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11. 发明授权

US5013794A Polymers of diisobutylene-sulfonate alkane maleic acid derivatives 失效
标题翻译：二异丁烯磺酸烷烃马来酸衍生物的聚合物
公开(公告)号：US5013794A
公开(公告)日：1991-05-07
申请号：US475623
申请日：1990-02-06
申请人： Gunter Sackmann , Joachim Konig , Heinz Baumgen
发明人： Gunter Sackmann , Joachim Konig , Heinz Baumgen
IPC分类号： C08F267/10 , D21H17/34 , D21H21/16
CPC分类号： C08F267/10 , D21H17/34 , D21H21/16
摘要： Polymers obtainable by subjecting at least one monomer, polymerizable by free radicals, to a free-radical emulsion polymerization in the presence of a polymer of the formulae I and/or II ##STR1## in which M, n, R, R.sup.1, R.sup.2, x and y have the meanings mentioned in the description, the use of the polymers obtained for surface-sizing of paper or paper-like materials and also novel polymers of the formulae I and/or II.
摘要翻译：聚合物可以通过使至少一种可自由基聚合的单体在式I和/或II的聚合物存在下进行自由基乳液聚合，其中M，n，R R1，R2，x和y具有说明书中提到的含义，用于纸或纸状材料表面施胶的聚合物的用途，以及式I和/或II的新型聚合物。

12. 发明授权

US4568391A Sizing agents 失效
标题翻译：施胶剂
公开(公告)号：US4568391A
公开(公告)日：1986-02-04
申请号：US566644
申请日：1983-12-29
申请人： Wulf von Bonin , Hans-Ulrich Buschhaus , Ulrich Beck , Heinz Baumgen
发明人： Wulf von Bonin , Hans-Ulrich Buschhaus , Ulrich Beck , Heinz Baumgen
IPC分类号： D21H19/10 , C07C68/02 , D21H17/14 , C09K3/00 , C07C68/00
CPC分类号： D21H17/14 , C07C68/02
摘要： The invention provides new sizing agents, in particular for paper, which contain chloroformic acid esters of ester alcohols and/or carboxamide alcohols.The chloroformic acid esters in question preferably have the following idealized structure:(RCOX).sub.n R'(OCOCL).sub.m (I)whereinX=an oxygen atom or an NH radical,R=an aliphatic, araliphatic or cycloaliphatic hydrocarbon radical having 8 to 28 carbon atoms,R'=the radical of an (n+m)-functional alcohol or amino alcohol having 2 to 10 carbon atoms, where the functionality refers to the total number of OH and NH.sub.2 groups,n=an integer from 1 to 4, andm=an integer from 1 to 3.
摘要翻译：本发明提供了新的上浆剂，特别是用于纸，其含有酯醇和/或羧酰胺醇的氯甲酸酯。所讨论的氯甲酸酯优选具有以下理想化结构：（RCOX）nR'（OCOCL）m（I）其中X =氧原子或NH基，R =具有8至28的脂族，芳脂族或脂环族烃基碳原子，R'=具有2至10个碳原子的（n + m） - 官能醇或氨基醇的基团，其中官能度是指OH和NH 2基团的总数，n = 1至4的整数，m = 1〜3的整数。

13. 发明授权

US4614546A Sizes based on ketene dimers 失效
标题翻译：基于烯酮二聚体的尺寸
公开(公告)号：US4614546A
公开(公告)日：1986-09-30
申请号：US738640
申请日：1985-05-29
申请人： Wolf-Dieter Schroer , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
发明人： Wolf-Dieter Schroer , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
IPC分类号： D21H17/17 , C08L3/00
CPC分类号： D21H17/17
摘要： New aqueous sizes, in particular paper sizes, are made available which contain(a) ketene dimers of the formula ##STR1## in which R.sub.1 and R.sub.2 can be identical or different and represent hydrocarbon radicals having 6 to 30 carbon atoms,(b) amine-modified starch,(c) hydrophobic compound(s) which contain(s) one or more functional groups which are reactive towards OH groups within a pH range of 2 to 6, and(d) if desired further auxiliaries.
摘要翻译：提供新的水性尺寸，特别是纸张尺寸，其包含（a）式（I）的烯酮二聚体，其中R 1和R 2可以相同或不同，并且表示具有6至30个碳原子的烃基（ b）胺改性的淀粉，（c）含有一个或多个官能团的疏水性化合物，所述官能团在pH范围为2-6范围内对OH基团具有反应性，和（d）如果需要的话还有其他助剂。

14. 发明授权

US4596863A N-alkylimide copolymers and their use as sizing agents 失效
标题翻译： N-烷基酰亚胺共聚物及其作为上浆剂的用途
公开(公告)号：US4596863A
公开(公告)日：1986-06-24
申请号：US607103
申请日：1984-05-04
申请人： Gunter Sackmann , Ulrich Beck , Heinz Baumgen
发明人： Gunter Sackmann , Ulrich Beck , Heinz Baumgen
IPC分类号： C08F8/14 , C08F8/32 , D21H17/43 , C08F22/40 , D21D3/00
CPC分类号： C08F8/14 , C08F8/32 , D21H17/43
摘要： The present invention relates to new copolymers based on maleic anhydride/.alpha.,.beta.-unsaturated compounds and characterized in that they consist of(A) 10 to 40 mol percent of the structural element ##STR1## (B) 40 to 80 mol percent of the structural element ##STR2## and (C) 10 to 50 mol percent of the structural element ##STR3## where the total of mol percentages of (A), (B) and (C) is 100 and whereR.sub.1 =hydrogen or alkyl,R.sub.2 =hydrogen, alkyl or optionally substituted aryl,R.sub.3 =a hydrocarbon radical having 10 to 22 C atoms,R.sub.4 =a hydrocarbon radical having 10 to 22 C atoms, andX=an oxygen atom or an NR.sub.5 group where R.sub.5 represents a hydrocarbon radical having 1 to 18 C atoms.The copolymers in question are excellent active ingredients for sizing agents for paper and are suitable not only for pulp-sizing but also for surface-sizing.
摘要翻译：本发明涉及基于马来酸酐/α，β-不饱和化合物的新共聚物，其特征在于它们由（A）10〜40摩尔％的结构单元组成（I）（B）40〜80摩尔（A），（B）和（C）的总摩尔百分数为100的结构单元（II）和（C）的10〜50摩尔％的结构单元的百分比（IMA）并且其中R 1 =氢或烷基，R 2 =氢，烷基或任选取代的芳基，R 3 =具有10-22个碳原子的烃基，R4 =具有10-22个碳原子的烃基，X =氧原子或 NR5基，其中R5表示具有1至18个C原子的烃基。所述共聚物是用于纸张的上浆剂的优异活性成分，并且不仅适用于浆浆施胶，而且适用于表面施胶。

15. 发明授权

US4784727A Sizing agent and use thereof 失效
标题翻译：上浆剂及其用途
公开(公告)号：US4784727A
公开(公告)日：1988-11-15
申请号：US459314
申请日：1983-01-20
申请人： Wolf-Dieter Schroer , Joachim Probst , Ingeborg Kolb , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
发明人： Wolf-Dieter Schroer , Joachim Probst , Ingeborg Kolb , Ulrich Beck , Peter Mummenhoff , Heinz Baumgen
IPC分类号： D21H17/08 , D21H17/15 , D21H17/17 , D21H17/35 , D21H17/36 , D21H17/37 , D21H17/45 , D21H3/02
CPC分类号： D21H17/08 , D21H17/15 , D21H17/17 , D21H17/35 , D21H17/36 , D21H17/37 , D21H17/455
摘要： A sizing agent which contains from 1 to 60 parts, by weight, of a fixing and sizing accelerating agent and from 0 to 80 parts, by weight, of conventional auxiliaries per 10 parts by weight of hydrophobic, cellulose-reactive sizing materials, the fixing and sizing accelerating agent being a polymer composed of linear or branched carbon chains, to which primary, secondary or tertiary amino and/or quaternary ammonium groups are bound directly or by side chains exhibits a thorough and rapid sizing effect, in particular in the better sizing of paper.
摘要翻译：一种施胶剂，其含有1至60重量份的定影和施胶促进剂和0至80重量份的常规助剂，每10重量份疏水性纤维素反应性施胶材料，固定和作为由直链或支链碳链构成的聚合物的定型促进剂，其中伯，仲或叔氨基和/或季铵基团直接或由侧链结合，表现出彻底和快速的施胶效果，特别是在更好的施胶的纸。

16. 发明授权

US4659431A Cationic sizing agent for paper, and a process for its preparation 失效
标题翻译：用于纸张的阳离子上胶剂及其制备方法
公开(公告)号：US4659431A
公开(公告)日：1987-04-21
申请号：US691991
申请日：1985-01-16
申请人： Joachim Probst , Ulrich Beck , Heinz Baumgen
发明人： Joachim Probst , Ulrich Beck , Heinz Baumgen
IPC分类号： C08F2/00 , C08F2/24 , C08F2/28 , C08F212/00 , C08F212/08 , C08F220/00 , C08F220/10 , C08F220/12 , C08F257/02 , D21H17/35 , D21H17/37 , D21H17/45 , D21H19/20 , D21H21/16 , D21H3/38
CPC分类号： C08F257/02 , C08F2/24 , C08F212/08 , D21H17/35 , D21H17/37 , D21H17/455 , D21H21/16
摘要： New, highly effective cationic sizing agents for paper have been provided. They can be obtained by a method in which a water-soluble cationic chemically pure terpolymer compound consisting of(a) 7-40% by weight of N,N-dimethylaminoethyl acrylate and/or methacrylate,(b) 40-80% by weight of styrene and(c) 4-40% by weight of acrylonitrileis dissolved in an aqueous medium, the sum of the components (a) to (c) always being 100% by weight and at least 10% of the N,N-dimethylamino groups of the terpolymer being quaternized and the remainder being protonated, and, in the presence of 10 to 70% by weight, relative to the monomer mixture below, of this emulsifier,(d) 0 to 90% by weight of acrylonitrile and/or methacrylonitrile,(e) 5 to 95% by weight of styrene and(f) 5 to 95% by weight of acrylates and/or methacrylates having 1 to 12 C atoms in the alcohol radical,the sum of the components (d) to (f) always being 100% by weight, are emulsified, and the emulsion thus obtained is subjected to free radical-initiated emulsion polymerization at temperatures from 20.degree. to 150.degree. C.
摘要翻译：已经提供了用于纸的新的高效阳离子上胶剂。它们可以通过以下方法获得：其中由（a）7-40重量％的丙烯酸N，N-二甲基氨基乙酯和/或甲基丙烯酸酯组成的水溶性阳离子化学纯三元共聚物，（b）40-80重量％的苯乙烯和（c）4-40重量％的丙烯腈溶解在水性介质中，组分（a）至（c）的总和总是为100重量％，并且至少10重量％的N，三元共聚物的二甲基氨基被季铵化，其余部分被质子化，并且在该乳化剂相对于单体混合物的10至70重量％的存在下，（d）0至90重量％的丙烯腈和/ 或甲基丙烯腈，（e）5至95重量％的苯乙烯和（f）5至95重量％的醇基中具有1至12个碳原子的丙烯酸酯和/或甲基丙烯酸酯，组分（d）至（f）总是为100重量％，乳化，得到的乳液在20D的温度下进行自由基引发的乳液聚合 EG至150℃

17. 发明授权

US4568421A Monofluorotriazinyl compounds, processes for their preparation and their use as sizing agents 失效
标题翻译：单氟三嗪化合物，其制备方法及其作为施胶剂的用途
公开(公告)号：US4568421A
公开(公告)日：1986-02-04
申请号：US537476
申请日：1983-09-30
申请人： Gunter Sackmann , Horst Jager , Ulrich Beck , Heinz Baumgen
发明人： Gunter Sackmann , Horst Jager , Ulrich Beck , Heinz Baumgen
IPC分类号： C07D251/38 , C07D251/50 , D21H17/03 , D21H17/09 , D21H17/11 , D21H19/10 , D21H3/12
CPC分类号： C07D251/50 , D21H17/09 , D21H17/11
摘要： New monofluorotriazinyl compounds of the formula ##STR1## wherein R.sup.1 and R.sup.2 can be identical or different and represent a hydrocarbon radical with 12 to 24 C atoms andX represents an oxygen atom, a sulphur atom or the group NR.sup.3,whereinR.sup.3 denotes hydrogen or a hydrocarbon radical with 1 to 24 C atoms.In formula (1), the hydrocarbon radicals R.sup.1 and R.sup.2 preferably represent linear or branched alkyl (C.sub.12 -C.sub.24), cycloalkyl (C.sub.12 -C.sub.24) or aromatic radicals with fused-on hydroaromatic systems with 12 to 24 C atoms. The hydrocarbon radical R.sup.3 is preferably one of the abovementioned substituents or methyl.The compounds of the formula (1) are suitable as effective components in reactive sizing agents for paper.
摘要翻译：新颖的式（IMAGE）的单氟三嗪化合物，其中R 1和R 2可相同或不同，表示具有12至24个C原子的烃基，X表示氧原子，硫原子或基团NR 3，其中R 3表示氢或具有1至24个C原子的烃基。在式（1）中，烃基R 1和R 2优选表示具有12至24个C原子的具有稠合的氢芳族体系的直链或支链烷基（C 12 -C 24），环烷基（C 12 -C 24）或芳族基团。烃基R 3优选为上述取代基之一或甲基。式（1）的化合物适用于纸张的反应性施胶剂中的有效成分。

18. 发明授权

US4499153A Sizes 失效
标题翻译：尺寸
公开(公告)号：US4499153A
公开(公告)日：1985-02-12
申请号：US466708
申请日：1983-02-15
申请人： Wulf von Bonin , Peter Mummenhoff , Ulrich Beck , Heinz Baumgen
发明人： Wulf von Bonin , Peter Mummenhoff , Ulrich Beck , Heinz Baumgen
IPC分类号： D21H17/07 , C08L91/00 , B32B27/06 , D21D3/00
CPC分类号： D21H17/07 , Y10T428/31783
摘要： New products having excellent sizing action, in particular on paper are obtained by reacting .alpha.,.beta.-unsaturated carboxylic acids or their reactive derivatives (such as, for example, esters or anhydrides) with amide-amines of higher carboxylic acids at temperatures above 120.degree. C.The new products are used in size formulations, preferably as aqueous alkaline and, in particular, aqueous ammoniacal, dispersions.
摘要翻译：通过使α，β-不饱和羧酸或其反应性衍生物（例如酯或酸酐）与高于120℃的高羧酸的酰胺 - 胺反应，得到具有优异施胶作用的新产品，特别是在纸上。 C.新产品用于尺寸配方中，优选用作碱性水溶液，特别是氨水分散体。

19. 发明授权

US4418175A Cationic sizing agents for paper 失效
标题翻译：阳离子上胶剂纸
公开(公告)号：US4418175A
公开(公告)日：1983-11-29
申请号：US329721
申请日：1981-12-11
申请人： Joachim Probst , Gunter Kolb , Friedhelm Muller , Heinz Baumgen
发明人： Joachim Probst , Gunter Kolb , Friedhelm Muller , Heinz Baumgen
IPC分类号： D21H19/20 , C08F8/44 , D21H17/35 , D21H17/37 , D21H17/45 , C08F220/46
CPC分类号： D21H17/455 , C08F8/44 , D21H17/35 , D21H17/37
摘要： The aqueous solution of a statistical terpolymer containing quaternized amino groups and having a regular chemical structure of(a) from 8 to 20%, by weight, of N,N-dimethylaminoethyl acrylate and/or N,N-dimethylaminoethyl methacrylate;(b) from 45 to 80%, by weight, of styrene; and(c) from 8 to 35%, by weight, of acrylonitrile;the sum of (a) to (c) being 100%, by weight, and at least 10% of the dimethylamino groups of the terpolymer being quaternized and the remainder protonated is suitable as cationic paper sizing agent.
摘要翻译：具有季铵化氨基的统计三元共聚物的水溶液，其具有规则的化学结构（a）8至20重量％的丙烯酸N，N-二甲基氨基乙酯和/或甲基丙烯酸N，N-二甲基氨基乙酯; （b）45〜80重量％的苯乙烯; 和（c）8至35重量％的丙烯腈; （a）至（c）的总和为100重量％，并且至少10％的三元共聚物的二甲基氨基被季铵化，其余被质子化适合作为阳离子纸上胶剂。

20. 发明授权

US4481319A Low-foam surface sizing agents for paper which contain copolymeric _maleic anhydride semi-amides 失效
标题翻译：用于含有共聚马来酸酐半酰胺的纸的低泡表面施胶剂
公开(公告)号：US4481319A
公开(公告)日：1984-11-06
申请号：US410906
申请日：1982-08-24
申请人： Gunter Sackmann , Gunter Kolb , Joachim Probst , Friedhelm Muller , Heinz Baumgen
发明人： Gunter Sackmann , Gunter Kolb , Joachim Probst , Friedhelm Muller , Heinz Baumgen
IPC分类号： C08F8/32 , D21H17/35 , D21H17/43 , D21H17/45 , C08K5/21 , C08K5/05
CPC分类号： D21H17/45 , C08F8/32 , D21H17/35 , D21H17/43
摘要： Low-foam surface sizing agents for paper in the form of aqueous or aqueous-alcoholic alkali metal, amine or ammonium salt solutions of copolymers containing carboxylic acid semi-amide groups obtainable by reacting copolymers of maleic acid anhydride and diisobutylene and/or terpolymers of maleic acid anhydride, diisobutylene and a vinyl monomer copolymerizing with maleic acid anhydride, with from 5 to 50 mole percent, based on maleic acid anhydride groups, of a primary aliphatic or aromatic monoamine. The solutions may optionally contain urea or derivatives of urea.
摘要翻译：水性或水性醇碱金属形式的纸的低泡表面施胶剂，含有羧酸半酰胺基团的共聚物的胺或铵盐溶液，可通过马来酸酐和二异丁烯的共聚物和/或马来酸三元共聚物与马来酸酐共聚的酸酐，二异丁烯和乙烯基单体，基于马来酸酐基团的5-50摩尔％的伯脂肪族或芳族单胺。溶液可以任选地含有脲或尿素衍生物。

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