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21. 发明授权

US06951956B2 Crystalline polyglycolic acid, polyglycolic acid composition and production process thereof 有权
标题翻译：结晶聚乙醇酸，聚乙醇酸组合物及其制备方法
公开(公告)号：US06951956B2
公开(公告)日：2005-10-04
申请号：US10132578
申请日：2002-04-25
申请人： Kazuyuki Yamane , Hiromitsu Miura , Toshihiko Ono , Junji Nakajima , Daisuki Itoh
发明人： Kazuyuki Yamane , Hiromitsu Miura , Toshihiko Ono , Junji Nakajima , Daisuki Itoh
IPC分类号： B29C49/00 , B65D1/02 , C07C59/10 , C08G63/08 , C08G63/80 , C08G63/88 , C08K5/49 , C08K5/527
CPC分类号： C08G63/08 , C08G63/80 , C08G63/88 , C08K5/527 , C08L67/04
摘要： Crystalline polyglycolic acid wherein a difference between the melting point Tm and the crystallization temperature Tc2 is not lower than 35° C., and a difference between the crystallization temperature Tc1 and the glass transition temperature Tg is not lower than 40° C. A production process of polyglycolic acid modified in crystallinity, comprising applying heat history to crystalline polyglycolic acid at a temperature of not lower than (the melting point Tm of the crystalline polyglycolic acid+38° C.). A polyglycolic acid composition comprising crystalline polyglycolic acid and a heat stabilizer, wherein a difference (T2−T1) between the temperature T2 at 3%-weight loss on heating of the polyglycolic acid composition and the temperature T1 at 3%-weight loss on heating of the crystalline polyglycolic acid is not lower than 5° C.
摘要翻译：其中熔点Tm和结晶温度Tc 2之差的结晶聚乙醇酸不低于35℃，结晶温度Tc 1和玻璃化转变温度Tg不低于40℃。结晶度改性的聚乙醇酸的制备方法包括在不低于（结晶聚乙醇酸+ 38的熔点Tm）的温度下对结晶聚乙醇酸施加热历史 C。）。一种包含结晶聚乙醇酸和热稳定剂的聚乙醇酸组合物，其中温度T 2℃之间的差异（T 2 2 -T 1 H 2）在聚乙醇酸组合物加热时3％重量损失和结晶聚乙醇酸加热时3％重量损失温度T 1不低于5℃。

22. 发明授权

US06916939B2 Process for the preparation of cyclic esters and method for purification of the same 有权
标题翻译：环酯的制备方法及其纯化方法
公开(公告)号：US06916939B2
公开(公告)日：2005-07-12
申请号：US10344461
申请日：2001-08-08
申请人： Kazuyuki Yamane , Yukichika Kawakami , Hajime Hoshi , Kazuhiko Sunagawa
发明人： Kazuyuki Yamane , Yukichika Kawakami , Hajime Hoshi , Kazuhiko Sunagawa
IPC分类号： C07D319/12
CPC分类号： C08J3/28 , C07D319/12 , C08J11/24 , C08J2300/14 , C08J2367/04 , Y02W30/706
摘要： The present invention provides a process for production of a cyclic ester by depolymerization of an aliphatic polyester. In the process, a mixture containing the aliphatic polyester and a specific polyalkylene glycol ether, which has a boiling point of 230-450° C. and a molecular weight of 150-450, is heated under normal or reduced pressure to a temperature at which depolymerization of the aliphatic polyester takes place. Then, a substantially homogeneous solution phase, consisting of the melt phase of the aliphatic polyester and the liquid phase of the polyalkylene glycol ether, is formed. Heating of the solution phase is continued to form the cyclic ester by depolymerization and distil out the cyclic ester together with the polyalkylene glycol ether, and then the cyclic ester is recovered from the distillate. The present invention also provides a process for purification of a crude cyclic ester by use of the specific polyalkylene glycol ether described above.
摘要翻译：本发明提供了通过脂肪族聚酯的解聚制备环状酯的方法。在该方法中，将含有脂族聚酯和特定的聚亚烷基二醇醚的混合物在沸点为230-450℃，分子量为150-450的条件下，在正常或减压下加热至发生脂肪族聚酯的解聚。然后，形成由脂肪族聚酯的熔融相和聚亚烷基二醇醚的液相组成的基本均匀的溶液相。溶液相的加热继续通过解聚形成环酯，并与聚亚烷基二醇醚一起蒸馏出环状酯，然后从馏出物中回收环状酯。本发明还提供了通过使用上述特定的聚亚烷基二醇醚来纯化粗环酯的方法。

23. 发明授权

US06852827B2 Polyester production process and reactor apparatus 失效
标题翻译：聚酯生产工艺和反应器设备
公开(公告)号：US06852827B2
公开(公告)日：2005-02-08
申请号：US10476117
申请日：2002-07-05
申请人： Kazuyuki Yamane , Yukichika Kawakami , Hiroyuki Sato , Tomohiro Hoshi
发明人： Kazuyuki Yamane , Yukichika Kawakami , Hiroyuki Sato , Tomohiro Hoshi
IPC分类号： C08G63/89 , B01J19/02 , B01J19/24 , C08G63/08 , C08G63/78 , C08G63/02
CPC分类号： B01J19/24 , B01J19/02 , B01J19/2415 , B01J2219/0236 , B01J2219/1943 , B01J2219/1946 , C08G63/08 , C08G63/78 , C08G63/785 , C08G63/89
摘要： The invention provides a polyester production process by bulk polymerization in a reactor, wherein the volume of the resulting polyester is shrunk for a release from the inner surface of the reactor, so that the polyester can be recovered in the form of a bulky mass. The invention also provides a reactor for bulk polymerization for polyester, which comprises an inner surface that enabling the resulting polyester to be released therefrom upon its volume shrinkage.
摘要翻译：本发明提供了在反应器中本体聚合的聚酯制造方法，其中所得聚酯的体积收缩以从反应器的内表面释放，使得聚酯可以以体积质量的形式回收。本发明还提供了一种用于聚酯的本体聚合反应器，其包括使得所得聚酯在其体积收缩时能够从其中释放的内表面。

24. 发明申请

US20120178870A1 AROMATIC POLYESTER RESIN COMPOSITION 审中-公开
标题翻译：芳香聚酯树脂组合物
公开(公告)号：US20120178870A1
公开(公告)日：2012-07-12
申请号：US13429837
申请日：2012-03-26
申请人： Hiroyuki SATO , Kazuyuki Yamane , Yuki Hokari , Fuminori Kobayashi
发明人： Hiroyuki SATO , Kazuyuki Yamane , Yuki Hokari , Fuminori Kobayashi
IPC分类号： C08L67/00
CPC分类号： C08L67/02 , C08K5/29 , C08K5/521 , C08K2201/008 , C08L67/04 , C08L2666/18
摘要： An aromatic polyester resin composition, comprising: a melt-kneaded product of 99-70 wt. parts of an aromatic polyester resin and 1-30 wt. parts (providing a total of 100 wt. parts together with the aromatic polyester resin) of a polyglycolic acid resin, wherein the aromatic polyester resin is an aromatic polyester resin polymerized with an antimony compound (catalyst), the polyglycolic acid resin is a polyglycolic acid resin obtained by ring-opening polymerization of glycolide, and the composition further contains a metal-deactivating agent in a proportion of 17-500 mol. % with respect to the antimony in the aromatic polyester resin. As a result, gas generation during the melt-processing of a composition obtained by adding a relatively small amount of polyglycolic acid resin to an aromatic polyester resin is effectively suppressed to provide an aromatic polyester resin composition with a good gas-barrier property.
摘要翻译：一种芳族聚酯树脂组合物，其包含：99-70重量份的熔融捏合产物，部分芳族聚酯树脂和1-30wt。聚乙醇酸树脂的部分（与芳族聚酯树脂一起共提供100重量份），其中芳族聚酯树脂是用锑化合物（催化剂）聚合的芳族聚酯树脂，聚乙醇酸树脂是聚乙醇酸通过乙交酯的开环聚合获得的树脂，并且该组合物还含有比例为17-500mol的金属钝化剂。相对于芳族聚酯树脂中的锑。结果，通过将相对少量的聚乙醇酸树脂加入到芳族聚酯树脂中而获得的组合物进行熔融加工时的气体产生被有效地抑制，从而提供具有良好阻气性的芳族聚酯树脂组合物。

25. 发明授权

US08163866B2 Aromatic polyester resin composition 有权
标题翻译：芳香族聚酯树脂组合物
公开(公告)号：US08163866B2
公开(公告)日：2012-04-24
申请号：US12449093
申请日：2008-01-22
申请人： Hiroyuki Sato , Kazuyuki Yamane , Yuki Hokari , Fuminori Kobayashi
发明人： Hiroyuki Sato , Kazuyuki Yamane , Yuki Hokari , Fuminori Kobayashi
IPC分类号： C08G63/86 , C08G63/06 , C08K5/22 , C08K5/49
CPC分类号： C08L67/02 , C08K5/0091 , C08K2201/008 , C08L67/04 , C08L2666/18
摘要： An aromatic polyester resin composition, including: a melt-kneaded product of 99-70 wt. parts of an aromatic polyester resin and 1-30 wt. parts (providing a total of 100 wt. parts together with the aromatic polyester resin) of a polyglycolic acid resin, wherein the aromatic polyester resin is an aromatic polyester resin polymerized with a germanium compound (catalyst), and the polyglycolic acid resin is a polyglycolic acid resin obtained by ring-opening polymerization of glycolide. As a result, gas generation during the melt-processing of a composition obtained by adding a relatively small amount of polyglycolic acid resin to an aromatic polyester resin is effectively suppressed to provide an aromatic polyester resin composition with a good gas-barrier property.
摘要翻译：一种芳族聚酯树脂组合物，包括：99-70重量份的熔融捏合产物，部分芳族聚酯树脂和1-30wt。聚乙醇酸树脂的部分（与芳族聚酯树脂一起共提供100重量份），其中芳族聚酯树脂是用锗化合物（催化剂）聚合的芳族聚酯树脂，聚乙醇酸树脂是聚乙醇酸由乙交酯开环聚合得到的酸性树脂。结果，通过将相对少量的聚乙醇酸树脂加入到芳族聚酯树脂中而获得的组合物进行熔融加工时的气体产生被有效地抑制，从而提供具有良好阻气性的芳族聚酯树脂组合物。

26. 发明申请

US20110263875A1 Production Process of Glycolide 有权
标题翻译：乙交酯的生产工艺
公开(公告)号：US20110263875A1
公开(公告)日：2011-10-27
申请号：US13142012
申请日：2009-12-09
申请人： Shigeru Suzuki , Kazuyuki Yamane , Toshihiko Ono , Kazuhiko Sunagawa
发明人： Shigeru Suzuki , Kazuyuki Yamane , Toshihiko Ono , Kazuhiko Sunagawa
IPC分类号： C07D319/12
CPC分类号： C07D319/12
摘要： The invention provides a production process of glycolide comprising the respective steps of: Step 1 of heating a mixture containing a glycolic acid oligomer and a high boiling polar organic under normal or reduced pressure to reflux the mixture and at that time, conducting a total reflux operation in a reflux time within a range of 0.1 to 20 hours under conditions that substantially the whole amount of a distillate distilled out of a reflux system containing the mixture is refluxed into the reflux system; Step 2 of heating the mixture after the total reflux operation or a mixture obtained by adding the high boiling polar organic solvent to a glycolic acid oligomer component recovered from the mixture after the total reflux operation to conduct depolymerization; and Step 3 of collecting glycolide from a co-distillate.
摘要翻译：本发明提供了一种乙交酯的制备方法，其包括以下各步骤：步骤1，在正常或减压下加热含有乙醇酸低聚物和高沸点极性有机物的混合物以回流混合物，并且此时进行总的回流操作在从含有该混合物的回流系统蒸馏出的基本上全部量的馏出物回流至回流系统的条件下，在0.1至20小时的范围内的回流时间内，在全部回流操作之后加热混合物的步骤2或通过在完全回流操作后从混合物中回收的乙醇酸低聚物组分加入高沸点极性有机溶剂而获得的混合物进行解聚; 和从共馏出物收集乙交酯的步骤3。

27. 发明申请

US20110045235A1 METHOD FOR MANUFACTURING POROUS POLYMER MOLDED ARTICLE 审中-公开
标题翻译：制造多孔聚合物成型品的方法
公开(公告)号：US20110045235A1
公开(公告)日：2011-02-24
申请号：US12744025
申请日：2008-10-15
申请人： Kazuyuki Yamane , Yuki Hokari , Toshihiko Ono , Takeshi Saitou
发明人： Kazuyuki Yamane , Yuki Hokari , Toshihiko Ono , Takeshi Saitou
IPC分类号： C08J9/00 , B32B38/10 , B32B3/24
CPC分类号： B01D67/0034 , B01D67/0023 , B01D71/48 , B01D2323/42 , B29C67/20 , Y10T428/24273
摘要： A method for manufacturing a porous polymer molded article, comprising a step of laminating a first mask with a plurality of openings formed therein and a second mask with a plurality of openings formed therein and having a mean opening diameter that is larger than the mean opening diameter of the first mask, on a polymer molded article, and a step of forming through-holes in the polymer molded article by dry etching from the second mask side.
摘要翻译：一种多孔聚合物成型体的制造方法，其特征在于，包括将形成有多个开口的第一掩模层压的步骤和形成有多个开口的第二掩模，所述第二掩模的平均开口直径大于平均开口直径的第一掩模，聚合物成型体，以及通过从第二掩模侧的干蚀刻在聚合物成型体中形成贯通孔的工序。

28. 发明授权

US07799837B2 Bottle excellent in recyclability and method for recycling the bottle 失效
标题翻译：瓶子具有优异的可回收性和回收瓶子的方法
公开(公告)号：US07799837B2
公开(公告)日：2010-09-21
申请号：US12232365
申请日：2008-09-16
申请人： Kazuyuki Yamane , Ryo Kato , Hiroyuki Sato
发明人： Kazuyuki Yamane , Ryo Kato , Hiroyuki Sato
IPC分类号： C08J11/16
CPC分类号： B32B27/08 , B29B17/02 , B29B17/04 , B29B2017/0289 , B29B2017/0293 , B29B2017/0436 , B29K2003/00 , B29K2067/043 , B29K2067/046 , B29K2667/043 , B29L2031/712 , B29L2031/7158 , B32B27/36 , B32B2307/402 , B32B2439/60 , B65D1/0215 , B65D2565/385 , C08J11/14 , C08J2367/04 , Y02P20/582 , Y02W30/622 , Y02W30/625 , Y02W30/704 , Y10T428/1352
摘要： There are provided a bottle which has a laminate structure including a glycolic acid polymer layer showing good gas-barrier property in addition to a principal resin layer and is yet provided with excellent recyclability, and also an efficient method of recycling the bottle. More specifically, a bottle having a laminate structure including at least one layer of glycolic acid polymer in addition to a principal resin layer, is obtained. After breaking the bottle, the broken pieces are washed with alkaline water, water or acidic water to remove the glycolic acid polymer layer, thereby recovering the principal resin.
摘要翻译：提供了一种具有层叠结构的瓶子，除了主树脂层之外还具有显示出良好的阻气性的乙醇酸聚合物层，并且还具有优异的可再循环性，并且还具有回收瓶子的有效方法。更具体地，获得具有包括至少一层乙醇酸聚合物的主层树脂层的层压结构的瓶子。破瓶后，用碱性水，水或酸性水洗涤破碎片，除去乙醇酸聚合物层，从而回收主树脂。

29. 发明授权

US07785682B2 Multilayer sheet made of polyglycolic acid resin 失效
标题翻译：由聚乙醇酸树脂制成的多层板
公开(公告)号：US07785682B2
公开(公告)日：2010-08-31
申请号：US11630255
申请日：2005-06-20
申请人： Takashi Sato , Kazuyuki Yamane , Juichi Wakabayashi , Tomoaki Sato , Takehisa Suzuki
发明人： Takashi Sato , Kazuyuki Yamane , Juichi Wakabayashi , Tomoaki Sato , Takehisa Suzuki
IPC分类号： B27M3/00 , B27N5/02
CPC分类号： B32B9/02 , B32B7/12 , B32B9/045 , B32B27/36 , B32B2307/7163 , B32B2439/70 , B65D65/466 , Y02A40/961 , Y02W90/13 , Y10T428/1303 , Y10T428/1334 , Y10T428/1338 , Y10T428/1348 , Y10T428/1352
摘要： A polyglycolic acid resin-based multilayer sheet, comprising: a plant substrate sheet and a biodegradable resin layer laminated by melt-adhesion onto the plant substrate sheet, wherein said biodegradable resin layer comprises one or plural layer including at least a polyglycolic acid resin layer, and the multilayer sheet includes on the substrate sheet a melt-adhesion layer comprising a biodegradable resin exhibiting a melt viscosity of 10-5.0×103 Pa·sec as measured at a temperature of 240° C. and a shear speed of 122 sec−1 and having a melting point of at most 235° C. The multilayer sheet has a laminate structure composed of biodegradable materials exerting little load to the environment at the time of disposable thereof and yet is excellent in oxygen-barrier property and moisture resistance, thus being suitable as a food container-forming material.
摘要翻译：一种聚乙醇酸树脂系多层片材，其特征在于，具有：植物基片和通过熔融粘合层叠在所述植物基片上的生物降解性树脂层，其中，所述生物降解性树脂层包含至少包含聚乙醇酸树脂层的一层或多层，并且所述多层片材在所述基材片材上包含熔融粘合层，所述熔融粘合层包含在240℃的温度下测定的熔融粘度为10-5.0×103Pa·sec的剪切速度和122秒-1的剪切速度的生物降解性树脂熔点为235℃以下。多层片材具有由一次性使用时对环境几乎没有负载的生物降解性材料构成的层压结构，但是具有优异的阻氧性和耐湿性，因此，适合作为食品容器形成材料。

30. 发明申请

US20100148391A1 Filament of polyglycolic acid resin and process for producing the same 有权
标题翻译：聚乙醇酸树脂的丝及其制造方法
公开(公告)号：US20100148391A1
公开(公告)日：2010-06-17
申请号：US12656810
申请日：2010-02-17
申请人： Satoshi Hashimoto , Kazuyuki Yamane , Juichi Wakabayashi , Hirokazu Matsui
发明人： Satoshi Hashimoto , Kazuyuki Yamane , Juichi Wakabayashi , Hirokazu Matsui
IPC分类号： D01D5/088
CPC分类号： D01F6/625 , D01D5/0885 , D01D5/12 , D02G3/444 , D02J1/22 , D02J1/223 , D02J1/228
摘要： A biodegradable filament of polyglycolic acid resin having practical properties represented by high tensile strength and knot strength is produced. A polyglycolic acid resin having a residual monomer content of below 0.5 wt. % is melt-spun, quenched in a liquid bath of at most 10° C. and then stretched in a liquid bath of 60-83° C. to produce a polyglycolic acid resin filament having a tensile strength of at least 750 MPa and a knot strength of at least 600 MPa.
摘要翻译：制造具有高拉伸强度和结强度代表的实用性能的聚乙醇酸树脂的生物可降解长丝。残留单体含量低于0.5重量％的聚乙醇酸树脂％熔体纺丝，在至多10℃的液槽中淬火，然后在60-83℃的液浴中拉伸，得到拉伸强度为至少750MPa的聚乙醇酸树脂长丝和结强度至少为600MPa。

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