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11. 发明授权

US6166208A Preparation of fungicidal quinazolinones and useful intermediates 有权
标题翻译：杀真菌喹唑啉酮和有用的中间体的制备
公开(公告)号：US6166208A
公开(公告)日：2000-12-26
申请号：US202394
申请日：1998-12-09
申请人： James Francis Bereznak , Eric Allen Marshall , Charlene Gross Sternberg , Jeffrey Arthur Sternberg , King-Mo Sun
发明人： James Francis Bereznak , Eric Allen Marshall , Charlene Gross Sternberg , Jeffrey Arthur Sternberg , King-Mo Sun
IPC分类号： C07C271/68 , C07C331/28 , C07D239/95 , C07D239/96
CPC分类号： C07C271/68 , C07C331/28 , C07D239/95 , C07D239/96
摘要： This invention provides advantageous processes for preparing quinazolinones of Formula I ##STR1## wherein: R.sup.1 is C.sub.1 -C.sub.10 alkyl; C.sub.3 -C.sub.10 alkenyl; C.sub.3 -C.sub.10 cycloalkyl; C.sub.3 -C.sub.10 halocycloalkyl; C.sub.4 -C.sub.10 cycloalkylalkyl; C.sub.4 -C.sub.10 halocycloalkylalkyl; or C.sub.3 -C.sub.10 alkynyl;R.sup.2 is C.sub.1 -C.sub.10 alkyl; C.sub.3 -C.sub.10 alkenyl; C.sub.3 -C.sub.10 cycloalkyl; C.sub.3 -C.sub.10 halocycloalkyl; C.sub.4 -C.sub.10 cycloalkylalkyl; C.sub.4 -C.sub.10 halocycloalkylalkyl; C.sub.4 -C.sub.10 cycloalkyl; C.sub.4 -C.sub.10 halocycloalkyl; or C.sub.3 -C.sub.10 alkynyl; andR.sup.3 and R.sup.4 are each independently hydrogen or halogen; from compounds containing the moiety IIg ##STR2## This invention further provides certain compounds of Formula II, IIIa, or IVa ##STR3## where R.sup.7 is C.sub.2 -C.sub.6 alkyl.
摘要翻译： PCT No.PCT / US97 / 10254 Sec。 371 1998年12月9日第 102（e）日期1998年12月9日PCT提交1997年6月12日PCT公布。公开号WO97 / 48684 日期1997年12月24日本发明提供了制备式I的喹唑啉酮的有利方法，其中：R1是C1-C10烷基; C 3 -C 10烯基; C3-C10环烷基; C 3 -C 10卤代环烷基; C4-C10环烷基烷基; C 4 -C 10卤代环烷基烷基; 或C 3 -C 10炔基; R2是C1-C10烷基; C 3 -C 10烯基; C3-C10环烷基; C 3 -C 10卤代环烷基; C4-C10环烷基烷基; C 4 -C 10卤代环烷基烷基; C4-C10环烷基; C 4 -C 10卤代环烷基; 或C 3 -C 10炔基; 且R 3和R 4各自独立地为氢或卤素; 含有部分IIg的化合物本发明进一步提供某些其中R 7为C 2 -C 6烷基的式II，IIIa或IVa化合物。

12. 发明授权

US5118844A New fluorinated alkoxy imines and their N-chloro- and N-bromo-derivatives, and process for their preparation 失效
标题翻译：新的氟化烷基化合物及其N-氯代和N-溴代衍生物及其制备方法
公开(公告)号：US5118844A
公开(公告)日：1992-06-02
申请号：US677173
申请日：1991-03-29
申请人： Darryl D. Desmarteau , Stefan P. Kotun
发明人： Darryl D. Desmarteau , Stefan P. Kotun
IPC分类号： C07C239/20 , C07C251/52 , C07C259/02 , C07C271/68
CPC分类号： C07C271/68 , C07C239/20
摘要： The present invention relates to novel fluorinated alkoxyimines having the formula:R.sub.x --CF.dbd.N--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (I)wherein:R.sub.x is either F or a perhalogenated alkyl group containing from 1 to 3 carbon atoms, andZ.sub.1 and Z.sub.2, either equal to, or different from, each other, are F, Cl, Br, H or a perfluorinated alkyl group containing from 1 to 3 carbon atoms.They are prepared by reacting a fluorinated alkoxyamine haivng the formula:R.sub.x --CF.sub.2 --NH--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (V)with KF at a temperature comprised within the range of from 0.degree. C. to 100.degree. C.The present invention relates furthermore to the N-chloro- and N-bromo-derivatives of said fluorinated alkoxyimines (I), which derivatives have the formulae:R.sub.x --CF.sub.2 --NCl--O--CZ.sub.1 Z.sub.2 CF.sub.3 (VII)andR.sub.x --CF.sub.2 --NBr--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (VIII).

13. 发明授权

US5237084A Preparation of dialkyl (N-cyanoimido)carbonates from dialkyl imidocarbonates and cyanogen halides 失效
标题翻译：由二烷基亚氨基碳酸酯和氰卤化物制备二烷基（N-氰基亚氨基）碳酸酯
公开(公告)号：US5237084A
公开(公告)日：1993-08-17
申请号：US823518
申请日：1992-01-21
申请人： Michael A. Oliver , Ward H. Oliver
发明人： Michael A. Oliver , Ward H. Oliver
IPC分类号： C07C271/68
CPC分类号： C07C271/68
摘要： Dialkyl (N-cyanoimido) carbonates are prepared in good yield in a non-aqueous solvent by a process which comprises either (a) adding a cyanogen halide at a controlled rate to a reactor containing an unsubstituted or substituted dialkyl imidocarbonate, an inorganic base and/or a trialkyl amine, or (b) by adding a trialkyl amine to a solution of the unsubstituted or substituted dialkyl imidocarbonate and a cyanogen halide. The dialkyl imidocarbonate precursors are prepared by using a stoichiometric ratio (2:1) of alcohol to cyanogen halide in the presence of an acid acceptor and in a non-aqueous solvent.Dialkyl (N-cyanoimido)carbonates are useful as intermediates for pesticides and pharmaceuticals.
摘要翻译：在非水溶剂中通过以下方法制备二烷基（N-氰基亚氨基）碳酸酯，该方法包括（a）以受控的速率将氰卤化物加入到含有未取代或取代的亚氨基碳酸二烷基酯的无机碱的反应器中， /或三烷基胺，或（b）通过将三烷基胺加入到未取代或取代的酰亚胺碳酸二烷基酯和氰卤化物的溶液中。通过在酸受体和非水溶剂的存在下，使用化学计量比（2:1）的醇与氰卤化物来制备二烷基亚氨碳酸酯前体。二烷基（N-氰基亚氨基）碳酸酯可用作农药和药物的中间体。

14. 发明专利

JP2822625B2 失效
公开(公告)号：JP2822625B2
公开(公告)日：1998-11-11
申请号：JP18610890
申请日：1990-07-13
IPC分类号： C07C333/02 , C07C269/06 , C07C271/68 , C07C333/14

15. 发明专利

JPS63126856A MANUFACTURE OF DI-SUBSTITUTED IMIDOCARBONATE 失效
公开(公告)号：JPS63126856A
公开(公告)日：1988-05-30
申请号：JP25748887
申请日：1987-10-14
申请人： ICI PLC
发明人： GURAHAMU AANESUTO ROBINSON
IPC分类号： C07C271/68 , C07C20060101 , C07C67/00 , C07C239/00 , C07C261/04 , C07D317/32 , C07D317/36 , C07D319/06

16. 发明专利

JP3165871B2 失效
公开(公告)号：JP3165871B2
公开(公告)日：2001-05-14
申请号：JP18633692
申请日：1992-06-19
IPC分类号： C07C261/04 , C07C269/00 , C07C271/68

17. 发明专利

JPH0474158A N-NITRIMIDOCARBONIC ACID ESTERS AND PRODUCTION THEREOF 失效
公开(公告)号：JPH0474158A
公开(公告)日：1992-03-09
申请号：JP18610890
申请日：1990-07-13
申请人： NIPPON SODA CO
发明人： KOJIMA SHIGERU , WATAI TOSHIYUKI , IIYOSHI KOJI
IPC分类号： C07C333/02 , C07C269/06 , C07C271/68 , C07C333/14
摘要： NEW MATERIAL:N-Nitrimidocarbonic acid esters expressed by formula I (X and Y are O or S; R1 and R2 are alkyl or phenyl substituted with halogen or nitro). EXAMPLE:Dimethyl N-nitrimidodithiocarbonate. USE:Useful as an intermediate for medicines and agricultural chemicals. PREPARATION:Imidocarbonic acid esters expressed by formula II are nitrated to provide the compounds expressed by formula I. Combinations of nitric acid or salts thereof with an acid anhydride are cited as the nitrating agent. Ammo nium nitrate, etc., are cited as the salts of the nitric acid. The reaction is carried out at -50 to +100 deg.C, preferably -20 to +30 deg.C.

18. 发明专利

JPS6317055B2 失效
公开(公告)号：JPS6317055B2
公开(公告)日：1988-04-12
申请号：JP702180
申请日：1980-01-25
申请人： ICI PLC
发明人： GURAHAMU AANESUTO ROBINSON
IPC分类号： C07C271/68 , C07C20060101 , C07C67/00 , C07C239/00 , C07C261/04 , C07D317/32 , C07D317/36 , C07D319/06

19. 发明授权

US5208351A Process for the preparation of N-cyanoimidocarbonates 失效
标题翻译：制备N-氰基碳酸酯的方法
公开(公告)号：US5208351A
公开(公告)日：1993-05-04
申请号：US914268
申请日：1992-07-15
申请人： Franz Thalhammer , Stefan Weiss
发明人： Franz Thalhammer , Stefan Weiss
IPC分类号： C07C261/04 , C07C269/00 , C07C271/68 , C07D317/32 , C07D319/06
CPC分类号： C07D319/06 , C07C261/04 , C07D317/32
摘要： The present invention provides a process for the preparation of N-cyanoimidocarbonates of the general formula: ##STR1## in which R.sup.1 and R.sup.2 are the same and are alkyl radicals containing up to 4 carbon atoms or R.sup.1 and R.sup.2 are joined together to give an ethylene or propylene chain which is optionally substituted by an alkyl radical containing up to 3 carbon atoms, wherein an imidocarbonate obtained in aqueous alkaline solution from the appropriate alcohol and cyanogen chloride is added with an acid to an aqueous solution of cyanamide in such a manner that the reaction mixture has a pH value of from 3 to 8.
摘要翻译：本发明提供了制备通式如下的N-氰酰亚氨基碳酸酯的方法：其中R 1和R 2相同并且是含有至多4个碳原子的烷基，或者R 1和R 2连接在一起，得到乙烯或任选被含有至多3个碳原子的烷基取代的丙烯链，其中将由适当的醇和氯化氰在碱性水溶液中获得的酰亚胺碳酸酯加入到氰胺水溶液中，使得反应混合物的pH值为3-8。

20. 发明授权

US5081299A Fluorinated alkoxyimines and their N-chloro- and N-bromo-derivatives, and process for their preparation 失效
标题翻译：氟化烷氧基化物及其N-氯代和N-溴代衍生物及其制备方法
公开(公告)号：US5081299A
公开(公告)日：1992-01-14
申请号：US692960
申请日：1991-04-26
申请人： Darryl D. DesMarteau , Stefan P. Kotun
发明人： Darryl D. DesMarteau , Stefan P. Kotun
IPC分类号： C07C239/20 , C07C251/52 , C07C259/02 , C07C271/68
CPC分类号： C07C271/68 , C07C239/20
摘要： Novel fluorinated alkoxy imines having the formula:R.sub.x --CF.dbd.N--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (I)wherein:R.sub.x is either F or a perhalogenated alkyl group containing from 1 to 3 carbon atoms, andZ.sub.1 and Z.sub.2, either equal to, or different from, each other, are F, C1, Br, H or a perfluorinated alkyl group containing 1 to 3 carbon atoms. They are prepared by reacting a fluorinated alkoxy-amine having the formula:R.sub.x --CF.sub.2 --NH--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (V)with Kf at a temperature within the range of from 0.degree. to 100.degree. C. Furthermore, N-chloro- and N-bromo-derivatives of said fluorinated alkoxy-imines (I) are provided, which derivatives have the formulae:R.sub.x --CF.sub.2 --NCl--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (VII)andR.sub.x --CF.sub.2 --NBr--O--CZ.sub.1 Z.sub.2 --CF.sub.3 (VIII)

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