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21. 发明授权

US06410678B1 Aromatic polycarbonate, production method and molded products thereof 有权
标题翻译：芳香族聚碳酸酯，其制造方法及其成型品
公开(公告)号：US06410678B1
公开(公告)日：2002-06-25
申请号：US09890465
申请日：2001-08-01
申请人： Makoto Ishida , Koji Ishihata , Koji Maeda , Wataru Funakoshi , Hiroaki Kaneko , Yuichi Kageyama , Katsushi Sasaki
发明人： Makoto Ishida , Koji Ishihata , Koji Maeda , Wataru Funakoshi , Hiroaki Kaneko , Yuichi Kageyama , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： G11B7/2534 , C08G63/06 , C08G64/14 , C08G64/307 , G11B7/2533 , G11B7/2535 , G11B7/2536
摘要： An aromatic polycarbonate which has high durability and is excellent in color tone, transparency and mechanical strength, especially an aromatic polycarbonate which has high durability and stability when it is used under high temperature and high humidity conditions for a long time, and production method and use thereof. In the aromatic polycarbonate which has a sodium element content of 100 ppb or less and a content of each of Ni, Pb, Cr, Mn and Fe of 70 ppb or less and the method of producing a polycarbonate by polycondensing an aromatic dihydroxy compound and a carbonic acid diester, the above aromatic polycarbonate is produced by controlling 1) the content of sodium element contained in each of the above raw materials to 52 ppb or less, 2) the content of each of Fe, Cr, Mn, Ni and Pb to 40 ppb or less and 3) the amount of a specific catalyst to a specific value based on the content of Fe contained in the raw materials.
摘要翻译：具有高耐久性和色调，透明性和机械强度优异的芳族聚碳酸酯，特别是长时间在高温高湿条件下使用时具有高耐久性和稳定性的芳族聚碳酸酯，以及制造方法和用途其中。在钠元素含量为100ppb以下的芳族聚碳酸酯中，Ni，Pb，Cr，Mn和Fe的含量为70ppb以下，芳香族二羟基化合物和碳酸二酯，上述芳香族聚碳酸酯通过控制1）上述原料中含有的钠元素的含量为52ppb以下，2）将Fe，Cr，Mn，Ni，Pb各自的含量调整为 40ppb以下，3）根据原料中所含的Fe的含量，特定催化剂的量达到特定值。

22. 发明授权

US06300459B1 Process for producing aromatic polycarbonate 失效
标题翻译：制备芳香族聚碳酸酯的方法
公开(公告)号：US06300459B1
公开(公告)日：2001-10-09
申请号：US09403862
申请日：2000-01-21
申请人： Hiroaki Kaneko , Wataru Funakoshi , Katsushi Sasaki
发明人： Hiroaki Kaneko , Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C08G64/06 , C08G64/42
摘要： An aromatic polycarbonate and an active-hydrogen compound are subjected to the transesterification reaction in the presence of a transesterification catalyst under a reduced pressure condition followed by reaction with a salicylic acid ester derivative expressed by the following chemical formula (1), {wherein X is methyl or ethyl, and Y is a carbonyl group or a divalent functional group expressed by the following formula (2), (where Z is an alkylene group having a carbon number of 1 to 30, an arylene group having a carbon number of 6 to 30 or an aralkylene group having a carbon number of 7 to 30)}. An aromatic polycarbonate having a high molecular weight can be produced by this process.
摘要翻译：芳族聚碳酸酯和活性氢化合物在酯交换催化剂存在下，在减压条件下进行酯交换反应，随后与下列化学式（1）表示的水杨酸酯衍生物反应，其中X为甲基或乙基，Y为由下式（2）表示的羰基或二价官能团，（Z为碳数为1〜30的亚烷基，碳数为6〜 30或碳数为7〜30的亚芳基）}，可以通过该方法制造具有高分子量的芳香族聚碳酸酯。

23. 发明授权

US5858499A Polycarbonate copolymer containing oxaspiroundecane group and production process therefor 失效
标题翻译：含有氧杂环十一烷基团的聚碳酸酯共聚物及其制备方法
公开(公告)号：US5858499A
公开(公告)日：1999-01-12
申请号：US769418
申请日：1996-12-19
申请人： Masanori Abe , Keisuke Shinohara , Wataru Funakoshi , Katsushi Sasaki
发明人： Masanori Abe , Keisuke Shinohara , Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08G64/06 , C08G64/16 , C08G64/30 , G02B1/04 , G02B6/02 , G11B7/24
CPC分类号： C08G64/1608 , C08G64/30 , G02B6/02033
摘要： A polycarbonate copolymer which consists essentially of 5 to 95 mol % of recurring units containing a specific spiroglycol unit and 95 to 5 mol % of recurring units containing a specific biphenol unit, and has a reduced viscosity (.eta..sub.sp /c), measured at 20.degree. C. in a solution containing methylene chloride as a solvent and having a concentration of 0.5 g/dl, of at least 0.3 dl/g, a photoelasticity coefficient of 70.times.10.sup.-13 cm.sup.2 /dyne or less, and a glass transition temperature of at least 95.degree. C.; and a process for the production thereof. This polycarbonate copolymer is useful as a material for an information transmission medium or an information recording medium.
摘要翻译：一种聚碳酸酯共聚物，其基本上由5至95摩尔％的含有特定螺旋体单体的重复单元和95至5摩尔％的含有特定双酚单元的重复单元组成，并且具有在20℃下测量的粘度（η值）在含有二氯甲烷溶剂并且浓度为0.5g / dl，至少0.3dl / g，光弹性系数为70×10-13 cm 2 /达因或更低的溶液中，并且玻璃化转变温度为至少95℃。及其生产方法。该聚碳酸酯共聚物可用作信息传输介质或信息记录介质的材料。

24. 发明授权

US06485657B1 Gamma-ray stabilizer and thermoplastic polymer compound including the said stabilizer 失效
标题翻译： γ射线稳定剂和包括所述稳定剂的热塑性聚合物化合物
公开(公告)号：US06485657B1
公开(公告)日：2002-11-26
申请号：US09485509
申请日：2000-02-11
申请人： Wataru Funakoshi , Tetsuo Kanda , Fumitaka Kondo , Katsushi Sasaki
发明人： Wataru Funakoshi , Tetsuo Kanda , Fumitaka Kondo , Katsushi Sasaki
IPC分类号： G21C512
CPC分类号： C08K5/04 , A61M1/16 , B01D61/30 , B01D65/00 , B01D65/022 , B01D2321/346 , C08K5/005 , C08K5/527 , C08L69/00
摘要： A new gamma-ray stabilizer comprising a combination of 100 parts by weight of a benzyl compound (A) having a specific chemical structure and 0.01 to 10 parts by weight of a pentaerythritol phosphorous ester (B) having a spirocyclic structure. Said stabilizer is preferably blended in such a manner that said (A) is contained in an amount of 0.01 to 10 parts by weight based on 100 parts by weight of a thermoplastic polymer (polycarbonate or the like), and said (B) is contained in an amount of 0.01 to 1 part by weight based on 100 parts by weight of said (A). When the thermoplastic polymer is subjected to gamma-ray irradiation, said stabilizer can efficiently protect the thermoplastic polymer from the deterioration of physical properties and yellowing; and on molding processing, the stabilizer-added polymer is suffered from little color tone deterioration and has excellent color tone, and at the same time, the polymer is scarcely suffered from molecular weight decrease on molding, and exhibits excellent thermal stability, moldability or the like. The thermoplastic polymer (especially polycarbonate) composition containing said stabilizer thus obtained is suitable for medical apparatus and medical material uses, especially a jacket case for an artificial dialyzer.
摘要翻译：包含100重量份具有特定化学结构的苄基化合物（A）和0.01至10重量份具有螺环结构的季戊四醇磷酸酯（B）的组合的新型γ射线稳定剂。所述稳定剂优选以所述（A）的含量相对于100重量份的热塑性聚合物（聚碳酸酯等）为0.01〜10重量份的方式进行配合，所述（B）含有相对于所述（A）100重量份，为0.01〜1重量份。当热塑性聚合物进行γ射线照射时，所述稳定剂可以有效地保护热塑性聚合物免于物理性能的劣化和变黄; 在成型加工中，稳定剂添加聚合物几乎没有色调劣化，并且具有优异的色调，同时聚合物在成型时几乎没有分子量降低，并且显示出优异的热稳定性，成型性或喜欢。含有所得稳定剂的热塑性聚合物（特别是聚碳酸酯）组合物适用于医疗器械和医疗材料用途，尤其适用于人造透析器的外套。

25. 发明授权

US6103856A Polycarbonate composition 有权
标题翻译：聚碳酸酯组合物
公开(公告)号：US6103856A
公开(公告)日：2000-08-15
申请号：US299600
申请日：1999-04-27
申请人： Wataru Funakoshi , Katsushi Sasaki
发明人： Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08K5/156 , C08L69/00 , G11B7/2534 , C08C64/00
CPC分类号： C08K5/156 , C08L69/00 , G11B7/2534
摘要： A polycarbonate composition contains 100 parts by weight of a linear aromatic polycarbonate and 0.001 to 100 parts by weight of a cyclic aromatic carbonate. The cyclic aromatic carbonate is useful as a flowability-improving agent and a shape-transferability-improving agent for the linear aromatic polycarbonate.
摘要翻译：聚碳酸酯组合物含有100重量份的线性芳族聚碳酸酯和0.001至100重量份的环状芳族碳酸酯。环状芳族碳酸酯可用作线性芳族聚碳酸酯的流动性改进剂和形状转移性改进剂。

26. 发明授权

US06265524B1 Process for the preparation of aromatic polycarbonate 失效
标题翻译：芳香族聚碳酸酯的制备方法
公开(公告)号：US06265524B1
公开(公告)日：2001-07-24
申请号：US09424318
申请日：1999-11-22
申请人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki
发明人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C07C68/00 , C07C69/96
摘要： A process for producing an aromatic polycarbonate through an ester interchange reaction between an aromatic carbonic acid diester and an aromatic dihydroxy compound, wherein the aromatic carbonic acid diester is obtained through the decarbonylation reaction of an aromatic oxalic acid diester represented by the following general formula (1): wherein two Ar's are the same or different aromatic hydrocarbon groups having 6 to 14 carbon atoms, and has a hydrolyzable halogen content of 5 ppm or less. According to the present invention, an aromatic polycarbonate having a high molecular weight and excellent color can be easily produced without impairing ester interchange reactivity for the production of the aromatic polycarbonate by using an aromatic carbonic acid diester obtained through the decarbonylation of an aromatic oxalic acid diester and controlling the amount of hydrolyzable halogen contained in the aromatic carbonic acid diester to a value smaller than a predetermined value.
摘要翻译：通过芳族碳酸二酯和芳族二羟基化合物之间的酯交换反应制备芳族聚碳酸酯的方法，其中芳族碳酸二酯通过由以下通式（1）表示的芳族草酸二酯的脱羰反应获得）：其中两个Ar是相同或不同的具有6至14个碳原子的芳族烃基，并且具有5ppm或更低的可水解卤素含量。根据本发明，具有高分子量和优异颜色的芳族聚碳酸酯可以通过使用通过芳香族草酸二酯的脱羰获得的芳香族碳酸二酯和将芳香族碳酸二酯中含有的可水解卤素的量控制在较小的值，可以容易地制造而不损害用于制备芳族聚碳酸酯的酯交换反应性超过预定值。

27. 发明授权

US06525171B2 Process for producing a polycarbonate and method of cleaning a production unit 有权
公开(公告)号：US06525171B2
公开(公告)日：2003-02-25
申请号：US09969582
申请日：2001-10-04
申请人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
发明人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
IPC分类号： C08F600
CPC分类号： C08G85/008 , C08G64/205 , C08G64/307
摘要： A method of cleaning the aromatic polycarbonate production unit with a carbonic acid diaryl ester at a temperature of 200 to 350° C. in an inert gas atmosphere.

28. 发明授权

US06471877B1 Filter device for polycarbonate and production method for polycarbonate 失效
标题翻译：聚碳酸酯过滤装置和聚碳酸酯的生产方法
公开(公告)号：US06471877B1
公开(公告)日：2002-10-29
申请号：US09763944
申请日：2001-09-28
申请人： Masahiro Murakami , Yoshiki Matsuoka , Toru Sawaki , Katsushi Sasaki
发明人： Masahiro Murakami , Yoshiki Matsuoka , Toru Sawaki , Katsushi Sasaki
IPC分类号： B01D3530
CPC分类号： C08G64/406 , B01D29/41 , B01D29/92 , B29B13/10 , B29K2069/00
摘要： Provided are a filtration apparatus for a polycarbonate comprising a filtration container, a flange plate, one or more leaf disc-type filters, a filter press and a center pole having an integral construction with the filter press as constituting elements, these components having specific structures, and a process for manufacturing a polycarbonate using the filtration apparatus. Foreign materials are effectively removed by using the polymer filter, and at the same time, discoloring, crosslinking and gel formation, which would occur in the filter, are suppressed; and as a result, a polycarbonate having excellent quality can be manufactured.
摘要翻译：本发明提供一种聚碳酸酯的过滤装置，其具有过滤容器，凸缘板，一个或多个叶片式过滤器，压滤机和具有作为构成元件的压滤机一体结构的中心杆，这些部件具有特定结构以及使用该过滤装置制造聚碳酸酯的方法。通过使用聚合物过滤器有效地除去异物，并且同时抑制在过滤器中发生的变色，交联和凝胶形成; 结果，可以制造质量优异的聚碳酸酯。

29. 发明授权

US06605686B2 Method for producing an aromatic polycarbonate and method of keeping raw materials thereof 失效
标题翻译：芳香族聚碳酸酯的制造方法及其原料的保存方法
公开(公告)号：US06605686B2
公开(公告)日：2003-08-12
申请号：US10088141
申请日：2002-03-15
申请人： Hidemi Takemoto , Toru Sawaki , Keiichi Kaneko , Katsushi Sasaki
发明人： Hidemi Takemoto , Toru Sawaki , Keiichi Kaneko , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： An aromatic polycarbonate having excellent color is obtained by keeping an aromatic dihydroxy compound and a carbonic acid diester which are raw materials for the production of an aromatic polycarbonate in consideration of the influences of storage atmosphere, temperature, temperature difference from a storage tank and residence time.
摘要翻译：考虑到储存气氛，温度，与储罐的温度差和停留时间的影响，保留作为芳香族聚碳酸酯的制造原料的芳香族二羟基化合物和碳酸二酯，得到颜色优异的芳香族聚碳酸酯。

30. 发明授权

US06252034B1 Process for producing a polycarbonate resin 有权
标题翻译：聚碳酸酯树脂的制造方法
公开(公告)号：US06252034B1
公开(公告)日：2001-06-26
申请号：US09324053
申请日：1999-06-02
申请人： Kazuhiro Uenishi , Masashi Shimonaru , Toru Sawaki , Katsushi Sasaki
发明人： Kazuhiro Uenishi , Masashi Shimonaru , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/205 , C08G64/307
摘要： A process for producing a polycarbonate resin through the melt polycondensation of an aromatic diol compound and a carbonic acid diester compound, wherein (1) valves, (2) gear pumps, (3) flanges and (4) flow passages having the specified structures and characteristic properties are used in the production process. According to the present invention, a high-quality polycarbonate can be obtained by an industrial process.
摘要翻译：通过芳族二醇化合物和碳酸二酯化合物的熔融缩聚制备聚碳酸酯树脂的方法，其中（1）阀，（2）齿轮泵，（3）凸缘和（4）具有特定结构的流动通道和在制造方法中使用特性。根据本发明，可以通过工业方法获得高质量的聚碳酸酯。

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