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21. 发明授权

US4313842A Process for hydrogenation of 2,6,6-trimethyl cyclohexene derivatves, products produced thereby and organoleptic uses of said products 失效
标题翻译： 2,6,6-三甲基环己烯衍生物的氢化方法，由此生产的产品和所述产品的感官用途
公开(公告)号：US4313842A
公开(公告)日：1982-02-02
申请号：US239049
申请日：1981-02-27
申请人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C07C403/16 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/0034 , C11D3/50 , C07C2101/16
摘要： Described is a process for preparing hydrogenated derivatives of 2,6,6-trimethyl cyclohexene derivatives by means of treating said derivatives with hydrogen in the presence of a supported palladium catalyst such as palladium-on-calcium carbonate or palladium-on-barium sulfate in the presence of a quinoline activator. The resulting products are useful for their organoleptic properties as foodstuff flavorants and flavor enhancers, perfume composition ingredients, perfumed article ingredients and tobacco flavorants and flavor enhancers.
摘要翻译：描述了通过在负载的钯催化剂如碳酸钯/钯/硫酸钡的存在下用氢处理所述衍生物来制备2,6,6-三甲基环己烯衍生物的氢化衍生物的方法，其中喹啉激活剂的存在。所得到的产品对于其感官特性可用作食品香料和风味增强剂，香料组合物成分，香料制品成分和烟草香料以及风味增强剂。

22. 发明授权

US4278098A 2,6,6-Trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanols and -1,3-cyclohexadiene-1-methanols and organoleptic uses thereof 失效
标题翻译： 2,6,6-三甲基-α-（异）丙烯-1-环己烯-1-甲醇和1,3-环己二烯-1-甲醇及其感官用途
公开(公告)号：US4278098A
公开(公告)日：1981-07-14
申请号：US119858
申请日：1980-02-08
申请人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
发明人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
IPC分类号： A24B15/30 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C11B9/00 , A24B3/12 , A24B15/36
CPC分类号： C11B9/0034 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C07C403/08 , C07B2200/09 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma, smoking tobacco flavor and aroma and perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, smoking tobacco, perfume and perfumed article aroma and/or flavor imparting materials of 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanol and -1,3-cyclohexadiene-1-methanol derivatives or one or more of their geometric or stereoisomers as defined by the generic structure: ##STR1## wherein one of R.sub.1, R.sub.2 or R.sub.3 is methyl and the other two of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; the dashed line is a carbon-carbon double bond or a carbon-carbon single bond; with the proviso that when R.sub.1 is hydrogen, the dashed line is a carbon-carbon double bond.Addition of one or more of the 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanols or -1,3-cyclohexadiene-1-methanols of our invention to consumable materials is indicated to produce:A. In foodstuffs, chewing gums, toothpastes and medicinal products, sweet, camphoraceous, damascenone, raspberry-like, raspberry juice-like, rosey, woody/ionone-like, oriental, tobacco-like, tea-like, grape-like, fruity and ionone-like aromas and flavor notes;B. In perfumes, colognes and perfumed articles, leathery, hay, woody, mustard, minty, spicey (clove) and pulegone-like aromas and hay/tobacco and honey ionone-like topnotes with safronal-like nuances; andC. In tobaccos and tobacco flavors, a sweet-musty, hay-tobacco-like, fruity-raspberry, ionone-like aroma prior to smoking and a fruity tobacco-like, Virginia tobacco-like aroma on smoking both in the main stream and in the side stream.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和香气，吸烟烟草风味和香气以及香料和香料制品香气增强，增强和赋予组合物的方法和组合物; 以及2,6,6-三甲基-α-（异）丙烯基-1-环己烯-1-甲醇的食品，口香糖，牙膏，药用产品，吸烟烟草，香料和香料制品香气和/或调味材料，以及 -1,3-环己二烯-1-甲醇衍生物或其一般结构定义的其几何或立体异构体中的一种或多种：其中R 1，R 2或R 3中的一个为甲基，R 1，R 2和R 3中的另外两个为表示氢; 虚线是碳 - 碳双键或碳 - 碳单键; 条件是当R1是氢时，虚线是碳 - 碳双键。将本发明的一种或多种2,6,6-三甲基-α-（异）丙烯-1-环己烯-1-甲醇或-1,3-环己二烯-1-甲醇添加到消耗材料中被指示产生：A.在食品，口香糖，牙膏和药用产品中，甜，樟脑，大马士革，覆盆子样，覆盆子汁，玫瑰，木/紫罗兰酮样，东方，烟草状，茶状，葡萄状，水果和紫罗兰酮样香气和风味香气; B.香水，古龙水和香水制品，革质，干草，木质，芥末，小茴香，香料（丁香）和香菇样香气和干草/烟草和蜂蜜类似紫罗兰酮的顶峰，具有丰富的细微差别; 在烟草和烟草香料中，在吸烟之前是一种甜味，干草烟样，果香 - 覆盆子，类胡萝卜素的香气，并且在主流中吸烟时具有类似烟草般的弗吉尼亚烟草样香气并在旁边的流。

23. 发明授权

US4275087A Flavoring with 2,6,6-trimethyl-.alpha.-propenyl-1,3-cyclohexadiene-1-methanol substances 失效
标题翻译：用2,6,6-三甲基-α-丙烯基-1,3-环己二烯-1-甲醇物质调味
公开(公告)号：US4275087A
公开(公告)日：1981-06-23
申请号：US120102
申请日：1980-02-08
申请人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
发明人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
IPC分类号： A23L27/20 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C11B9/00 , A23L1/226 , A23L1/235
CPC分类号： C11B9/0034 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C07C403/08 , C07B2200/09 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma, smoking tobacco flavor and aroma and perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, smoking tobacco, perfume and perfumed article aroma and/or flavor imparting materials of 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanol and -1,3-cyclohexadiene-1-methanol derivatives or one or more of their geometric or stereoisomers as defined by the generic structure: ##STR1## wherein one of R.sub.1, R.sub.2 or R.sub.3 is methyl and the other two of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; the dashed line is a carbon-carbon double bond or a carbon-carbon single bond; with the proviso that when R.sub.1 is hydrogen, the dashed line is a carbon-carbon double bond.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和香气，吸烟烟草风味和香气以及香料和香料制品香气增强，增强和赋予组合物的方法和组合物; 以及2,6,6-三甲基-α-（异）丙烯基-1-环己烯-1-甲醇的食品，口香糖，牙膏，药用产品，吸烟烟草，香料和香料制品香气和/或调味材料，以及 -1,3-环己二烯-1-甲醇衍生物或其一般结构定义的其几何或立体异构体中的一种或多种：其中R 1，R 2或R 3中的一个为甲基，R 1，R 2和R 3中的另外两个为表示氢; 虚线是碳 - 碳双键或碳 - 碳单键; 条件是当R1是氢时，虚线是碳 - 碳双键。

24. 发明授权

US4315953A Process for augmenting or enhancing the aroma or taste of raspberry flavored foodstuffs using 2,6,6-trimethylcyclohexene derivatives 失效
标题翻译：使用2,6,6-三甲基环己烯衍生物增强或增强覆盆子风味食品的香味或味道的方法
公开(公告)号：US4315953A
公开(公告)日：1982-02-16
申请号：US239048
申请日：1981-02-27
申请人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A23L27/29 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/00 , C11D3/50 , A23L1/235
CPC分类号： C07C403/16 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/0034 , C11D3/50 , C07C2101/16
摘要： Described is a process for augmenting or enhancing the aroma or taste of raspberry flavored foodstuffs comprising the step of adding to a foodstuff, an aroma augmenting or enhancing quantity of certain 2,6,6-trimethylcyclohexene derivatives.
摘要翻译：描述了增加或增强覆盆子风味食品的香气或味道的方法，其包括向食品添加增强或增加某些2,6,6-三甲基环己烯衍生物的量的步骤。

25. 发明授权

US4292447A Process for hydrogenation of 2,6,6-trimethyl cyclohexene derivatives, products produced thereby and organoleptic uses of said products 失效
标题翻译： 2,6,6-三甲基环己烯衍生物的氢化方法，由此生产的产品和所述产品的感官用途
公开(公告)号：US4292447A
公开(公告)日：1981-09-29
申请号：US969852
申请日：1978-12-15
申请人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C07C403/00 , C11B9/00 , C11D3/50
CPC分类号： C07C403/16 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/0034 , C11D3/50 , C07C2101/16
摘要： Described is a process for preparing hydrogenated derivatives of 2,6,6-trimethyl cyclohexene derivatives by means of treating said derivatives with hydrogen in the presence of a supported palladium catalyst such as palladium-on-calcium carbonate or palladium-on-barium sulfate in the presence of a quinoline activator. The resulting products are useful for their organoleptic properties as foodstuff flavorants and flavor enhancers, perfume composition ingredients, perfumed article ingredients and tobacco flavorants and flavor enhancers.
摘要翻译：描述了通过在负载的钯催化剂如碳酸钯/钯/硫酸钡的存在下用氢处理所述衍生物来制备2,6,6-三甲基环己烯衍生物的氢化衍生物的方法，其中喹啉激活剂的存在。所得到的产品对于其感官特性可用作食品香料和风味增强剂，香料组合物成分，香料制品成分和烟草香料以及风味增强剂。

26. 发明授权

US4287133A 6-Hydroxy-2,6-dimethylheptanal, organoleptic uses thereof and processes for preparing the same 失效
标题翻译： 6-羟基-2,6-二甲基庚醛，其感官用途及其制备方法
公开(公告)号：US4287133A
公开(公告)日：1981-09-01
申请号：US169900
申请日：1980-07-17
申请人： Mark A. Sprecker , Robert W. Trenkle , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Mark A. Sprecker , Robert W. Trenkle , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
IPC分类号： C07C45/54 , C07C45/56 , C07C45/64 , C07C47/19 , C11B9/00 , C07C141/10
CPC分类号： C11B9/0015 , C07C45/54 , C07C45/56 , C07C45/64 , C07C47/19
摘要： Described is the compound 6-hydroxy-2,6-dimethylheptanal and methods for preparing foodstuffs, flavoring compositions for foodstuffs, tobacco compositions, flavoring compositions for tobacco, perfume compositions, ingredients for perfume compositions, perfumed articles and ingredients for perfumed articles by including said 6-hydroxy-2,6-dimethylheptanal therein in order to produce:(a) In food flavorings, sweet, green, melon-like, tropical fruit-like, seedy and raspberry aromas and/or tastes;(b) In perfumes, sweet, green, melony, floral and muguet-like aromas; and(c) In tobaccos, sweet, fruity-melon-like, peach-like, and floral aromas prior to and on smoking in the main stream and in the sidestream in smoking tobaccos and the same aroma and taste nuances in the filter.Processes for synthesizing the 6-hydroxy-2,6-dimethylheptanal by hydrolysis of 2,6-dimethyl-5-heptenal are also described.
摘要翻译：描述了化合物6-羟基-2,6-二甲基庚醛以及制备食品的方法，用于食品的调味组合物，烟草组合物，烟草调味组合物，香料组合物，香料组合物成分，香料制品和用于香料制品的成分，包括所述 6-羟基-2,6-二甲基庚醛，以产生：（a）在食品香料中，甜味，绿色，瓜类，热带水果样，种子和覆盆子香气和/或口味; （b）香水，甜，绿，香，香，香，香; 和（c）在主烟道和吸烟烟草之间的吸烟之前和烟草中的烟草，甜味，水果瓜状，桃子状和花香味，以及过滤器中相同的香气和味道细微差别。还描述了通过2,6-二甲基-5-庚烯醛水解合成6-羟基-2,6-二甲基庚醛的方法。

27. 发明授权

US4255293A 2,6,6-Trimethyl-.alpha.-(iso-propenyl-1-cyclohexene-1-methanol and 1,3 cyclohexadiene-1-methanol 失效
标题翻译： 2,6,6-三甲基-α-（异丙烯基-1-环己烯-1-甲醇和1,3环己二烯-1-甲醇
公开(公告)号：US4255293A
公开(公告)日：1981-03-10
申请号：US119859
申请日：1980-02-08
申请人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
发明人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
IPC分类号： A23L27/20 , A23L27/29 , A24B15/34 , C07C29/40 , C07C33/14 , C07C403/00 , C11B9/00
CPC分类号： C11B9/0034 , A23L27/203 , A23L27/29 , A24B15/34 , C07C29/40 , C07C33/14 , C07C403/08 , C07C2101/16
摘要： Described are processes for augmenting or enhancing the aroma of perfume compositions or colognes, comprising the step of adding in an aroma augmenting or enhancing quantity to a perfume base or a cologne base, one or more compounds defined according to the generic structure: ##STR1## wherein one of R.sub.1, R.sub.2 or R.sub.3 is methyl and the other two of R.sub.1, R.sub.2 and R.sub.3 are hydrogen; wherein the dashed line represents a carbon-carbon double bond or a carbon-carbon single bond with the proviso that when R.sub.1 is hydrogen, the dashed line represents a carbon-carbon double bond.
摘要翻译：描述了用于增强或增强香料组合物或古龙水香气的方法，其包括将香味增强或增强量添加到香料基料或古龙水碱中的步骤，一种或多种根据通用结构定义的化合物：其中R 1，R 2或R 3中的一个为甲基，R 1，R 2和R 3中的另外两个为氢; 其中虚线表示碳 - 碳双键或碳 - 碳单键，条件是当R1为氢时，虚线表示碳 - 碳双键。

28. 发明授权

US4242281A Process for preparing 6-hydroxy-2,6-dimethylheptanal and intermediates thereof 失效
标题翻译：制备6-羟基-2,6-二甲基庚醛的方法及其中间体
公开(公告)号：US4242281A
公开(公告)日：1980-12-30
申请号：US88519
申请日：1979-10-26
申请人： Mark A. Sprecker , Robert W. Trenkle , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Mark A. Sprecker , Robert W. Trenkle , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
IPC分类号： C07C45/54 , C07C45/56 , C07C45/58 , C07C45/64 , C07C47/19 , C11B9/00
CPC分类号： C11B9/0015 , C07C45/54 , C07C45/562 , C07C45/58 , C07C45/64 , C07C47/19
摘要： Described is the compound 6-hydroxy-2,6-dimethylheptanal useful in augmenting or enhancing the aroma or taste of foodstuffs, flavoring compositions for foodstuffs, tobacco compositions, flavoring compositions for tobacco, perfume compositions, ingredients for perfume compositions, perfumed articles and ingredients for perfumed articles as well as a process for preparing 6-hydroxy-2,6-dimethylheptanal comprising the steps of:(i) forming a sulfite addition salt of 2,6-dimethyl-5-heptenal by mixing an alkali metal sulfite in boric acid with 2,6-dimethyl-5-heptenal and(ii) hydrating the thus formed 2,6-dimethyl-5-heptenal sulfite addition salt with a hydrating reagentas well as the intermediate which is the sulfite addition salt of 2,6-dimethyl-5-heptenal.
摘要翻译：描述了可用于增强或增强食品的香气或味道，食品调味组合物，烟草组合物，烟草调味组合物，香料组合物，香料组合物成分，香料制品和成分的化合物6-羟基-2,6-二甲基庚醛用于加香制品以及制备6-羟基-2,6-二甲基庚醛的方法，包括以下步骤：（i）通过将硼酸中的碱金属亚硫酸盐混合形成2,6-二甲基-5-庚烯醛的亚硫酸盐加成盐酸与2,6-二甲基-5-庚烯醛反应，和（ii）将如此形成的2,6-二甲基-5-庚烯酸亚硫酸酯加成盐与水合试剂以及作为亚硫酸盐加成盐的中间体2,6 - 二甲基-5-庚烯醛。

29. 发明授权

US4252828A Flavoring with bornyl ethyl ether 失效
标题翻译：用冰醋酸乙醚调味
公开(公告)号：US4252828A
公开(公告)日：1981-02-24
申请号：US88375
申请日：1979-10-26
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Shuster , James M. Sanders , Bette M. Light , Edward J. Granda
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Shuster , James M. Sanders , Bette M. Light , Edward J. Granda
IPC分类号： A23L27/20 , A61K9/68 , C11B9/00 , A23L1/226
CPC分类号： C11B9/0046 , A23L27/203 , A61K9/0058
摘要： Described are processes and compositions for augmenting or enhancing the flavor and/or aroma of foodstuffs, chewing gums, medicinal products and toothpastes using as the essential ingredient bornyl ethyl ether, synthetically produced and substantially pure.
摘要翻译：描述了用于增强或增强食品，口香糖，药用产品和牙膏的风味和/或香气的方法和组合物，其使用合成产生的和基本上纯的作为必需组分的冰醋基乙醚。

30. 发明授权

US4173711A 3-(2-Chloroallyloxy)-2(10)-pinene 失效
标题翻译： 3-（2-氯烯丙氧基）-2（10）蒎烯
公开(公告)号：US4173711A
公开(公告)日：1979-11-06
申请号：US939895
申请日：1978-09-05
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Shuster , James M. Sanders , Bette M. Light , Edward J. Granda
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Shuster , James M. Sanders , Bette M. Light , Edward J. Granda
IPC分类号： A24B15/34 , C07C41/16 , C07C43/15 , C07C43/166 , C07C43/18 , C07C43/188 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0061 , A24B15/345 , C07C41/06 , C07C41/09 , C07C41/16 , C11B9/0015 , C11B9/0034 , C11B9/0046 , C11D3/50 , C07C2101/16 , C07C2102/42
摘要： Described are processes and compositions for augmenting or enhancing the flavor and/or aroma of consumable materials including foodstuffs, chewing gums, medicinal products, toothpastes, perfumes, colognes, and perfumed articles using as the essential ingredient at least one C.sub.10 -terpene alkyl, alkenyl, haloalkenyl, and alkynyl ether and diether having the formula:(C.sub.10 -TERPENYL) (O--R.sub.1).sub.nwherein n is 1 or 2; the terpene group is a moiety having one of the structures: ##STR1## and R.sub.1 is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, C.sub.3 alkynyl, or C.sub.3 haloalkenyl. The compounds wherein R.sub.1 is C.sub.2 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, C.sub.3 alkynyl or C.sub.3 haloalkenyl are novel compounds.
摘要翻译：描述了用于增加或增强消耗材料的风味和/或香气的方法和组合物，包括食品，口香糖，药用产品，牙膏，香料，古龙水和使用作为必需成分的至少一种C10-萜烯烷基，烯基，卤代烯基，炔基醚和具有下式的二醚（C10-TERPENYL）（O-R1）n，其中n为1或2; 萜烯基团是具有以下结构之一的部分：R 1是C 1 -C 4烷基，C 3或C 4链烯基，C 3炔基或C 3卤代烯基之一。其中R1是C2-C4烷基，C3或C4烯基，C3炔基或C3卤代烯基的化合物是新化合物。

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