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21. 发明授权

US4772583A Beta-alkylidene phenethyl alcohol esters and ethers, organoleptic uses thereof and processes for preparing same 失效
标题翻译： β-亚烷基苯乙醇酯和醚，其感官用途及其制备方法
公开(公告)号：US4772583A
公开(公告)日：1988-09-20
申请号：US134817
申请日：1987-12-18
申请人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0061
摘要： Described is the novel compound genus the beta-alkylidene phenethyl alcohol esters and ethers of our invention defined according to the generic structure: ##STR1## wherein R.sub.5 represents hydrogen or methyl; wherein R.sub.6 represents one of the moieties: ##STR2## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 each represents the same or different hydrogen or methyl; wherein R.sub.7 represents methyl or ethyl; and wherein R.sub.8 represents hydrogen or methyl; useful in augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener articles, fabric softener compositions, cosmetic powders and hair preparations.
摘要翻译：描述了根据通用结构定义的本发明的β-亚烷基苯乙醇酯和醚的新化合物：其中R 5表示氢或甲基; 其中R 6表示以下部分之一：其中R 1，R 2，R 3和R 4各自表示相同或不同的氢或甲基; 其中R 7表示甲基或乙基; 并且其中R8表示氢或甲基; 可用于增强或增强消耗材料的香气，包括香料，古龙水和加香制品，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂制品，织物柔软剂组合物，化妆粉和头发制剂。

22. 发明授权

US4629805A Alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones and organoleptic uses thereof 失效
公开(公告)号：US4629805A
公开(公告)日：1986-12-16
申请号：US726603
申请日：1985-04-23
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C69/757
CPC分类号： C11B9/0034 , C08K5/101 , C11D3/50
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.

23. 发明授权

US4613706A Isomer-directed process for producing asymmetric ketones using catalytic Claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
公开(公告)号：US4613706A
公开(公告)日：1986-09-23
申请号：US765231
申请日：1985-08-13
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C07C49/203 , C07C49/217 , C07C403/00 , C11B9/00
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloalkyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##

24. 发明授权

US4543192A Use of norbornyl oxyacetaldehyde in augmenting or enhancing aroma of detergents or fabric softeners 失效
标题翻译：降冰片基氧乙醛在增加或增强洗涤剂或织物软化剂香气中的应用
公开(公告)号：US4543192A
公开(公告)日：1985-09-24
申请号：US620133
申请日：1984-06-13
申请人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C07C45/38 , C07C47/198 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0046 , C07C45/38 , C07C47/198 , Y02P20/582
摘要： Described is a compound having the structure: ##STR1## a norbornyl oxyacetaldehyde, prepared by oxidizing the norbornyl oxyethanol compound having the structure: ##STR2## using air or oxygen and a silver or copper chromite catalyst; and organoleptic uses of such oxidation product in the field of perfumery, colognes and perfumed articles (e.g. perfumed plastics, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or drier-added fabric softener articles).
摘要翻译：描述了具有以下结构的化合物：通过使用空气或氧气和银或亚铬酸铜催化剂氧化具有以下结构的降冰片基氧基乙醇化合物制备的降冰片基氧乙醛：以及在香料，古龙水和香水制品（例如加香塑料，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物或干燥剂添加的织物柔软剂制品）领域中的这种氧化产物的感官用途。

25. 发明授权

US4493790A Organoleptic use of isopropyl tetramethylindanes 失效
标题翻译：感官使用异丙基四甲基茚满
公开(公告)号：US4493790A
公开(公告)日：1985-01-15
申请号：US541263
申请日：1983-10-12
申请人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
发明人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
IPC分类号： C07C5/29 , C07C45/46 , C07C49/792 , C11B9/00
CPC分类号： C11B9/0049 , C07C45/46 , C07C49/792 , C07C5/29
摘要： Described are isopropyl tetramethylindan musks defined according to the generic structure: ##STR1## wherein R.sub.3 and R.sub.4 are each acetyl or methyl with the provisos:(a) one of R.sub.3 or R.sub.4 is methyl;(b) when R.sub.4 is methyl, then R.sub.3 is acetyl and(c) when R.sub.4 is acetyl, R.sub.3 is methyland organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles.
摘要翻译：描述了根据通用结构定义的异丙基四甲基茚满麝香：其中R 3和R 4各自为乙酰基或甲基，条件是：（a）R 3或R 4中的一个为甲基; （b）当R 4为甲基时，R 3为乙酰基，（c）当R 4为乙酰基时，R 3为甲基和感官用途，用于增强或增强香水组合物，古龙水和香料制品的香味。

26. 发明授权

US4460795A Process for preparing mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4460795A
公开(公告)日：1984-07-17
申请号：US478355
申请日：1983-03-24
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C93/16
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "', R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "', R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "' and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

27. 发明授权

US4359390A Norbornyl oxyacetaldehyde, organoleptic uses thereof and process for preparing same 失效
标题翻译：降冰片基氧乙醛，感官用途及其制备方法
公开(公告)号：US4359390A
公开(公告)日：1982-11-16
申请号：US357078
申请日：1982-03-11
申请人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C07C45/38 , C07C47/198 , C11B9/00 , D06M13/00 , D06M13/20
CPC分类号： D06M13/005 , C07C45/38 , C07C47/198 , C11B9/0046 , Y02P20/582
摘要： Described is a compound having the structure: ##STR1## a norbornyl oxyacetaldehyde, prepared by oxidizing the norbornyl oxyethanol compound having the structure: ##STR2## using air or oxygen and a silver or copper chromite catalyst; and organoleptic uses of such oxidation product in the field of perfumery, colognes and perfumed articles (e.g. perfumed plastics, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or drier-added fabric softener articles).
摘要翻译：描述了具有以下结构的化合物：通过使用空气或氧气和银或亚铬酸铜催化剂氧化具有以下结构的降冰片基氧基乙醇化合物制备的降冰片基氧乙醛：以及在香料，古龙水和香水制品（例如加香塑料，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物或干燥剂添加的织物柔软剂制品）领域中的这种氧化产物的感官用途。

28. 发明授权

US5378685A Process for preparing mixture of trimethyl and dimethylmethylene propyl polyhydropyrans, products produced thereby perfumery uses of such product 失效
标题翻译：制备三甲基和二甲基亚甲基丙基多羟基吡喃的混合物的方法，由此产生的产品由此产生香料的用途
公开(公告)号：US5378685A
公开(公告)日：1995-01-03
申请号：US214185
申请日：1994-03-17
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07D309/04 , C07D309/12 , C11B9/00 , A61K7/46
CPC分类号： C07D309/12 , C07D309/04 , C11B9/008
摘要： Described is a process for preparing trimethyl and dimethylmethylene propyl polyhydropyran derivatives including compounds defined according to the structure: ##STR1## which defines a mixture wherein in the mixture, in each of the compounds one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represents a carbon-carbon single bond as well as the compound having the structure: ##STR2## products produced thereby; perfumery uses of such products; process intermediates of such process including compounds defined according to the structures: ##STR3## wherein X represents chloro or bromo.
摘要翻译：描述了一种制备三甲基和二甲基亚甲基丙基多氢吡喃衍生物的方法，其包括根据以下结构定义的化合物：其定义为混合物，其中在每种化合物中，虚线中的一个为碳 - 碳双键，虚线中的每一个代表碳 - 碳单键，以及具有以下结构的化合物：由此产生的产物; 这种产品的香水用途; 该方法的加工中间体包括根据以下结构定义的化合物：其中X表示氯或溴。

29. 发明授权

US4933488A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4933488A
公开(公告)日：1990-06-12
申请号：US456744
申请日：1989-12-26
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C33/025 , C07C67/11 , C11B9/0015
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4--4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen; and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢; 并且R1“和R2”不都是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

30. 发明授权

US4933321A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4933321A
公开(公告)日：1990-06-12
申请号：US457174
申请日：1989-12-26
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C07C33/025 , C07C67/11 , C11B9/0015 , C11D3/50
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4-4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen; and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume composition, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or switterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢; 并且R1“和R2”不都是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或转换洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

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