje Halvorsen , Alf Berg , Trine Granby , Mona Christensen
发明人： Erlend Skjold , Øyvind Hammer Johansen , Richard Gjersøe , Terje Halvorsen , Alf Berg , Trine Granby , Mona Christensen
IPC分类号： C07C24302
CPC分类号： C07C241/00 , C07C243/02
摘要： The present invention relates to a continuous process of preparing N-alkyl-nitratoethylamines and a production plant for carrying out a continuous process of preparing such N-alkyl-nitratoethylamines.
摘要翻译：本发明涉及一种制备N-烷基 - 硝基乙胺的连续方法和一种制备这种N-烷基 - 硝基乙胺的连续方法的生产装置。

26. 发明授权

US06255512B1 Energetic nitramine-linked azoles and hydroxylammonium salts as oxidizers, initiators and gas generators 失效
标题翻译：能量的硝胺连接的唑类和羟基铵盐作为氧化剂，引发剂和气体发生器
公开(公告)号：US06255512B1
公开(公告)日：2001-07-03
申请号：US09414977
申请日：1999-10-07
申请人： Jeffrey C. Bottaro , Robert J. Schmitt , Mark A. Petrie , Paul E. Penwell
发明人： Jeffrey C. Bottaro , Robert J. Schmitt , Mark A. Petrie , Paul E. Penwell
IPC分类号： C07C24302
CPC分类号： C07D257/04 , C06B25/34 , C07C243/02 , C07D249/10
摘要： Novel compounds are provided having the structural formula R[—N(NO2)—L—R1]n wherein R, L, R1 and n are defined herein. The compounds are useful in a variety of contexts, but are primarily to be used as high energy oxidizing agents in explosive compositions, propellant formulations, gas-generating compositions and the like. The compounds are also useful as pharmaceutical agents. Compositions containing the compounds are also provided, including energetic compositions, as are methods for using the novel compounds and compositions.
摘要翻译：提供具有结构式R [-N（NO 2）-L-R 1] n的新化合物，其中R，L，R 1和n如本文所定义。这些化合物可用于各种情况，但主要用作爆炸组合物中的高能氧化剂，推进剂制剂，产气组合物等。这些化合物也可用作药剂。还提供了含有化合物的组合物，包括能量组合物，以及使用新化合物和组合物的方法。

27. 发明授权

US5081255A High melting aromatic nitrate esters 失效
标题翻译：高熔点芳香族硝酸酯
公开(公告)号：US5081255A
公开(公告)日：1992-01-14
申请号：US704561
申请日：1991-05-17
申请人： Michael E. Sitzmann
发明人： Michael E. Sitzmann
IPC分类号： C07C219/32 , C07C243/02 , C07D271/10 , C07D271/107
CPC分类号： C07D271/107 , C07C219/32 , C07C243/02
摘要： A nitrate ester which is 2,4,6-trinitro-1-(2-hydroxyethylamino)-3- (2-hydyethylnitramino)benzenedinitrate; 2,4,6-trinitro-1,3,5-tris(2-hydroxyethylamino)benzenetrinitrate; 2,2',4,4',6,6'-hexanitro-3-(2-hydroxyethylnitramino)stilbenitrate; 2,5-bis[3-(hydroxyethylaminonitrate)-2,4,6-trinitrophenyl]1,3,4-oxadiazole; or 2,5-bis[3-(hydroxyethylaminonitrate)-5- (hydroxyethylnitraminonitrate)-2,4,6-trinitrophenyl]-1,3,4-oxiazole and a process for preparing these compounds.
摘要翻译： 2,4,6-三硝基-1-（2-羟乙基氨基）-3-（2-羟基乙基硝基）苯甲酸酯的硝酸酯; 2,4,6-三硝基-1,3,5-三（2-羟乙基氨基）苯甲腈酸盐; 2,2'，4,4'，6,6'-六硝基-3-（2-羟乙基硝基甲硅烷基）二苯乙烯盐; 2,5-双[3-（羟乙基氨基硝酸盐）-2,4,6-三硝基苯基] 1,3,4-氧杂唑; 或2,5-双[3-（羟乙基氨基硝酸盐）-5-（羟基乙基硝基柠檬酸盐）-2,4,6-三硝基苯基] -1,3,4-噻唑及其制备方法。

28. 发明授权

US4820859A Process for the production of high energy material 失效
标题翻译：高能材料生产工艺
公开(公告)号：US4820859A
公开(公告)日：1989-04-11
申请号：US794340
申请日：1985-11-05
申请人： Ross W. Millar , Norman C. Paul , David H. Richards
发明人： Ross W. Millar , Norman C. Paul , David H. Richards
IPC分类号： C07C201/02 , C07C203/04 , C08C19/40 , C07C77/02
CPC分类号： C08C19/40 , C07C201/02 , C07C243/02
摘要： A process for the production of a high energy material involves reacting, in an inert organic solvent, a heterocyclic compound selected from oxirane, aziridine, oxetane or azetidine with a nitrogen oxide selected from dinitrogen tetroxide (N.sub.2 O.sub.4) and dinitrogen pentoxide (N.sub.2 O.sub.5) and, when the nitrogen oxide is N.sub.2 O.sub.4, oxidizing the O- or N- nitroso substituent or substituents in the product obtained to O- or N- nitro substituent or substituents. The heterocyclic compounds may be substituents or unsubstituted. In the former case the preferred substituents groups are halogen, alkyl, alkenyl, nitro and epoxy (as in epoxidized polybutadiene). The solvent is preferably a chlorinated alkane.Novel nitrated derivatives of polybutadiene, in which between 1% and 25% of the carbon atoms in the polymer are substituted by nitrate (ONO.sub.2), are also provided. These novel materials are liquid rubbers when the polybutadiene starting material has a molecular weight between 2000 and 10000.
摘要翻译：用于生产高能材料的方法包括在惰性有机溶剂中使选自环氧乙烷，氮丙啶，氧杂环丁烷或氮杂环丁烷的杂环化合物与选自四氧化二氮（N 2 O 4）和五氧化二氮（N 2 O 5）的氮氧化物反应，当氮氧化物是N 2 O 4时，将获得的产物中的O-或N-亚硝基取代基或取代基氧化成O-或N-硝基取代基。杂环化合物可以是取代基或未取代的。在前一种情况下，优选的取代基是卤素，烷基，烯基，硝基和环氧基（如在环氧化的聚丁二烯中）。溶剂优选为氯化烷烃。还提供了聚合物中1％至25％的碳原子被硝酸（ONO 2）取代的聚丁二烯的新型硝化衍生物。当聚丁二烯起始材料的分子量在2000和10000之间时，这些新型材料是液体橡胶。

29. 发明申请

WO00041798A1 PROCESS FOR THE BENIGN DIRECT FIXATION AND CONVERSION OF NITROGEN OXIDES 审中-公开
标题翻译：硝酸直接固定和转化的方法
公开(公告)号：WO00041798A1
公开(公告)日：2000-07-20
申请号：PCT/US2000/001025
申请日：2000-01-14
IPC分类号： B01D53/04 , C07C243/00 , C07C243/02 , C07F3/00 , B01D53/56
CPC分类号： B01D53/02 , B01D2253/102 , B01D2253/106 , B01D2257/404 , C07C243/00 , C07C243/02 , C07F3/003
摘要： A direct fixation of NO2 and N2O4 at room temperature and atmospheric pressure is described using bis(diorganoamino)magnesium compounds formed from reactions between donor-solvent free diorganomagnesium compounds and primary or secondary amines, yielding new compositions of matter having the general formulas [(R2N)i(R2NNxOy)jMg]m and [(R2N)i(R2NNxOy)j(NxOy)kMg]m. Methods are also described to convert these new compositions of matter into useful organic compounds and nitrogen gas.
摘要翻译：使用由供体无溶剂二有机镁化合物与伯胺或仲胺之间的反应形成的双（二有机基氨基）镁化合物来描述在室温和大气压下直接固定NO 2和N 2 O 4，产生具有通式[（R 2 N ）i（R2NNxOy）jMg] m和[（R2N）i（R2NNxOy）j（NxOy）kMg] m。还描述了将这些新的物质组合物转化为有用的有机化合物和氮气的方法。

30. 发明申请

WO1994005643A1 NEOPENTYL DIFLUOROAMINO COMPOUNDS FOR USE IN ENERGETIC FORMULATIONS 审中-公开
标题翻译： NEOPYYL DIFLOOROAMINO化合物用于能量配方
公开(公告)号：WO1994005643A1
公开(公告)日：1994-03-17
申请号：PCT/US1993008224
申请日：1993-09-01
申请人： AEROJET-GENERAL CORPORATION
发明人： AEROJET-GENERAL CORPORATION , ARCHIBALD, Thomas, G. , MANSER, Gerald, E.
IPC分类号： C07D239/04
CPC分类号： C07C247/04 , C07C239/04 , C07C243/02 , C07D205/04 , C07D239/04
摘要： This invention relates to novel neopentyl difluoroamino compounds which are useful as plasticizers and oxidizers in energetic formulations, such as propellants, explosives, and gasifiers. These neopentyl difluoroamino compounds can be prepared either: (1) by the direct fluorination of amine derivatives containing energetic pendant groups; or (2) by first preparing NF2-derivatives and then substituting these derivatives with energetic pendant groups. In particular, mono- and bis-(difluoroaminomethyl) oxetanes are synthesized and further reacted to yield the corresponding dinitrate esters. It has been discovered that these NF2-dinitrate esters are very useful as energetic plasticizers in high-energy formulations.
摘要翻译：本发明涉及新型新戊基二氟氨基化合物，其可用作能量制剂中的增塑剂和氧化剂，例如推进剂，爆炸物和气化器。这些新戊基二氟氨基化合物可以制备成：（1）通过直接氟化含有能量侧基的胺衍生物; 或（2）首先制备NF2衍生物，然后用能量侧基代替这些衍生物。特别地，合成单 - 和二 - （二氟氨基甲基）氧杂环丁烷并进一步反应以产生相应的硝酸酯。已经发现，这些NF2-硝酸酯在高能量配方中作为能量增塑剂非常有用。

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