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21. 发明申请

WO1989005336A1 CHEMICAL REACTIONS IN REVERSE MICELLE SYSTEMS 审中-公开
标题翻译：反向麦克勒系统中的化学反应
公开(公告)号：WO1989005336A1
公开(公告)日：1989-06-15
申请号：PCT/US1988004230
申请日：1988-11-23
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： BATTELLE MEMORIAL INSTITUTE , MATSON, Dean, W. , FULTON, John, L. , SMITH, Richard, D. , CONSANI, Keith, A.
IPC分类号： C09K11/07
CPC分类号： A61K9/1075 , B01D11/0203 , B01F3/0811 , B01F17/00 , B01F2003/0064 , B01F2003/0834 , B01J3/008 , B01J10/002 , B01J2219/00058 , B01J2219/00065 , B01J2219/00191 , C01B13/32 , C01B13/328 , C01B33/163 , C01F7/34 , C01G3/02 , C01G5/02 , C01P2004/03 , C01P2004/61 , C08F2/32 , Y02P20/544 , Y10S516/925
摘要： This invention is directed to conducting chemical reactions in reverse micelle or microemulsion systems comprising a substantially discontinuous phase including a polar fluid, typically an aqueous fluid, and a microemulsion promoter, typically a surfactant, for facilitating the formation of reverse micelles in the system. The system further includes a substantially continuous phase including a non-polar or low-polarity fluid material which is a gas under standard temperature and pressure and has a critical density, and which is generally a water-insoluble fluid in a near critical or supercritical state. Thus, the microemulsion system is maintained at a pressure and temperature such that the density of the non-polar or low-polarity fluid exceeds the critical density thereof. The method of carrying out chemical reactions generally comprises forming a first reverse micelle system including an aqueous fluid including reverse micelles in a water-insoluble fluid in the supercritical state. Then, a first reactant is introduced into the first reverse micelle system, and a chemical reaction is carried out with the first reactant to form a reaction product. In general, the first reactant can be incorporated into, and the product formed in, the reverse micelles. A second reactant can also be incorporated in the first reverse micelle system which is capable of reacting with the first reactant to form a product.

22. 发明申请

US20140296356A1 Method for Manufacturing Emulsion 审中-公开
标题翻译：制造乳液的方法
公开(公告)号：US20140296356A1
公开(公告)日：2014-10-02
申请号：US14239534
申请日：2012-06-08
申请人： Shigeru Deguchi , Nao Ifuku
发明人： Shigeru Deguchi , Nao Ifuku
IPC分类号： B01F3/08
CPC分类号： B01F3/0815 , B01F17/00 , B01F2003/0064
摘要： The disclosed invention is a method for producing an emulsion, comprising the steps of: (1) causing water and a water-insoluble substance that is to be emulsified to become freely miscible under conditions of temperature and pressure in the vicinity of the vapor-liquid critical point of water; and (2) cooling the product comprised of the water-insoluble substance and water solved each other in the presence of a surfactant to obtain a liquid comprised of the water-insoluble substance dispersed in water or a liquid comprised of water dispersed in the water-insoluble substance. The present invention provides a new method for producing emulsions with high efficiency without requiring a long period of processing or a great amount of energy.
摘要翻译：所公开的发明是一种乳液的制造方法，其特征在于，包括以下步骤：（1）使水和水不溶性物质被乳化，在气液体附近的温度和压力条件下自由混溶临界点水; 和（2）在表面活性剂存在下，将由水不溶性物质和水溶性物质组成的溶液冷却，得到由分散于水中的水不溶性物质或由水分散在水溶性物质中的水构成的液体，不溶物。本发明提供了一种在不需要长时间处理或大量能量的情况下高效率地生产乳液的新方法。

23. 发明授权

US08628802B2 Continuous process for microspheres production by using expanded fluids 失效
标题翻译：通过使用膨胀液进行微球生产的连续工艺
公开(公告)号：US08628802B2
公开(公告)日：2014-01-14
申请号：US12670852
申请日：2008-07-25
申请人： Ernesto Reverchon , Giovanna Della Porta
发明人： Ernesto Reverchon , Giovanna Della Porta
IPC分类号： A61K9/16 , B01F3/00 , B01J3/00
CPC分类号： A61K9/16 , A61K9/1635 , A61K9/1647 , A61K9/1694 , B01F3/0092 , B01F2003/0064 , B01J3/008 , B01J2203/00
摘要： The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an “expanded liquid” for the production of micro- and/or nano-particles or micro- and/or nano-spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds.The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.
摘要翻译：本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法，用于生产微米和/或纳米颗粒或微米和/或纳米球体，其中含有一种或多种更活跃的成分。特别地，通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触，或者由通过压缩CO 2膨胀的液体的外部相形成的W / O乳液或多重乳液接触。膨胀的液体形成具有乳液分散相的溶液，并提取它，诱导所需溶解化合物颗粒的形成。该方法在逆流填充塔中进行，其中从顶部进料发泡乳液，同时从底部进料膨胀的液体。由于存在膨胀的液体，避免了在包装元件上产生的固体颗粒的任何沉积，从而防止任何柱堵塞。所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

24. 发明申请

US20080274275A1 Method For Preparing Composite Fine Particles 审中-公开
标题翻译：复合微粒制备方法
公开(公告)号：US20080274275A1
公开(公告)日：2008-11-06
申请号：US11791578
申请日：2005-11-21
申请人： Kenji Mishima , Kiyoshi Matsuyama
发明人： Kenji Mishima , Kiyoshi Matsuyama
IPC分类号： B05D7/00
CPC分类号： B01J13/04 , A61K9/501 , B01F3/0853 , B01F3/088 , B01F2003/0064 , B01F2215/0404 , B01J3/008 , C08J3/122 , C08J2367/04 , C08K9/08 , Y02P20/544
摘要： A method for preparing composite microspheres of a high-molecular material and a core substance includes the steps of: dissolving a high-molecular material and dispersing a core substance in a high pressure fluid containing a supercritical fluid and an entrainer, under a shear stress of 1 Pa or more; and spraying the resultant high pressure fluid containing the high-molecular material and the core substance into a poor solvent to cause rapid expansion. According to the method composite microspheres having a uniform size of several micrometers or less, and more preferably nanometer order (a size of 1 μm or less) can be obtained.
摘要翻译：制备高分子材料和核心物质的复合微球的方法包括以下步骤：将高分子材料溶解并将核心物质分散在含有超临界流体和夹带剂的高压流体中，在剪切应力 1 Pa以上; 并将含有高分子材料和核心物质的所得高压流体喷射到不良溶剂中以引起快速膨胀。根据该方法，可以获得具有几微米或更小的均匀尺寸，更优选纳米级（1μm或更小的尺寸）的复合微球。

25. 发明申请

US20050051917A1 Devices and methods for the production of particles 失效
标题翻译：用于生产颗粒的装置和方法
公开(公告)号：US20050051917A1
公开(公告)日：2005-03-10
申请号：US10483194
申请日：2002-07-10
申请人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
发明人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
IPC分类号： B01D11/04 , B01F5/00 , B01J2/04 , B29B9/00
CPC分类号： B01J2/04 , B01D11/0403 , B01D11/0407 , B01D11/0473 , B01F5/0057 , B01F2003/0064
摘要： The present invention provides methods and devices for producing particles with an average diameter less than about 15 μm using the precipitation with compressed fluid-antisolvent (PCA) process and the carbon-dioxide assisted nebulization with a bubble dryer (CAN-BD) process. In the methods and nozzles of the invention, at least one jet of supercritical or near-supercritical fluid and at least one jet of solution interact to mix the supercritical or near-supercritical fluid and the solution within a chamber. The solution contains at least one solvent and at least one solute. At least one of the jets is a swirling jet. To form particles, the solvent and supercritical or near-supercritical fluid are then injected into a PCA or a CAN-BD process chamber. The degree of mixing depends in part on the power input into the mixing chamber. Power inputs of about 6.5×109 W/m3 enhance the degree of mixing and allow production of nanoscale particles with the PCA process. The nanoscale particles have a size distribution so that polydispersity is less than about 1.75.
摘要翻译：本发明提供了使用压缩流体 - 反溶剂（PCA）沉淀法和用气泡干燥器（CAN-BD）方法进行二氧化碳辅助雾化来生产平均直径小于约15μm的颗粒的方法和装置。在本发明的方法和喷嘴中，至少一个超临界或近超临界流体射流和至少一个溶液射流相互作用以将超临界或近超临界流体和溶液在腔室内混合。该溶液含有至少一种溶剂和至少一种溶质。至少有一架喷气式飞机是旋流式飞机。为了形成颗粒，然后将溶剂和超临界或近临界流体注入PCA或CAN-BD处理室中。混合程度部分取决于输入混合室的功率。大约6.5×10 9 W / m 3的功率输入提高了混合的程度，并允许用PCA工艺生产纳米级颗粒。纳米级颗粒具有尺寸分布，使得多分散性小于约1.75。

26. 发明授权

US06837611B2 Fluid driven agitator used in densified gas cleaning system 有权
标题翻译：用于致密气体清洁系统的流体驱动搅拌器
公开(公告)号：US06837611B2
公开(公告)日：2005-01-04
申请号：US10327850
申请日：2002-12-23
申请人： Tzu-Chen Kuo
发明人： Tzu-Chen Kuo
IPC分类号： B01F3/00 , B01F15/00 , B08B7/00 , D06F43/00 , B01F7/00 , B01F15/02
CPC分类号： D06F43/00 , B01F3/0092 , B01F15/00545 , B01F2003/0064 , B01F2003/0888 , B08B7/0021
摘要： This invention relates to a fluid driven agitator used in densified gas cleaning system, which comprises a hydraulic motor mounted to a cleaning vessel of the densified gas cleaning system, wherein the hydraulic motor comprises a fluid in-port for charging the fluid into the hydraulic motor from outside of the cleaning vessel, and a fluid out-port for discharging the fluid from the hydraulic motor out of the cleaning vessel. An output shaft of the hydraulic motor can be joined to a rotatable component, such as a rotary basket or an impeller, subjecting circulation of the fluid and resulting in stirring.

27. 发明公开

KR1020010042566A 압축된 기체 및 계면활성제중에 용해시킴으로써, 크기가마이크론 이하인 입자를 제조하는 방법 无效
标题翻译：通过将其溶解在压缩气体和表面活性剂中，从而产生尺寸不超过微米的颗粒
公开(公告)号：KR1020010042566A
公开(公告)日：2001-05-25
申请号：KR1020007011231
申请日：1999-04-06
申请人： 에프. 호프만-라 로슈 아게
发明人： 바우슈알렉산더 , 히드베르피르민
IPC分类号： A61K9/14
CPC分类号： B01F3/1214 , A61K9/14 , A61K9/145 , A61K9/1688 , B01F3/1271 , B01F5/0287 , B01F2003/0064 , B01F2003/125 , B01F2215/0032 , B01J2/04 , B01J3/008 , B01J13/02 , Y02P20/544 , Y10S977/906
摘要： 본발명은 (1) 표면개질제를함유하는압축된기체, 액체또는초임계유체중에, 또는표면개질제를임의로함유하는압축된디메틸에테르중에생물학적으로활성인화합물을승압하에용해시키는단계; (2a) 단계 (1)의압축된용액을신속하게팽창시켜용해된화합물을침전시키는단계; 또는 (2b) 단계 (1)의압축된용액을진공, 대기압또는승압하에표면개질제를임의로함유하는역용매(antisolvent)상중으로분무하는단계; 및 (3) 경우에따라, 통상적인분말가공기술을사용하여단계 (2b)의역용매상을분말상제제로전환시키는단계를포함하는, 마이크론이하의크기를갖는생물학적으로활성인화합물의분말상제제를제조하는방법에관한것이다. 본발명에따른방법에의해, 초임계용액중에용해된입자의뭉침또는응집의형성이방지되고, 또한보조용매의첨가가필요하지않아서공업적규모에서현탁액의안정성이증가된다.

28. 发明授权

US10058827B2 Method for manufacturing emulsion 有权
公开(公告)号：US10058827B2
公开(公告)日：2018-08-28
申请号：US14239534
申请日：2012-06-08
申请人： Shigeru Deguchi , Nao Ifuku
发明人： Shigeru Deguchi , Nao Ifuku
IPC分类号： B01F3/08 , B01F17/00 , B01F3/00
CPC分类号： B01F3/0815 , B01F17/00 , B01F2003/0064
摘要： The disclosed invention is a method for producing an emulsion, comprising the steps of: (1) causing water and a water-insoluble substance that is to be emulsified to become freely miscible under conditions of temperature and pressure in the vicinity of the vapor-liquid critical point of water; and (2) cooling the product comprised of the water-insoluble substance and water solved each other in the presence of a surfactant to obtain a liquid comprised of the water-insoluble substance dispersed in water or a liquid comprised of water dispersed in the water-insoluble substance. The present invention provides a new method for producing emulsions with high efficiency without requiring a long period of processing or a great amount of energy.

29. 发明授权

US09802176B2 Method for mixing in a hydrocarbon conversion process 有权
公开(公告)号：US09802176B2
公开(公告)日：2017-10-31
申请号：US14666362
申请日：2015-03-24
申请人： Saudi Arabian Oil Company
发明人： Ki-Hyouk Choi , Mohammad S. Garhoush , Bader M. Alotaibi , Mohammad A. Alabdullah
IPC分类号： B01J19/24 , C10G9/34 , B01F15/02 , B01F5/04 , B01F3/08 , C10G31/08 , B01F3/00
CPC分类号： B01J19/24 , B01F3/0865 , B01F5/0478 , B01F5/0485 , B01F15/0254 , B01F2003/0064 , B01F2015/0221 , B01F2215/0088 , B01J2219/00123 , B01J2219/24 , C10G9/34 , C10G31/08 , C10G2300/805
摘要： A sequential mixer for mixing a heated hydrocarbon stream and a supercritical fluid to produce an intimately mixed stream upstream of a supercritical reactor. The sequential mixer comprising a body having a body length and a body diameter; a hydrocarbon inlet physically connected to the body, having an inlet diameter, the heated hydrocarbon stream is introduced through the hydrocarbon inlet; a mixed stream outlet physically connected to the body and fluidly connected to the supercritical reactor, having an outlet diameter; a traversing axis extending through the center of the body from the hydrocarbon inlet to the mixed stream outlet; and a plurality of fluid ports physically connected to the body, the plurality of fluid ports are arranged in a port alignment arrayed along the traversing axis, each fluid port has a port diameter and a port angle, the supercritical fluid is injected through the plurality of fluid ports.

30. 发明授权

US07621993B2 Method for producing pigment dispersion and pigment dispersion producing apparatus 失效
标题翻译：颜料分散体和颜料分散体制造装置的制造方法
公开(公告)号：US07621993B2
公开(公告)日：2009-11-24
申请号：US11260893
申请日：2005-10-27
申请人： Takayuki Teshima , Shoji Ihara , Kenji Yamada , Yukio Hanyu
发明人： Takayuki Teshima , Shoji Ihara , Kenji Yamada , Yukio Hanyu
IPC分类号： C09D17/00 , C09D11/00 , B05D1/02
CPC分类号： C09C3/08 , B01F3/1214 , B01F5/045 , B01F13/0059 , B01F2003/0064 , B01J3/008 , B01J19/0093 , B01J2219/00873 , B01J2219/00891 , C01P2002/80 , C01P2004/64 , C09B67/0014 , C09B67/0091 , C09C1/00 , Y02P20/544
摘要： A method for producing a pigment dispersion, including the steps of: preparing a fluid in a supercritical or subcritical state in which a pigment is dissolved; and introducing into a microreactor the fluid in a supercritical or subcritical state in which the pigment is dissolved and a solution containing a dispersant for dispersing the pigment in a dispersing medium, precipitating the pigment in the microreactor, and dispersing the precipitated pigment in the dispersing medium using the dispersant.
摘要翻译：一种制备颜料分散体的方法，包括以下步骤：制备其中溶解颜料的超临界或亚临界状态的流体; 在微反应器中将颜料溶解在超临界或亚临界状态的液体和含有分散剂的溶液引入到分散介质中，使颜料沉淀在微反应器中，并将沉淀的颜料分散在分散介质中使用分散剂。

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