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21. 发明申请

WO2019211170A8 GRANULES OR POWDERS AND METHODS FOR THEIR MANUFACTURE 审中-公开
公开(公告)号：WO2019211170A8
公开(公告)日：2019-11-07
申请号：PCT/EP2019/060638
申请日：2019-04-25
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , DETERING, Juergen , SUELING, Carsten , SCHMIDT, Kati , MUELLER, Michael Klemens , TUERKOGLU, Gazi , SCHMIDT, Thomas
IPC分类号： C11D11/02 , C11D11/00 , C11D3/33 , C11D3/37 , C11D17/06
摘要： Process for manufacturing granules or powders comprising the steps of (a) providing an aqueous solution or slurry of (A) at least one chelating agent according to general formula (I a) [CH 3 -CH(COO)-N(CH 2 -COO) 2 ]M 3-X H X (I a) wherein M is selected from alkali metal cations and ammonium, same or different, and x is in the range of from 0.01 to 1.0 or (I b) [OOC-CH 2 CH 2 -CH(COO)-N(CH 2 -COO) 2 ]M 4-X H X (I b) wherein M is as defined above, and x in formula (I b) is in the range of from 0.01 to 2.0, and (B) at least one polymer selected from (B1 ) polyaspartates with an average molecular weight M w in the range of from 1,000 to 20,000 g/mole, and (B2) copolymers comprising, in copolymerized form, (α) at least one ester of an ethylenically unsaturated mono- or dicarboxylic acid, and (β) at least one ethylenically unsaturated N-containing monomer, and (b) spray drying or granulating said solution or slurry.

22. 发明申请

WO2018197249A1 CONTAINER COMPRISING A DETERGENT COMPOSITION CONTAINING SALTS OF MGDA AND GLDA 审中-公开
公开(公告)号：WO2018197249A1
公开(公告)日：2018-11-01
申请号：PCT/EP2018/059670
申请日：2018-04-16
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , MORMUL, Verena , SCHMIDT, Thomas , MANNING, Jeremy
IPC分类号： C11D3/33 , C11D11/00 , C11D17/04
摘要： Container comprising a single unit dose of a detergent composition containing at least two complexing agents (A) dissolved in an aqueous medium, said complexing agents (A) being (A1) at least one alkali metal salt of MGDA, and (A2) at least one alkali metal salt of GLDA, the weight ratio of (A1) and (A2) being in the range of from 1:9 to 9:1, wherein said container is made from a polymer, and wherein such aqueous medium comprises at least 25% by weight of water, referring to the entire liquid phase without (A1) or (A2), wherein the amount of optically inactive impurities is in the range 0.1-5 wt%, referring to (A), and wherein complexing agents (A1) and (A2) are partially neutralized with alkali. Use of the said container for dishwashing or laundry cleaning. Process for making the said container or a compartment of the said container.

23. 发明申请

WO2014001077A1 PROCESS FOR EMULSION POLYMERIZATION 审中-公开
标题翻译：乳液聚合方法
公开(公告)号：WO2014001077A1
公开(公告)日：2014-01-03
申请号：PCT/EP2013/061964
申请日：2013-06-11
申请人： BASF SE , BASF SCHWEIZ AG
发明人： WEIDL, Christian, Hubert , KLAGGE, Ronald , HELD, Uwe , REINOSO GARCIA, Marta , MAUSBERG, Thomas
IPC分类号： C08F2/24 , C11D1/825 , C08F2/30
CPC分类号： C08F2/44 , B01F17/0021 , C08F2/24 , C08F2/30
摘要： Process for polymerizing at least one monomer under emulsion polymerization conditions, characterized in that the (co)monomers are selected from vinyl aromatic compounds, ethylenically unsaturated carboxylic acids with 3 to 10 carbon atoms, C 1 -C 10 -alkyl esters of ethylenically unsaturated carboxylic acids with 3 to 10 carbon atoms, 1,3-butadiene, and a-olefins bearing in the range of from 10 to 250 carbon atoms per molecule, in pure form or as mixture with isomers, and using a surfactant mixture comprising (A) an alkoxylation product of at least one alkanol (a), characterized in that alkanol (a) has 6 to 12 carbon atoms per molecule and the average number of alkylene oxide units per molecule in alkoxylation product (A) assumes a value in the range of from 35 to 55, the alkylene oxide units are selected from C 2 -C 10 -alkylene oxide units and alkanol (a) has an average degree of branching of at least 1; and (B) an alkoxylation product of at least one alkanol (b), characterized in that alkanol (b) has 13 to 19 carbon atoms per molecule and the average number of alkylene oxide units per molecule in alkoxylation product (B) assumes a value in the range of from 35 to 55, the alkylene oxide units are selected from C 2 -C 10 -alkylene oxide units, or (C) an alkoxylation product of at least one linear C 12 -C 22 -alkyl alcohol (c), characterized in that the average number of alkylene oxide units per molecule in alkoxylation product (C) assumes a value in the range of from 35 to 55, the alkylene oxide units are selected from C 2 -C 10 -alkylene oxide units.
摘要翻译：在乳液聚合条件下聚合至少一种单体的方法，其特征在于（共）单体选自乙烯基芳族化合物，具有3-10个碳原子的烯属不饱和羧酸，烯属不饱和羧酸的C 1 -C 10烷基酯与 3至10个碳原子，1,3-丁二烯和每分子具有10至250个碳原子的α-烯烃，以纯形式或与异构体混合，并使用表面活性剂混合物，其包含（A）烷氧基化至少一种链烷醇（a）的产物，其特征在于链烷醇（a）每分子具有6至12个碳原子，并且烷氧基化产物（A）中每分子的平均氧化烯单位数假定为35 至55，烯化氧单元选自C 2 -C 10 - 氧化烯单元，链烷醇（a）的平均支化度至少为1; 和（B）至少一种链烷醇（b）的烷氧基化产物，其特征在于链烷醇（b）每分子具有13至19个碳原子，并且烷氧基化产物（B）中每分子的平均氧化烯单元数呈现值在35至55的范围内，烯化氧单元选自C 2 -C 10 - 氧化烯单元，或（C）至少一种直链C 12 -C 22烷基醇（c）的烷氧基化产物，其特征在于，烷氧基化产物（C）中每分子的平均氧化烯单元数为35至55的范围，烯化氧单元选自C 2 -C 10 - 氧化烯单元。

24. 发明申请

WO2022184551A1 PROCESS FOR MAKING A PARTICULATE COATED ORGANIC SALT, AND PARTICULATE COATED SALT 审中-公开
公开(公告)号：WO2022184551A1
公开(公告)日：2022-09-09
申请号：PCT/EP2022/054695
申请日：2022-02-24
申请人： BASF SE
发明人： STREMPEL, Verena , REINOSO GARCIA, Marta , LOEFFLER, Daniel , SUELING, Carsten
IPC分类号： B01J13/14 , C11D17/00
摘要： Process for making a particulate coated chelating agent (A) wherein said process comprises the following steps: (a) Providing a granule or powder containing an alkali metal salt of methyl glycine diacetic acid (MGDA)or glutamic acid diacetic acid (GLDA), preferably with a moisture content in the range of from 1 to 15% by weight, (b) treating said salt with a metal alkoxide or metal halide or metal amide or alkyl metal compound or with an alkoxide, amide, halide or alkyl compound of silicon, (c) treating the material obtained in step (b) with moisture or (c*) with ozone, (d) optionally, repeating the sequence of steps (b) and (c) once to 25 times.

25. 发明申请

WO2021185702A1 PROCESS FOR MAKING A GRANULE 审中-公开
公开(公告)号：WO2021185702A1
公开(公告)日：2021-09-23
申请号：PCT/EP2021/056394
申请日：2021-03-12
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , HAREMZA, Sylke , GIESHOFF, Tile , TANG, Dan-Tam, Daniel , SCHMIDT, Thomas , MUELLER, Michael, Klemens
IPC分类号： C11D3/33 , C11D7/32 , C11D11/00 , C11D11/02 , C11D3/28 , C11D3/37
摘要： Process for making a powder or granule containing (A) at least one chelating agent selected from alkali metal salts of methyl glycine diacetic acid (MGDA) and of iminodisuccinic acid (IDS), (B) at least one compound of general formula (I a) or (I b) wherein A1 is selected from (CH2)a wherein the variable a is in the range of from 4 to 20, e is selected from zero and 1, and R1 being the same or different and selected from O-C1-C10-alkyl and C1-C10-alkyl, and, optionally, (C) at least one homo- or copolymer of (meth)acrylic acid, partially or fully neutralized with alkali, said process comprising the steps of (a) providing an aqueous solution or slurry containing chelating agent (A) and said com-pound (B) and, if applicable, (co)polymer (C), with a pH value in the range of from 10 to 12, (b) removing most of said water by spray drying or spray granulation.

26. 发明申请

WO2020104231A1 POWDERS AND GRANULES CONTAINING A CHELATING AGENT AND AN ENZYME 审中-公开
公开(公告)号：WO2020104231A1
公开(公告)日：2020-05-28
申请号：PCT/EP2019/080838
申请日：2019-11-11
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , SPANGENBERG, Oliver , SCHOENHERR, Michael , MUELLER, Michael Klemens , SUELING, Carsten
IPC分类号： C11D17/06 , C11D3/386 , C11D3/33
摘要： Process for making a powder or granule containing (A) at least one chelating agent selected from alkali metal salts of methyl glycine diacetic acid (MGDA) and of glutamic acid diacetate (GLDA) and of iminodisuccinic acid (IDS), (B) at least one enzyme in a weight ratio of (A):(B) of from 5 : 1 up to 1,000:1, wherein said powder or granule contains at least 75% by weight of chelating agent (A), said process comprising the steps of (a) mixing the at least one chelating agent (A) and the at least one enzyme (B) in the presence of water, thereby forming a solution or slurry, (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125°C.

27. 发明申请

WO2020094480A1 PROCESS FOR MANUFACTURING GRANULES, AND GRANULES AND THEIR USE 审中-公开
公开(公告)号：WO2020094480A1
公开(公告)日：2020-05-14
申请号：PCT/EP2019/079667
申请日：2019-10-30
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , MUELLER, Michael Klemens , SCHMIDT, Kati , JAEKEL, Frank
IPC分类号： C11D3/33 , C11D11/00 , C11D17/06 , C11D7/32 , C11D11/02
摘要： Process for manufacturing granules of salts of at least two aminopolycarboxylic acids (A), comprising the steps of : (a) providing an aqueous solution of : (A1) at least one alkali metal salt of methyl glycine diacetic acid (MGDA) and (A2) at least one alkali metal salt of L- and D-enantiomers of glutamic acid diacetic acid (GLDA) or of enantiomerically pure L-GLDA, the weight ratio of (A1) and (A2) being in the range of from 10:1 to 200:1; (b) spray granulating said solution with a gas inlet temperature of at least 125°C. Additionally, the present invention relates to granules and to their use.

28. 发明申请

WO2020030623A1 PACKAGING UNIT COMPRISING A DETERGENT COMPOSITION CONTAINING AN ENZYME AND AT LEAST ONE CHELATING AGENT 审中-公开
公开(公告)号：WO2020030623A1
公开(公告)日：2020-02-13
申请号：PCT/EP2019/071083
申请日：2019-08-06
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , BAIER, Grit , KUEBELBECK, Sonja
IPC分类号： C11D3/33 , C11D3/386 , C11D17/04
摘要： Packaging unit containing a detergent single unit dose wherein said packaging unit comprises a compartment 1 comprising an aqueous solution of enzyme (A) and at least one chelating agent (B) dissolved in an aqueous medium, said chelating agent (B) being (B1) at least one alkali metal salt of glutamic acid diacetic acid (GLDA), and (B2) at least one alkali metal salt of methyl glycine diacetic acid (MGDA), and one more compartment comprising at least one ingredient of a detergent other than en- zyme (A) and chelating agent(s) (B), wherein the overall concentration of chelating agent(s) (B) in compartment 1 is in the range of from 35 to 75 % by weight.

29. 发明申请

WO2018011027A1 PROCESS FOR MANUFACTURING OF MGDA AND GLDA CONTAINING GRANULES, THE GRANULES AND THEIR USE 审中-公开
标题翻译：制造含MGDA和GLDA的颗粒，颗粒及其使用的方法
公开(公告)号：WO2018011027A1
公开(公告)日：2018-01-18
申请号：PCT/EP2017/066705
申请日：2017-07-05
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , MUELLER, Michael Klemens , SUELING, Carsten , MORMUL, Verena
IPC分类号： C11D3/33 , C11D7/32 , C11D11/02 , C11D17/00
摘要： Process for manufacturing granules of salts of at least two aminopolycarboxylic acids (A), com- prising the steps of (a) providing an aqueous solution of (A1) at least one alkali metal salt of a mixture of L- and D- enantiomers of methyl glycine diacetic acid (MGDA), said mixture containing predominantly the respective L-isomer with an enantiomeric excess (ee) in the range of from 10 to 95 %, (A2) at least one alkali metal salt of L- and D-enantiomers of glutamic acid diacetic acid (GLDA) or of enantiomerically pure L-GLDA, the weight ratio of (A1) and (A2) being in the range of from 1:9 to 9:1, (b) spray granulating said solution with a gas inlet temperature of at least 125°C. Additionally, the present invention relates to granules and to their use.
摘要翻译：制备至少两种氨基多羧酸（A）的盐的颗粒的方法，包括以下步骤：（a）提供（A1）至少一种混合物的碱金属盐的水溶液的甲基甘氨酸二乙酸（MGDA）的L-和D-对映异构体，所述混合物主要含有相应的L-异构体，对映体过量（ee）为10-95％，（A2）至少一种碱金属谷氨酸二乙酸（GLDA）的L-和D-对映异构体的盐或对映体纯的L-GLDA的盐，（A1）和（A2）的重量比在1:9至9:1的范围内， b）用至少125℃的气体入口温度喷雾造粒所述溶液。此外，本发明涉及颗粒及其用途。

30. 发明申请

WO2016142228A1 PROCESS FOR MAKING MIXTURES OF ENANTIOMERS, AND MIXTURES OF ENANTIOMERS 审中-公开
标题翻译：制造增效剂混合物的方法和制剂的混合物
公开(公告)号：WO2016142228A1
公开(公告)日：2016-09-15
申请号：PCT/EP2016/054375
申请日：2016-03-02
申请人： BASF SE
发明人： FRANZKE, Constanze , REINOSO GARCIA, Marta , BAUMANN, Robert , GREINDL, Thomas
IPC分类号： C07C229/16 , C07C229/24 , C11D3/33
CPC分类号： C11D3/33 , C07C227/18 , C07C253/00 , C07C253/06 , C07C255/25 , C07C229/16 , C07C229/24
摘要： Process for preparation of a mixture of methyl glycine diacetic acid (MGDA) or its respective mono-, di-, trialkali metal salt or its respective mono-, di- or tri-ammonium salt or mixtures thereof, and glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri-, or tetra-alkali metal or mono-, di-, tri- or tetra-ammonium salt or mixtures thereof, wherein said process com- prises the steps of: (a) dissolution in water of (a1) alanine in its L- or D-enantiomeric form or its respective monoalkali metal salt or mixtures thereof, and (a2) glutamic acid as L- or D-enantiomer or its respective mono-, or dialkali metal or mixtures thereof, wherein the molar ratio of alanine to glutamic acid is in the range of from1:9 to 9:1, (b) converting the mixture obtained in step (a) with formaldehyde and hydrocyanic acid or alkali metal cyanide to the corresponding dinitriles, (c) saponification of the dinitriles resulting from step (b).
摘要翻译：制备甲基甘氨酸二乙酸（MGDA）或其相应的单，二，三碱金属盐或其相应的单 - ，二 - 或三 - 铵盐或其混合物和谷氨酸二乙酸（GLDA）的混合物的方法）或其相应的单 - ，二 - ，三 - 或四 - 碱金属或单 - ，二 - ，三 - 或四 - 铵盐或其混合物，其中所述方法包括以下步骤：（a）溶解（a1）丙氨酸以其L-或D-对映体形式或其相应的单碱金属盐或其混合物的水，和（a2）谷氨酸作为L-或D-对映异构体或其相应的单或二碱金属或混合物其中丙氨酸与谷氨酸的摩尔比在1:9至9:1的范围内，（b）将甲醛和氢氰酸或碱金属氰化物转化为相应的二腈，步骤（a）中得到的混合物与甲醛和氢氰酸或碱金属氰化物反应，（c）由步骤（b）产生的二腈的皂化。

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