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21. 发明申请

US20090022872A1 HIGHLY-BRANCHED STARCH, ITS PRODUCTION AND USES 有权
标题翻译：高分配淀粉，其生产和用途
公开(公告)号：US20090022872A1
公开(公告)日：2009-01-22
申请号：US11911090
申请日：2006-03-14
申请人： Tomoyuki Nishimoto , Katsuhiko Hino , Takanori Okura , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
发明人： Tomoyuki Nishimoto , Katsuhiko Hino , Takanori Okura , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
IPC分类号： A23L2/00 , C08B31/00 , A23L1/48 , C12P19/04
CPC分类号： C12P19/18 , A23L33/10 , A23V2002/00 , A61K9/0014 , A61K9/0056 , A61K9/06 , A61K9/2054 , A61K9/4816 , A61K9/7007 , A61K31/718 , C08B30/12 , A23V2200/302 , A23V2250/5118
摘要： An object of the present invention is to provide a novel starchy substance having a retrogradation-resistance, a process for producing the starchy substance efficiently from a material starch by enzymatic reaction, and uses thereof. The present invention attains the above object by providing branched starch having 6-α-maltosyl- and/or 6-α-maltotetraosyl-structure(s) with a marked retrogradation-resistance, a process for producing the branched starch without lowering the molecular weight of material starch, and uses thereof.
摘要翻译：本发明的目的是提供一种具有抗退行性的新型淀粉物质，通过酶促反应从材料淀粉有效地生产淀粉质物质的方法及其应用。本发明通过提供具有显着抗退行性的具有6-α-麦芽糖基 - 和/或6-α-麦芽四糖基结构的支链淀粉来实现上述目的，一种生产支化淀粉而不降低分子量的方法的材料淀粉及其用途。

22. 发明授权

US09265781B2 Process for producing a particulate composition comprising anhydrous crystalline 2-O-alpha-D-glucosyl-L-ascorbic acid 有权
标题翻译：制备包含无水结晶的2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物的方法
公开(公告)号：US09265781B2
公开(公告)日：2016-02-23
申请号：US13980223
申请日：2012-03-07
申请人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
发明人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/18 , A61K31/7048 , C07H17/04 , C12P19/60 , A61K9/16
CPC分类号： A61K31/7048 , A61K9/16 , C07H17/04 , C12P19/18 , C12P19/60 , C12Y204/01019
摘要： The invention provides a process for enabling the production of a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside that does not significantly cake even when the production yield of ascorbic acid 2-glucoside does not reach 35% by weight. The process for producing a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside, which comprises allowing a CGTase to act on a solution containing either liquefied starch or dextrin and L-ascorbic acid and then allowing a glucoamylase to act on the resulting solution to obtain a solution with an ascorbic acid 2-glucoside production yield of at least 27%, purifying the obtained solution to increase the ascorbic acid 2-glucoside content to a level of over 86% by weight, precipitating anhydrous crystalline ascorbic acid 2-glucoside by a controlled cooling method or pseudo-controlled cooling method, collecting the precipitated anhydrous crystalline ascorbic acid 2-glucoside, and ageing and drying the collected anhydrous crystalline ascorbic acid 2-glucoside.
摘要翻译：本发明提供了一种能够生产含有抗坏血酸2-葡萄糖苷的无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，即使当抗坏血酸2-葡萄糖苷的产率不达到35重量％时也不显着。制备含有无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，其包括使CGT酶作用于含有液化淀粉或糊精和L-抗坏血酸的溶液，然后使葡糖淀粉酶作用于所得溶液以获得将抗坏血酸2-葡萄糖苷产率至少为27％的溶液，纯化得到的溶液，将抗坏血酸2-葡萄糖苷含量提高到86重量％以上，将无水结晶性抗坏血酸2-葡萄糖苷通过控制冷却方式或假控制冷却方法，收集沉淀的无水结晶抗坏血酸2-葡萄糖苷，并对收集的无水结晶抗坏血酸2-葡萄糖苷进行老化和干燥。

23. 发明授权

US5824521A Saccharide composition containing trehalulose, its preparation and uses 失效
标题翻译：含有海藻糖的糖组成物，其制备及用途
公开(公告)号：US5824521A
公开(公告)日：1998-10-20
申请号：US57562
申请日：1998-04-09
申请人： Tomoyuki Nishimoto , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
发明人： Tomoyuki Nishimoto , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
IPC分类号： A23G3/00 , A23L27/00 , A23L27/30 , A61K8/60 , A61Q19/00 , C12P19/12 , C12P19/18 , C13K13/00 , C07H3/04 , C12P19/00 , C12P19/14
CPC分类号： C13K13/00 , A23L27/33 , A61K8/60 , A61Q19/00 , C12P19/18 , A61Q11/00
摘要： A saccharide composition containing trehalulose, which is obtainable by allowing a maltose/trehalose converting enzyme to act on a sucrose solution to produce trehalulose, and collecting the resulting trehalulose-containing mixture. Since the enzyme converts sucrose into trehalulose in a relatively high yield and the conversion rate is controllable, a saccharide composition rich in trehalulose is readily obtained on an industrial scale.
摘要翻译：含有海藻糖的糖组合物，其可通过使麦芽糖/海藻糖转化酶作用于蔗糖溶液以产生海藻糖酮并且收集所得含海藻糖糖的混合物而获得。由于酶以较高的产率将蔗糖转化成海藻糖，并且转化率是可控的，所以在工业规模上容易获得富含海藻糖的糖组成。

24. 发明授权

US06294360B1 Saccharide composition containing trehalulose, its preparation and uses 失效
标题翻译：含有海藻糖的糖组成物，其制备及用途
公开(公告)号：US06294360B1
公开(公告)日：2001-09-25
申请号：US08811003
申请日：1997-03-04
申请人： Tomoyuki Nishimoto , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
发明人： Tomoyuki Nishimoto , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P1912
CPC分类号： C13K13/00 , A23L27/33 , A61K8/60 , A61Q11/00 , A61Q19/00 , C12P19/18
摘要： A saccharide composition containing trehalulose, which is obtainable by allowing a maltose/trehalose converting enzyme to act on a sucrose solution to produce trehalulose, and collecting the resulting trehalulose-containing mixture. Since the enzyme converts sucrose into trehalulose in a relatively high yield and the conversion rate is controllable, a saccharide composition rich in trehalulose is readily obtained on an industrial scale.
摘要翻译：含有海藻糖的糖组合物，其可通过使麦芽糖/海藻糖转化酶作用于蔗糖溶液以产生海藻糖酮并且收集所得含海藻糖糖的混合物而获得。由于酶以较高的产率将蔗糖转化成海藻糖，并且转化率是可控的，所以在工业规模上容易获得富含海藻糖的糖组成。

25. 发明申请

US20130295618A1 PROCESS FOR PRODUCING A PARTICULATE COMPOSITION COMPRISING ANHYDROUS CRYSTALLINE 2-O-ALPHA-D-GLUCOSYL-L-ASCORBIC ACID 有权
标题翻译：生产包含无水晶体2-O-ALPHA-D-葡萄糖-L-抗坏血酸的颗粒组合物的方法
公开(公告)号：US20130295618A1
公开(公告)日：2013-11-07
申请号：US13980223
申请日：2012-03-07
申请人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
发明人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/18
CPC分类号： A61K31/7048 , A61K9/16 , C07H17/04 , C12P19/18 , C12P19/60 , C12Y204/01019
摘要： The invention provides a process for enabling the production of a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside that does not significantly cake even when the production yield of ascorbic acid 2-glucoside does not reach 35% by weight. The process for producing a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside, which comprises allowing a CGTase to act on a solution containing either liquefied starch or dextrin and L-ascorbic acid and then allowing a glucoamylase to act on the resulting solution to obtain a solution with an ascorbic acid 2-glucoside production yield of at least 27%, purifying the obtained solution to increase the ascorbic acid 2-glucoside content to a level of over 86% by weight, precipitating anhydrous crystalline ascorbic acid 2-glucoside by a controlled cooling method or pseudo-controlled cooling method, collecting the precipitated anhydrous crystalline ascorbic acid 2-glucoside, and ageing and drying the collected anhydrous crystalline ascorbic acid 2-glucoside.
摘要翻译：本发明提供了一种能够生产含有抗坏血酸2-葡萄糖苷的无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，即使当抗坏血酸2-葡萄糖苷的产率不达到35重量％时也不显着。制备含有无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，其包括使CGT酶作用于含有液化淀粉或糊精和L-抗坏血酸的溶液，然后使葡糖淀粉酶作用于所得溶液以获得将抗坏血酸2-葡萄糖苷产率至少为27％的溶液，纯化得到的溶液，将抗坏血酸2-葡萄糖苷含量提高至86重量％以上，将无水结晶性抗坏血酸2-葡萄糖苷通过控制冷却方式或假控制冷却方法，收集沉淀的无水结晶抗坏血酸2-葡萄糖苷，并对收集的无水结晶抗坏血酸2-葡萄糖苷进行老化和干燥。

26. 发明授权

US08168778B2 Highly-branched starch, its production and uses 有权
标题翻译：高分支淀粉，其生产和用途
公开(公告)号：US08168778B2
公开(公告)日：2012-05-01
申请号：US11911090
申请日：2006-03-14
申请人： Tomoyuki Nishimoto , Katsuhiko Hino , Takanori Okura , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
发明人： Tomoyuki Nishimoto , Katsuhiko Hino , Takanori Okura , Hiroto Chaen , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C08B31/00 , C12P19/04 , C13K7/00 , C07H1/00
CPC分类号： C12P19/18 , A23L33/10 , A23V2002/00 , A61K9/0014 , A61K9/0056 , A61K9/06 , A61K9/2054 , A61K9/4816 , A61K9/7007 , A61K31/718 , C08B30/12 , A23V2200/302 , A23V2250/5118
摘要： An object of the present invention is to provide a novel starchy substance having a retrogradation-resistance, a process for producing the starchy substance efficiently from a material starch by enzymatic reaction, and uses thereof. The present invention attains the above object by providing branched starch having 6-α-maltosyl- and/or 6-α-maltotetraosyl-structure(s) with a marked retrogradation-resistance, a process for producing the branched starch without lowering the molecular weight of material starch, and uses thereof.
摘要翻译：本发明的目的是提供一种具有抗退行性的新型淀粉物质，通过酶反应从材料淀粉有效地生产淀粉质物质的方法及其应用。本发明通过提供具有显着的耐退化性的具有6-α-麦芽糖基和/或6-α-麦芽四糖基结构的支链淀粉来实现上述目的，一种不降低分子量的支链淀粉的制备方法的材料淀粉及其用途。

27. 发明申请

US20110091726A1 PARTICULATE COMPOSITION CONTAINING ANHYDROUS CRYSTALLINE 2-O-alpha-D-GLUCOSYL-L-ASCORBIC ACID, PROCESS FOR PRODUCING THE SAME, AND USES THEREOF 有权
标题翻译：包含无水晶体2-O-α-D-葡糖醛酸-L-抗坏血酸的颗粒组合物，其生产方法及其用途
公开(公告)号：US20110091726A1
公开(公告)日：2011-04-21
申请号：US12875786
申请日：2010-09-03
申请人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
发明人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
IPC分类号： B32B5/00 , C07H19/01 , C12P19/60
CPC分类号： C12P19/60 , A23L33/10 , A23L33/15 , A61K8/0241 , A61K8/676 , A61K8/732 , A61K31/7048 , A61K2800/57 , A61K2800/654 , A61Q19/02 , C07H17/04 , Y10T428/2982
摘要： The present invention aims to provide a particulate composition containing anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic acid having a significantly, hardly solidifiable property compared to conventional ones in a grade for use in quasi-drugs; a process for producing the same; and uses thereof. The present invention solves the above object by providing a particulate composition containing anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic in an amount of over 98.0% by weight but less than 99.9% by weight, on a dry solid basis; or a degree of crystallinity of 90% or higher for anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic acid, when calculated based on a profile of powder X-ray diffraction analysis of the particulate composition, and a dynamic vapor sorption level of 0.01% by weight or lower, when kept at 25° C. under a relative humidity of 35% by weight for 12 hours after removal water in the particulate composition under nitrogen gas stream; and by providing a process for producing the same and uses thereof.
摘要翻译：本发明的目的在于提供一种含有无水结晶2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物，其与用于准药物的级别相比，具有显着难以固化的性能; 其制造方法; 及其用途。本发明通过提供含有无水结晶2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物来解决上述目的，其含量超过98.0重量％但小于99.9重量％，基于干固体 ; 或无水结晶2-O-α-D-葡糖基-L-抗坏血酸的结晶度为90％以上时，基于颗粒组合物的粉末X射线衍射分析曲线和动态蒸气当在氮气流下除去颗粒组合物中的水后，在25℃相对湿度35重量％下保持12小时，吸附水平为0.01重量％以下; 并提供其制造方法及其用途。

28. 发明授权

US08759030B2 Process for producing 2-O-alpha-D-glucopyranosyl-L-ascorbic acid 有权
标题翻译：制备2-O-α-D-吡喃葡萄糖基-L-抗坏血酸的方法
公开(公告)号：US08759030B2
公开(公告)日：2014-06-24
申请号：US10523920
申请日：2003-07-07
申请人： Kazuhisa Mukai , Keiji Tsusaki , Michio Kubota , Shigeharu Fukuda , Toshio Miyake
发明人： Kazuhisa Mukai , Keiji Tsusaki , Michio Kubota , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/44
CPC分类号： C12P19/60
摘要： The object of the present invention is to provide a method and a process for producing 2-O-α-glucopyranosyl-L-ascorbic acid where 5-O-α-glucopyranosyl-L-ascorbic acid and 6-O-α-glucopyranosyl-L-ascorbic acid are not formed or formed in such a small amount that the formation of these can nor be detected. The present invention solves the above object by providing a process for producing 2-O-α-glucopyranosyl-L-ascorbic acid comprising the steps of allowing α-isomaltosyl glucosaccharide-forming enzyme together with or without cyclomaltodextrin glucanotransferase (EC 2.4.1.19) to act on a solution comprising L-ascorbic acid and, an α-glucosyl saccharide to form 2-O-α-glucopyranosyl-L-ascorbic acid and collecting the formed 2-O-α-glucopyranosyl-L-ascorbic acid.
摘要翻译：本发明的目的是提供一种生产2-O-α-吡喃葡萄糖基-L-抗坏血酸的方法和方法，其中5-O-α-吡喃葡萄糖基-L-抗坏血酸和6-O-α-吡喃葡萄糖基 - L-抗坏血酸不是以这样的少量形成或形成，也可以不形成。本发明通过提供一种生产2-O-α-吡喃葡萄糖基-L-抗坏血酸的方法来解决上述目的，其包括以下步骤：将α-异麦芽糖基葡萄糖形成酶与或不与环糊精葡聚糖转移酶（EC 2.4.1.19）一起作用于包含L-抗坏血酸和α-葡萄糖基糖的溶液中以形成2-O-α-吡喃葡萄糖基-L-抗坏血酸并收集形成的2-O-α-吡喃葡萄糖基-L-抗坏血酸。

29. 发明申请

US20080003651A1 alpha-isomaltosylglucosaccharide-forming enzyme, process and uses of the same 有权
标题翻译： α-异麦芽糖基葡萄糖形成酶，其工艺和用途
公开(公告)号：US20080003651A1
公开(公告)日：2008-01-03
申请号：US11797932
申请日：2007-05-09
申请人： Michio Kubota , Keiji Tsusaki , Takanobu Higashiyama , Shigeharu Fukuda , Toshio Miyake
发明人： Michio Kubota , Keiji Tsusaki , Takanobu Higashiyama , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/04
CPC分类号： A23G1/40 , A21D2/181 , A23C9/005 , A23C9/1307 , A23C9/1544 , A23C9/156 , A23G3/42 , A23G4/10 , A23G9/34 , A23L2/60 , A23L15/00 , A23L15/20 , A23L27/30 , A23L33/10 , A23L33/21 , A61K8/60 , A61K8/66 , A61K9/0014 , A61K47/26 , A61Q11/00 , A61Q19/00 , A61Q19/02 , A61Q19/10 , C07H3/04 , C07H3/06 , C12N9/1051 , C12N9/2425 , C12N9/2428 , C12P19/04 , C12Y302/01001 , C12Y302/01002 , C12Y302/01003 , C12Y302/0102
摘要： The object of the present invention is to provide an α-isomaltosylglucosaccharide-forming enzyme, process of the same, cyclotetrasaccharide, and saccharide composition comprising the saccharide which are obtainable by using the enzyme; and is solved by establishing an α-isomaltosylglucosaccharide-forming enzyme which forms a saccharide, having a glucose polymerization degree of at least three and having both the α-1,6 glucosidic linkage as a linkage at the non-reducing end and the α-1,4 glucosidic linkage other than the linkage at the non-reducing end, by catalyzing the α-glucosyl-transfer from a saccharide having a glucose polymerization degree of at least two and having the α-1,4 glucosidic linkage as a linkage at the non-reducing end without substantially increasing the reducing power; α-isomaltosyl-transferring method using the enzyme; method for forming α-isomaltosylglucosaccharide; process for producing a cyclotetrasaccharide having the structure of cyclo{66)-α-D-glucopyranosyl-(163)-α-D-glucopyranosyl-(166)-α-D-glucopyranosyl-(163)-α-D-glucopyranosyl-(16} using both the α-isomaltosylglucosaccharide-forming enzyme and the α-isomaltosyl-transferring enzyme; and the uses of the saccharides obtainable therewith.
摘要翻译：本发明的目的是提供一种α-异麦芽糖基葡萄糖形成酶，其工艺，环四糖和包含可通过使用酶获得的糖的糖组合物; 并且通过建立形成葡糖聚合度至少为3并且在非还原末端具有α-1,6糖苷键作为连接的α糖异构体糖结合酶和α - 通过催化从葡萄糖聚合度至少为2并具有α-1,4糖苷键作为连接的糖的α-葡糖基转移而在非还原性末端的连接以外的1,4-葡糖苷键所述非还原端基本上不增加所述还原能力; 使用该酶的α-异麦芽糖基转移法; 形成α-异麦芽糖基糖的方法; 制备具有环{66）-alpha-D-吡喃葡萄糖基 - （163）-al-D-glucopyranosyl-（166）-al-D-glucopyranosyl-（163）-al-D-glucopyranosyl-（163）-al-D-glucopyranosyl- （16）同时使用α-异麦芽糖基糖产生酶和α-异麦芽糖基转移酶;以及可用其获得的糖的用途。

30. 发明授权

US08642575B2 Method of inhibiting formation of volatile aldehydes and/or decomposition of fatty acids and use thereof 有权
标题翻译：抑制挥发性醛形成和/或分解脂肪酸的方法及其用途
公开(公告)号：US08642575B2
公开(公告)日：2014-02-04
申请号：US10545078
申请日：2004-02-10
申请人： Kazuyuki Oku , Michio Kubota , Shigeharu Fukuda , Toshio Miyake
发明人： Kazuyuki Oku , Michio Kubota , Shigeharu Fukuda , Toshio Miyake
IPC分类号： A01N43/04 , A61K31/715
CPC分类号： A23L3/3562 , A23L2/60 , A23L5/27 , A23L27/33 , A61K8/60 , A61K8/73 , A61K9/0014 , A61K9/0019 , A61K47/26 , A61K2800/52 , A61Q19/00 , C11B5/0021
摘要： The present invention has objects to provide a method for inhibiting the formation of volatile aldehydes and/or the decomposition of fatty acids and use thereof. These objects are attained by establishing a method which comprises incorporating an α-oligoglucosyl α,α-trehalose(s) to a target product to inhibit the formation of volatile aldehydes per se and/or the decomposition of fatty acids per se in fatty acid-containing products; an inhibitory agent for inhibiting the formation of volatile aldehydes and/or the decomposition of fatty acids, which contains an α-oligoglucosyl α,α-trehalose(s) as an effective ingredient; and use thereof to thereby obtain various compositions such as food products, cosmetics, pharmaceuticals, and their materials and intermediates each having a high quality and stability.
摘要翻译：本发明的目的是提供抑制挥发性醛形成和/或脂肪酸分解的方法及其用途。这些目的通过建立一种方法来实现，该方法包括将α-低聚葡萄糖基α，α-海藻糖掺入目标产物以抑制挥发性醛本身的形成和/或脂肪酸 - 含有产品; 用于抑制挥发性醛形成和/或脂肪酸分解的抑制剂，其含有α-低聚葡萄糖基α，α-海藻糖作为有效成分; 并使用它们，从而获得各种具有高质量和稳定性的各种组合物，例如食品，化妆品，药物及其材料和中间体。

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