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21. 发明授权

US08242198B2 Polyolefin adhesive compositions 有权
标题翻译：聚烯烃粘合剂组合物
公开(公告)号：US08242198B2
公开(公告)日：2012-08-14
申请号：US12616637
申请日：2009-11-11
申请人： Peijun Jiang , George Rodriguez , Fran A. Shipley , Aspy K. Mehta
发明人： Peijun Jiang , George Rodriguez , Fran A. Shipley , Aspy K. Mehta
IPC分类号： D21H19/18
CPC分类号： C09J5/06 , C08L23/02 , C08L23/06 , C08L51/003 , C08L51/06 , C08L91/06 , C08L2666/02 , C09J123/142
摘要： An adhesive and method for hot melt application. The adhesive comprises polyolefin base polymer, from 1 to 10 wt % of at least one functionalized polyolefin, and from 1 to 15 wt % of a wax, based on the total weight of the polyolefin base polymer, functionalized polyolefin and wax, wherein the wax has a weight average molecular weight at least 8% of the weight average molecular weight of the polyolefin base polymer, viscosity at 190° C. of 60 mPa·s or more, and a crystallization temperature greater than the polyolefin base polymer and greater than 100° C., and wherein the adhesive has at least 5% fiber tear at 2° C., at least 50% fiber tear at 25° C., and a characteristic set time of less than 3 seconds.
摘要翻译：一种用于热熔胶应用的粘合剂和方法。基于聚烯烃基础聚合物，官能化聚烯烃和蜡的总重量，粘合剂包括聚烯烃基聚合物，1至10重量％的至少一种官能化聚烯烃和1至15重量％的蜡，其中蜡重均分子量为聚烯烃基聚合物的重均分子量的至少8％，190℃下的粘度为60mPa·s以上，结晶温度大于聚烯烃基聚合物，大于100 ℃，并且其中粘合剂在2℃下具有至少5％的纤维撕裂，在25℃下至少50％的纤维撕裂，以及小于3秒的特征设定时间。

22. 发明授权

US08106127B2 Heterogeneous in-reactor polymer blends 有权
标题翻译：不均匀的反应器内聚合物共混物
公开(公告)号：US08106127B2
公开(公告)日：2012-01-31
申请号：US12638861
申请日：2009-12-15
申请人： Carlos U. De Gracia , Kevin R. Squire , Peijun Jiang , Armenag H. Dekmezian , Beverly J. Poole , Cesar A. Garcia-Franco
发明人： Carlos U. De Gracia , Kevin R. Squire , Peijun Jiang , Armenag H. Dekmezian , Beverly J. Poole , Cesar A. Garcia-Franco
IPC分类号： C08F8/00 , C08L23/04 , C08L23/10 , C08K5/00
CPC分类号： C08L23/16 , C08L23/12 , C08L2314/06 , C08L2666/06
摘要： An in-reactor polymer blend comprises (a) a propylene-containing first polymer; and (b) an ethylene-containing second polymer such that the polymer blend comprises between about 50 wt % and about 80 wt % units derived from ethylene and between about 50 wt % and about 20 wt % units derived from propylene. The blend is substantially free of dienes and the content of ethylene in the second polymer in the form of ethylene-ethylene-ethylene triads is at least 40%. The second polymer contains at least 0.1 branch having 8 or more carbon atoms per 10,000 carbons. In addition, the blend has a strain hardening index of at least 1.8, a shear thinning slope in the plot of log(dynamic viscosity) versus log(frequency) of less than −0.2 and exhibits at least two peaks when subjected to Differential Scanning Calorimetry (first melt) corresponding to a first melting point of at least 150° C. and a second melting point of at least 40° C. such that the difference between the first and second melting temperatures is at least 20° C.
摘要翻译：反应器内聚合物共混物包含（a）含丙烯的第一聚合物; 和（b）含乙烯的第二聚合物，使得聚合物共混物包含衍生自乙烯的约50重量％至约80重量％的单元和衍生自丙烯的约50重量％至约20重量％的单元。共混物基本上不含二烯，乙烯 - 乙烯 - 乙烯三单元组形式的第二聚合物中的乙烯含量至少为40％。第二聚合物含有至少0.1个分支，每10,000个碳原子具有8个或更多个碳原子。此外，共混物的应变硬化指数为至少1.8，对数（动态粘度）对log（频率）的曲线图中的剪切变稀斜率小于-0.2，并且当进行差示扫描量热法时显示出至少两个峰（第一熔体），其对应于至少150℃的第一熔点和至少40℃的第二熔点，使得第一和第二熔融温度之间的差异为至少20℃。

23. 发明授权

US08093335B2 Thermoplastic polyolefin in-reactor blends and molded articles therefrom 有权
标题翻译：热塑性聚烯烃反应器内共混物及其模塑制品
公开(公告)号：US08093335B2
公开(公告)日：2012-01-10
申请号：US12638843
申请日：2009-12-15
申请人： Peijun Jiang , Armenag H. Dekmezian , Joseph Gustaaf M. Flendrig
发明人： Peijun Jiang , Armenag H. Dekmezian , Joseph Gustaaf M. Flendrig
IPC分类号： C08F8/00 , C08L23/00 , C08L23/04
CPC分类号： C08L23/12 , C08L23/14 , C08L2205/02 , C08L2314/06 , C08L2666/06
摘要： This invention relates to a molded article comprising an in-reactor polymer blend comprising: (a) a first propylene polymer comprising 90 to 100 wt % propylene and from 0 to less than 10 wt % comonomer, said first propylene component having a Tm of 135° C. or more; and (b) a second propylene polymer comprising from 30 to 90 wt % propylene and 70 to 10 wt % comonomer, said second propylene polymer having an Mw of 30,000 g/mol or more, and said second propylene-containing polymer having a crystallinity different by at least 5% from the first polymer, wherein the polymer blend has: (a) a Tm of at least 135° C., (b) a melt flow rate of at least 70 dg/min, (c) a tensile strength of at least 8 MPa, (d) an elongation at break of at least 200%, (e) a tensile strength at break of 10 MPa or more, and (f) a GME 60280 scratch resistance of less than 1.2 DL at a scratching load of 5 Newtons.
摘要翻译：本发明涉及包含反应器内聚合物共混物的模制品，其包含：（a）包含90至100重量％丙烯和0至小于10重量％共聚单体的第一丙烯聚合物，所述第一丙烯组分的Tm为135 ℃以上; 和（b）第二丙烯聚合物，其包含30至90重量％的丙烯和70至10重量％的共聚单体，所述第二丙烯聚合物的Mw为30,000g / mol或更高，并且所述第二丙烯聚合物具有不同的结晶度与第一聚合物相比至少5％，其中聚合物共混物具有：（a）Tm至少为135℃，（b）熔体流动速率至少为70dg / min，（c）拉伸强度至少8MPa，（d）断裂伸长率至少为200％，（e）断裂时的拉伸强度为10MPa以上，（f）在刮擦时GME 60280耐擦伤性小于1.2DL 负荷5牛顿。

24. 发明授权

US08022142B2 Thermoplastic olefin compositions 有权
标题翻译：热塑性烯烃组合物
公开(公告)号：US08022142B2
公开(公告)日：2011-09-20
申请号：US12335252
申请日：2008-12-15
申请人： Peijun Jiang , Armenag H. Dekmezian , Kevin R. Squire , Carlos U. de Gracia , Keith Edward Jolibois , Cesar A. Garcia-Franco , Ronald Raymond Thackston
发明人： Peijun Jiang , Armenag H. Dekmezian , Kevin R. Squire , Carlos U. de Gracia , Keith Edward Jolibois , Cesar A. Garcia-Franco , Ronald Raymond Thackston
IPC分类号： C08L23/04 , C08L23/10
CPC分类号： C08L23/16 , C08F10/06 , C08F210/06 , C08L23/12 , C08L2205/02 , C08L2207/02 , C08L2207/07 , C08L2308/00 , C08L2314/06 , C08F2/001 , C08F210/16 , C08F2500/04 , C08F2500/11 , C08F2500/12 , C08F2500/17 , C08F2500/18 , C08F2500/20
摘要： An in-reactor polymer blend including (a) a propylene-containing first polymer; and (b) propylene-containing second polymer having a different crystallinity from the first polymer. The polymer blend has a melting temperature, Tm, of at least 135° C., a melt flow rate of at least 70 dg/min, a tensile strength of at least 8 MPa, an elongation at break of at least 300%.
摘要翻译：一种反应器内聚合物共混物，包括（a）含丙烯的第一聚合物; 和（b）与第一聚合物具有不同结晶度的含丙烯的第二聚合物。聚合物共混物具有至少135℃的熔融温度Tm，至少70dg / min的熔体流动速率，至少8MPa的拉伸强度，至少300％的断裂伸长率。

25. 发明申请

US20110169199A1 Process For Preparing Articles 有权
标题翻译：准备文章的过程
公开(公告)号：US20110169199A1
公开(公告)日：2011-07-14
申请号：US13069721
申请日：2011-03-23
申请人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
发明人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
IPC分类号： B29C47/14 , C08J3/24 , B29C49/00
CPC分类号： B29C43/003 , C08L21/00 , C08L23/04 , C08L23/10 , C08L23/16 , C08L61/06 , C08L67/00 , C08L69/00 , C08L2312/04 , C08L2666/06 , C08L2666/08 , C08L2666/02
摘要： The present invention relates to a process for preparing a thermoplastic vulcanizate (TPV) comprising: contacting a thermoplastic polymer, a cross-linkable elastomer, at least one curative, and at least one cure activator in a solvent to form Composition A. The solvent is then removed, and thereafter the cross-linkable elastomer is at least partially cured. The average particle size of the cross-linkable elastomer is 10 microns or less after the solvent is removed.
摘要翻译：本发明涉及一种制备热塑性硫化橡胶（TPV）的方法，包括：使热塑性聚合物，可交联弹性体，至少一种固化剂和至少一种固化活化剂在溶剂中接触以形成组合物A.溶剂是然后除去，然后可交联弹性体至少部分固化。除去溶剂后，可交联弹性体的平均粒径为10微米以下。

26. 发明授权

US07935761B2 Process for preparing articles 失效
标题翻译：制备文章的过程
公开(公告)号：US07935761B2
公开(公告)日：2011-05-03
申请号：US11787855
申请日：2007-04-18
申请人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
发明人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
IPC分类号： C08F8/00 , C08J3/00 , C08L9/00 , C08L23/04 , C08L23/10 , C08L29/00 , C08L33/00 , C08L35/00 , C08L45/00
CPC分类号： B29C43/003 , C08L21/00 , C08L23/04 , C08L23/10 , C08L23/16 , C08L61/06 , C08L67/00 , C08L69/00 , C08L2312/04 , C08L2666/06 , C08L2666/08 , C08L2666/02
摘要： The present invention relates to a process for preparing a thermoplastic vulcanizate (TPV) comprising: contacting a thermoplastic polymer, a cross-linkable elastomer, at least one curative, and at least one cure activator in a solvent to form Composition A. The solvent is then removed, and thereafter the cross-linkable elastomer is at least partially cured. The average particle size of the cross-linkable elastomer is 10 microns or less after the solvent is removed.
摘要翻译：本发明涉及一种制备热塑性硫化橡胶（TPV）的方法，包括：使热塑性聚合物，可交联弹性体，至少一种固化剂和至少一种固化活化剂在溶剂中接触以形成组合物A.溶剂是然后除去，然后可交联弹性体至少部分固化。除去溶剂后，可交联弹性体的平均粒径为10微米以下。

27. 发明授权

US07935760B2 Process of making a heterogeneous polymer blend 失效
标题翻译：制造非均相聚合物共混物的方法
公开(公告)号：US07935760B2
公开(公告)日：2011-05-03
申请号：US11296830
申请日：2005-12-07
申请人： Peijun Jiang , Aspy K. Mehta , Armenag H. Dekmezian , Sunny Jacob , Andrew G. Narvaez , Pradeep P. Shirodkar
发明人： Peijun Jiang , Aspy K. Mehta , Armenag H. Dekmezian , Sunny Jacob , Andrew G. Narvaez , Pradeep P. Shirodkar
IPC分类号： C08L23/00 , C08L23/04
CPC分类号： C08L23/10 , C08F110/06 , C08F210/06 , C08L23/145 , C08L2308/00 , C08L2312/00 , C08L2312/02 , C08L2314/06 , C08F2/001 , C08L2666/06 , C08F210/18 , C08F236/20 , C08F2500/20
摘要： In a process for producing a heterogeneous polymer blend, at least one first monomer is polymerized in a first reaction zone in the presence of a supported catalyst to produce a thermoplastic first polymer having a crystallinity of at least 30%. At least part of said first polymer is then contacted with at least one second monomer and at least one polyene in a second reaction zone under conditions sufficient to polymerize said second monomer to produce a second polymer having a crystallinity of less than 20%. The second polymer is at least partially cross-linked in the second reaction zone such that at least a fraction of the second polymer is insoluble in xylene and such that the first and second polymers form different phases of the blend.
摘要翻译：在制备非均相聚合物共混物的方法中，至少一种第一单体在负载型催化剂的存在下在第一反应区中聚合以产生具有至少30％的结晶度的热塑性第一聚合物。然后在足以使所述第二单体聚合以产生结晶度小于20％的第二聚合物的条件下，将至少部分所述第一聚合物与至少一种第二单体和至少一种多烯在第二反应区中接触。第二聚合物在第二反应区域中至少部分交联，使得至少一部分第二聚合物不溶于二甲苯并使得第一和第二聚合物形成共混物的不同相。

28. 发明申请

US20100152383A1 Thermoplastic Elastomer Polyolefin In-Reactor Blends And Molded Articles Therefrom 有权
标题翻译：热塑性弹性体聚烯烃反应器共混物和成型制品
公开(公告)号：US20100152383A1
公开(公告)日：2010-06-17
申请号：US12638916
申请日：2009-12-15
申请人： Peijun Jiang , Armenag H. Dekmezian , Kevin R. Squire , Cesar A. Garcia-Franco
发明人： Peijun Jiang , Armenag H. Dekmezian , Kevin R. Squire , Cesar A. Garcia-Franco
IPC分类号： C08L23/04
CPC分类号： C08L23/06 , C08L23/08 , C08L2205/02 , C08L2314/06 , C08L2666/06
摘要： This invention relates to an in-reactor polymer blend comprising: (a) a first ethylene-containing polymer having a density of greater than 0.90 g/cm3 and a Mw of more than 20,000 g/mol and (b) a second ethylene-containing polymer having a density of less than 0.90 g/cm3, wherein the polymer blend has a Tm of at least 90° C. (DSC second melt), a density of less than 0.92 g/cm3, and the densities of the first and second polymers differ by at least 1%. Specifically this invention relates to an in-reactor polymer blend comprising: (a) a first ethylene polymer comprising 90 to 100 wt % ethylene and from 0 to less than 10 wt % comonomer, said first ethylene polymer component having density of greater than 0.920 g/cm3, an Mw of 20,000 g/mol or more; and (b) a second ethylene polymer comprising from 70 to 90 wt % ethylene and 30 to 10 wt % comonomer, said second ethylene polymer having a density of 0.910 g/cm3 or less, wherein the polymer blend has: (a) a Tm of at least 100° C. over a density ranging from 0.84 to 0.92 g/cm3; (b) a elongation at break of 300% or more; (c) a strain hardening index M300/M100 of at least 1.2; (d) a ratio of complex viscosity at 0.01 rad/s to the viscosity at 100 rad/s is of at least 30; and (e) a shear thinning slope of the plot of log(dynamic viscosity) versus log(frequency) less than −0.2.
摘要翻译：本发明涉及一种反应器内聚合物共混物，其包含：（a）密度大于0.90g / cm 3，Mw大于20,000g / mol的第一含乙烯聚合物和（b）第二含乙烯的聚合物聚合物的密度小于0.90g / cm 3，其中聚合物共混物具有至少90℃的Tm（DSC第二熔体），密度小于0.92g / cm 3，第一和第二密度聚合物的差异至少为1％。具体而言，本发明涉及一种反应器内聚合物共混物，其包含：（a）包含90至100重量％乙烯和0至小于10重量％共聚单体的第一乙烯聚合物，所述第一乙烯聚合物组分的密度大于0.920g / cm3，Mw为20,000g / mol以上; 和（b）包含70-90wt％乙烯和30-10wt％共聚单体的第二乙烯聚合物，所述第二乙烯聚合物的密度为0.910g / cm 3或更低，其中所述聚合物共混物具有：（a）Tm 至少100℃，密度范围为0.84至0.92g / cm 3; （b）断裂伸长率在300％以上; （c）至少为1.2的应变硬化指数M300 / M100; （d）0.01rad / s下的复数粘度与100rad / s下的粘度之比至少为30; 和（e）对数（动态粘度）对log（频率）小于-0.2的曲线的剪切变薄斜率。

29. 发明申请

US20090239999A1 Polymerization Process and Adhesives Therefrom 有权
标题翻译：聚合工艺和粘合剂
公开(公告)号：US20090239999A1
公开(公告)日：2009-09-24
申请号：US12480988
申请日：2009-06-09
申请人： Jo Ann M. Canich , Peijun Jiang
发明人： Jo Ann M. Canich , Peijun Jiang
IPC分类号： C08L23/00 , C08F110/06
CPC分类号： C08F10/06 , C08F4/65908 , C08F4/65912 , C08F210/06 , Y10S526/943 , C08F4/65927 , C08F210/16 , C08F2500/03 , C08F2500/17 , C08F2500/20
摘要： This invention relates to a propylene polymer comprising a component having a crystallinity of 10% or less and a component having a crystallinity of 20% or more, said propylene polymer having: a) a melting point of X ° C. or more where X=−0.0038(Tp)2+0.36(Tp)+150, where Tp is the temperature of polymerization in ° C.; b) an Mw of 10,000 g/mol or more; c) a heat of fusion of from 1-70 J/g; d) Stereodefects per 10,000 monomer units of Y or less where Y=2.35(Tp)−100 (where Tp is the temperature of polymerization in ° C.) for the portion of the blend that is insoluble in hexane at 23° C.; e) a dot T-Peel on Kraft paper of 1 N or more; and f) a branching factor of 0.98 or less, where the branching factor is the ratio of g′ measured at Mz to g′ measured at Mw, and process to produce such polymers.
摘要翻译：本发明涉及包含结晶度为10％以下的成分和结晶度为20％以上的成分的丙烯聚合物，所述丙烯类聚合物具有：a）熔点X℃以上，X = -0.0038（Tp）2 + 0.36（Tp）+150，其中Tp是以℃表示的聚合温度。 b）10,000g / mol以上的Mw; c）熔化热为1-70J / g; d）对于在23℃下不溶于己烷的共混物部分，每10,000单位单元的Y = 2.35（Tp）-100（其中Tp是聚合温度）的Y或更低的单位单位的立体缺陷度。 e）N型牛皮纸上的T型剥皮; 和f）0.98或更小的支化因子，其中支化因子是在Mw下测量的在Mz测量的g'与g'的比率，以及产生这种聚合物的方法。

30. 发明申请

US20080249231A1 Soft homogeneous isotactic polypropylene compositions 有权
标题翻译：软均匀全同立构聚丙烯组合物
公开(公告)号：US20080249231A1
公开(公告)日：2008-10-09
申请号：US12080486
申请日：2008-04-03
申请人： Sudhin Datta , Charles L. Sims , Peijun Jiang , Abdelhadi Sahnoune , Derek W. Thurman
发明人： Sudhin Datta , Charles L. Sims , Peijun Jiang , Abdelhadi Sahnoune , Derek W. Thurman
IPC分类号： C08L23/16 , C08L9/00
CPC分类号： C08L23/10 , C08L23/12 , C08L23/142 , C08L2205/02 , C08L2666/06
摘要： The present invention also discloses a homogeneous blend composition comprising; a) from 1% to 99% by weight of the blend of a first polymer component comprising a copolymer of 5% to 35% by weight of the first polymer component consisting predominantly of alpha olefin derived units and 65% to 95% by weight of the first polymer component of propylene derived units having a crystallinity of 0.1% to about 25% from isotactic polypropylene sequences, a melting point of from 45° C. to 105° C., and wherein the Melt Flow Rate (MFR @ 230° C.) of the first polymer component is between 300 g/10 min to 5000 g/10 min. b) from 1% to 99% by weight of the blend of a second polymer component comprising isotactic polypropylene and random copolymers of isotactic propylene, wherein the percentage of the copolymerized alpha-olefin in the copolymer is between 0.0% and 9% by weight of the second polymer component and wherein the second polymer component has a melting point greater than about 110° C., wherein the first polymer component has less than 1000 ppm of reaction products arising from the chemical reaction of a molecular degradation agent.
摘要翻译：本发明还公开了一种均匀的共混组合物，其包含： a）1重量％至99重量％的第一聚合物组分的共混物，其包含5重量％至35重量％的主要由α-烯烃衍生单元组成的第一聚合物组分和65重量％至95重量％来自全同立构聚丙烯序列的结晶度为0.1％至约25％的丙烯衍生单元的第一聚合物组分，熔点为45℃至105℃，并且其中熔体流动速率（MFR @ 230℃ 。）的第一聚合物组分在300g / 10min至5000g / 10min之间。 b）1重量％至99重量％的包含全同立构聚丙烯的第二聚合物组分和全同立构丙烯的无规共聚物的共混物的共混物，其中共聚物中共聚α-烯烃的百分比为0.0-9重量％所述第二聚合物组分并且其中所述第二聚合物组分具有大于约110℃的熔点，其中所述第一聚合物组分具有小于1000ppm的由分子降解剂的化学反应产生的反应产物。

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