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11. 发明申请

US20050170255A1 Solid electrolyte comprising fluorine-containing polymer having fluorine-containing ether chains 有权
标题翻译：含有含氟醚链的含氟聚合物的固体电解质
公开(公告)号：US20050170255A1
公开(公告)日：2005-08-04
申请号：US11096056
申请日：2005-04-01
申请人： Meiten Koh , Takayuki Araki
发明人： Meiten Koh , Takayuki Araki
IPC分类号： C08F216/14 , G01N27/26 , G02F1/15 , H01B1/06 , H01B1/12 , H01G9/025 , H01G9/028 , H01G9/032 , H01G9/035 , H01G11/14 , H01G11/54 , H01G11/56 , H01G11/84 , H01M8/02 , H01M8/10 , H01M10/05 , H01M10/0565 , H01M10/40
CPC分类号： G02F1/1508 , H01B1/122 , H01G9/025 , H01G9/028 , H01G9/038 , H01G11/56 , H01M8/0289 , H01M8/1025 , H01M8/1039 , H01M8/1044 , H01M8/1048 , H01M8/1072 , Y02E60/13 , Y02P70/56
摘要： There is provided a fluorine-containing polymer solid electrolyte which has an excellent ion-conducting property, is high in oxidation resistance, is stable electrochemically and thermally, has sufficient strength and is applicable to various electrochemical devices. The electrolyte comprises (A) a non-crystalline fluorine-containing polymer having, in a trunk chain and/or side chain of the polymer molecule, a structural unit D having five or more chained units derived from a fluorine-containing ether, (B) an electrolytic compound and (C) a solvent, and has an ionic conductivity of from 10−10 to 101 S/cm measured at 25° C. by an alternating current complex impedance method. The electrolyte is useful for various electrochemical devices.
摘要翻译：提供了具有优异的离子传导性，耐氧化性高，电化学和热稳定性好的含氟聚合物固体电解质，具有足够的强度并适用于各种电化学装置。电解质包含（A）在聚合物分子的主链和/或侧链中具有5个以上来自含氟醚的链状单元的结构单元D（B）的非结晶性含氟聚合物）电解化合物和（C）溶剂，并且在25℃下通过交替地测量的离子电导率为10 -10 -10 10 S / cm 当前复阻抗法。电解质可用于各种电化学装置。

12. 发明授权

US07553589B2 Solid electrolyte comprising fluorine-containing polymer having fluorine-containing ether chains 有权
标题翻译：含有含氟醚链的含氟聚合物的固体电解质
公开(公告)号：US07553589B2
公开(公告)日：2009-06-30
申请号：US11157957
申请日：2005-06-22
申请人： Takayuki Araki , Meiten Koh
发明人： Takayuki Araki , Meiten Koh
IPC分类号： H01M10/40
CPC分类号： H01G9/028 , H01B1/122 , H01G9/038 , H01G11/56 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M10/052 , H01M10/0565 , H01M2300/0082 , Y02E60/13
摘要： There is provided a fluorine-containing polymer solid electrolyte which has an excellent ion-conducting property, is high in oxidation resistance, is stable electrochemically and thermally, has sufficient strength and is applicable to various electrochemical devices. The electrolyte comprises (I) a non-crystalline fluorine-containing polymer which has a polar nonionic functional group and has, in a side chain of the polymer molecule, a structural unit D having 1 to 4 units derived from a fluorine-containing ether in the form of continuous chain, (II) an electrolytic compound and as case demands, (III) a solvent. The electrolyte has an ionic conductivity of from 10−10 to 101 S/cm measured at 25° C. by an alternating current complex impedance method, and is useful for various electrochemical devices.
摘要翻译：提供了具有优异的离子传导性，耐氧化性高，电化学和热稳定性好的含氟聚合物固体电解质，具有足够的强度并适用于各种电化学装置。电解质包含（I）具有极性非离子官能团的非结晶性含氟聚合物，在聚合物分子的侧链中，具有1〜4个由含氟醚衍生的单元的结构单元D 连续链的形式，（II）电解化合物，如果需要，（III）溶剂。电解质在25℃下通过交流复阻抗法测得的10-10至101S / cm的离子电导率，并且可用于各种电化学装置。

13. 发明申请

US20090291369A1 SOLID ELECTROLYTE COMPRISING FLUORINE-CONTAINING POLYMER HAVING FLUORINE-CONTAINING ETHER CHAINS 有权
标题翻译：包含含荧氟醚的含氟聚合物的固体电解质
公开(公告)号：US20090291369A1
公开(公告)日：2009-11-26
申请号：US12471860
申请日：2009-05-26
申请人： Takayuki Araki , Meiten Koh
发明人： Takayuki Araki , Meiten Koh
IPC分类号： H01M6/18 , H01G9/028
CPC分类号： H01G9/028 , H01B1/122 , H01G9/038 , H01G11/56 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M10/052 , H01M10/0565 , H01M2300/0082 , Y02E60/13
摘要： There is provided a fluorine-containing polymer solid electrolyte which has an excellent ion-conducting property, is high in oxidation resistance, is stable electrochemically and thermally, has sufficient strength and is applicable to various electrochemical devices. The electrolyte comprises (I) a non-crystalline fluorine-containing polymer which has a polar nonionic functional group and has, in a side chain of the polymer molecule, a structural unit D having 1 to 4 units derived from a fluorine-containing ether in the form of continuous chain, (II) an electrolytic compound and as case demands, (III) a solvent. The electrolyte has an ionic conductivity of from 10−10 to 101 S/cm measured at 25° C. by an alternating current complex impedance method, and is useful for various electrochemical devices.
摘要翻译：提供了具有优异的离子传导性，耐氧化性高，电化学和热稳定性好的含氟聚合物固体电解质，具有足够的强度并适用于各种电化学装置。电解质包含（I）具有极性非离子官能团的非结晶性含氟聚合物，在聚合物分子的侧链中，具有1〜4个由含氟醚衍生的单元的结构单元D 连续链的形式，（II）电解化合物，如果需要，（III）溶剂。电解质在25℃下通过交流复阻抗法测得的10-10至101S / cm的离子电导率，并且可用于各种电化学装置。

14. 发明申请

US20070172763A1 Fluorine-containing ethylenic monomer having hydroxyl group or fluoroalkyl carbonyl group and fluorine-containing polymer prepared by polymerization of same 审中-公开
公开(公告)号：US20070172763A1
公开(公告)日：2007-07-26
申请号：US11727908
申请日：2007-03-29
申请人： Takayuki Araki , Yuzo Komatsu , Meiten Koh
发明人： Takayuki Araki , Yuzo Komatsu , Meiten Koh
IPC分类号： G03C1/00 , C08F12/20 , C07C43/17
CPC分类号： G03F7/091 , C07C33/423 , C07C43/178 , C07C45/45 , C07C49/227 , C07C49/255 , C08F16/04 , C08F16/34 , C08F216/04 , G03F7/0046 , G03F7/0382 , G03F7/0392
摘要： There are provided a fluorine-containing ethylenic monomer having hydroxyl group or fluoroalkyl carbonyl group and represented by the formula (1): and the formula (14): respectively, wherein X1 and X2 are the same or different and each is H or F; X3 is H, F, Cl or CF3; Rf1 and Rf2 are the same or different and each is a perfluoroalkyl group having 1 to 20 carbon atoms; Rf3 is a fluorine-containing alkylene group having 1 to 40 carbon atoms or a fluorine-containing alkylene group having ether bond which has 1 to 100 carbon atoms and the sum of carbon atom and oxygen atom of two or more; a is 0 or 1, a fluorine-containing polymer having a structural unit of the above-mentioned monomer and a composition for a photoresist. The monomer has good polymerizability, particularly radical polymerizability, and the polymer obtained by polymerizing the monomer has excellent optical characteristics and is useful as a base polymer for an antireflection film and for a composition for a resist.

15. 发明授权

US08034490B2 Solid electrolyte comprising fluorine-containing polymer having fluorine-containing ether chains 有权
标题翻译：含有含氟醚链的含氟聚合物的固体电解质
公开(公告)号：US08034490B2
公开(公告)日：2011-10-11
申请号：US12471860
申请日：2009-05-26
申请人： Takayuki Araki , Meiten Koh
发明人： Takayuki Araki , Meiten Koh
IPC分类号： H01M10/40
CPC分类号： H01G9/028 , H01B1/122 , H01G9/038 , H01G11/56 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M10/052 , H01M10/0565 , H01M2300/0082 , Y02E60/13
摘要： There is provided a fluorine-containing polymer solid electrolyte which has an excellent ion-conducting property, is high in oxidation resistance, is stable electrochemically and thermally, has sufficient strength and is applicable to various electrochemical devices. The electrolyte comprises (I) a non-crystalline fluorine-containing polymer which has a polar nonionic functional group and has, in a side chain of the polymer molecule, a structural unit D having 1 to 4 units derived from a fluorine-containing ether in the form of continuous chain, (II) an electrolytic compound and as case demands, (III) a solvent. The electrolyte has an ionic conductivity of from 10—10 to 101 S/cm measured at 25° C. by an alternating current complex impedance method, and is useful for various electrochemical devices.
摘要翻译：提供了具有优异的离子传导性，耐氧化性高，电化学和热稳定性好的含氟聚合物固体电解质，具有足够的强度并适用于各种电化学装置。电解质包含（I）具有极性非离子官能团的非结晶性含氟聚合物，在聚合物分子的侧链中，具有1〜4个由含氟醚衍生的单元的结构单元D 连续链的形式，（II）电解化合物，如果需要，（III）溶剂。电解质在25℃下通过交流复阻抗法测得的10-10至101S / cm的离子电导率，并且可用于各种电化学装置。

16. 发明申请

US20070196763A1 Method of forming laminated resist 审中-公开
标题翻译：形成层压抗蚀剂的方法
公开(公告)号：US20070196763A1
公开(公告)日：2007-08-23
申请号：US10579855
申请日：2004-11-15
申请人： Takayuki Araki , Meiten Koh , Kazuyuki Sato , Mihoko Ohashi , Yosuke Kishikawa
发明人： Takayuki Araki , Meiten Koh , Kazuyuki Sato , Mihoko Ohashi , Yosuke Kishikawa
IPC分类号： G03C11/12
CPC分类号： G03F7/0046 , C09D133/16 , G03F7/091
摘要： There is formed a laminated resist which exhibits sufficient reflection reducing effect in a photolithography process using light of vacuum ultraviolet region and also has sufficient developing characteristics in a developing process. The method of forming the laminated photoresist comprises (I) a step for forming the photoresist layer (L1) on a substrate and (II) a step for forming the antireflection layer (L2) on the photoresist layer (L1) by applying the coating composition containing the fluorine-containing polymer (A) having hydrophilic group Y. The fluorine-containing polymer (A) contains a structural unit derived from a fluorine-containing ethylenic monomer having hydrophilic group Y and is characterized in that (i) the hydrophilic group Y contains an acidic OH group having a pKa value of not more than 11, (ii) a fluorine content is not less than 50% by mass, and (iii) the number of moles of the hydrophilic group Y in 100 g of the fluorine-containing polymer (A) is not less than 0.14.
摘要翻译：形成层叠抗蚀剂，其在使用真空紫外线区域的光的光刻工艺中表现出足够的反射降低效果，并且在显影过程中也具有足够的显影特性。形成层叠光致抗蚀剂的方法包括：（I）在基板上形成光致抗蚀剂层（L1）的工序，（II）在光致抗蚀剂层（L1）上形成抗反射层（L 2）的工序，含有具有亲水基团Y的含氟聚合物（A）的涂料组合物。含氟聚合物（A）含有由具有亲水性基团Y的含氟乙烯性单体衍生的结构单元，其特征在于，（i）亲水性基团Y含有pKa值不大于11的酸性OH基，（ii）氟含量不小于50质量％，和（iii）100g的亲水基Y的摩尔数含氟聚合物（A）不低于0.14。

17. 发明申请

US20050233221A1 Solid electrolyte comprising fluorine-containing polymer having fluorine-containing ether chains 有权
标题翻译：含有含氟醚链的含氟聚合物的固体电解质
公开(公告)号：US20050233221A1
公开(公告)日：2005-10-20
申请号：US11157957
申请日：2005-06-22
申请人： Takayuki Araki , Meiten Koh
发明人： Takayuki Araki , Meiten Koh
IPC分类号： G01N27/406 , H01B1/06 , H01B1/12 , H01G9/028 , H01G9/032 , H01G9/035 , H01G11/54 , H01G11/56 , H01M8/02 , H01M8/10 , H01M10/40 , H01G9/025
CPC分类号： H01G9/028 , H01B1/122 , H01G9/038 , H01G11/56 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M10/052 , H01M10/0565 , H01M2300/0082 , Y02E60/13
摘要： There is provided a fluorine-containing polymer solid electrolyte which has an excellent ion-conducting property, is high in oxidation resistance, is stable electrochemically and thermally, has sufficient strength and is applicable to various electrochemical devices. The electrolyte comprises (I) a non-crystalline fluorine-containing polymer which has a polar nonionic functional group and has, in a side chain of the polymer molecule, a structural unit D having 1 to 4 units derived from a fluorine-containing ether in the form of continuous chain, (II) an electrolytic compound and as case demands, (III) a solvent. The electrolyte has an ionic conductivity of from 10−10 to 101 S/cm measured at 25° C. by an alternating current complex impedance method, and is useful for various electrochemical devices.
摘要翻译：提供了具有优异的离子传导性，耐氧化性高，电化学和热稳定性好的含氟聚合物固体电解质，具有足够的强度并适用于各种电化学装置。电解质包含（I）具有极性非离子官能团的非结晶性含氟聚合物，在聚合物分子的侧链中，具有1〜4个由含氟醚衍生的单元的结构单元D 连续链的形式，（II）电解化合物，如果需要，（III）溶剂。电解质在25℃下通过交流复阻抗法测得的离子电导率为10 -10 -10 10 S / cm，可用于各种电化学装置。

18. 发明申请

US20070129576A1 Process for preparing fluorine-containing norbornene derivative 失效
标题翻译：含氟降冰片烯衍生物的制备方法
公开(公告)号：US20070129576A1
公开(公告)日：2007-06-07
申请号：US11649265
申请日：2007-01-04
申请人： Takayuki Araki , Takuji Ishikawa , Takuji Kume , Akinori Yamamoto
发明人： Takayuki Araki , Takuji Ishikawa , Takuji Kume , Akinori Yamamoto
IPC分类号： C07C45/45
CPC分类号： G03F7/0395 , C07C33/44 , C07C43/313 , C07C45/45 , C07C49/567 , C07C61/28 , C07C69/96 , C07C2602/42 , C07C2603/86 , G03F7/0046 , G03F7/0382
摘要： There are provided a novel norbornene derivative which is a material for a chemically amplifying type photoresist for F2 laser, possesses excellent transparency and improved dry etching resistivity and has a fluorine-containing ketone unit or fluorine-containing tertiary alcohol unit directly bonded to the norbornene backbone; a fluorine-containing polymer obtained by using the norbornene derivative as a copolymerizable monomer; and a chemically amplifying type photoresist composition comprising the fluorine-containing polymer, a photoacid generator and a solvent.
摘要翻译：提供了一种新颖的降冰片烯衍生物，其是用于F 2激光的化学放大型光致抗蚀剂的材料，具有优异的透明度和改善的干蚀刻电阻率，并且具有含氟酮单元或含氟三级直接与降冰片烯骨架结合的醇单元; 通过使用降冰片烯衍生物作为可共聚单体得到的含氟聚合物; 以及包含含氟聚合物，光致酸产生剂和溶剂的化学放大型光致抗蚀剂组合物。

19. 发明授权

US07163982B2 Process for preparing fluorine-containing polymer and method of forming fine pattern using same 失效
标题翻译：制备含氟聚合物的方法和使用其形成精细图案的方法
公开(公告)号：US07163982B2
公开(公告)日：2007-01-16
申请号：US10914203
申请日：2004-08-10
申请人： Takayuki Araki , Tetsuhiro Kodani , Takuji Ishikawa
发明人： Takayuki Araki , Tetsuhiro Kodani , Takuji Ishikawa
IPC分类号： C08F8/32
CPC分类号： C08F12/20 , G03F7/0046 , G03F7/0395
摘要： There is provided a method of forming a fine pattern by using a practicable fluorine-containing polymer which has a high transparency to exposure light having a short wavelength such as F2 laser and can undergo resolution of a fine pattern. The method comprises (I) a step for preparing a fluorine-containing polymer (A) having OH group which has a structural unit derived from a fluorine-containing norbornene derivative having OH group, (II) a step for preparing a fluorine-containing polymer (B) having a protective group by reacting a compound represented by X—CH2OR, wherein X is Cl, Br or I; R is a hydrocarbon group having 1 to 30 carbon atoms in which a part or the whole of hydrogen atoms may be substituted with fluorine atoms, with the above-mentioned fluorine-containing polymer (A) having OH group in the presence of a base, (III) a step for preparing a resist composition comprising (a) the above-mentioned fluorine-containing polymer (B) having a protective group, (b) a photoacid generator and (c) a solvent, (IV) a step for forming a resist film comprising the above-mentioned resist composition on a substrate or on a given layer on the substrate, (V) a step for exposing by selectively irradiating a given area of the resist film with energy rays, and (VI) a step for subjecting the exposed resist film to developing to selectively remove the exposed portion of the resist film, thus forming a fine pattern.
摘要翻译：提供了通过使用对具有短波长的曝光光如F 2激光具有高透明度的可行的含氟聚合物来形成精细图案的方法，并且可以经历精细图案的分辨。该方法包括：（I）具有OH基的含氟聚合物（A）的制备步骤，其具有衍生自具有OH基的含氟降冰片烯衍生物的结构单元，（II）制备含氟聚合物的步骤（B）通过使由X-CH 2 OR表示的化合物与其中X为Cl，Br或I的化合物反应而具有保护基; R是具有1至30个碳原子的烃基，其中一部分或全部氢原子可以被氟原子取代，上述含碱基的含氟聚合物（A）具有OH基团，（III）制备抗蚀剂组合物的步骤，包括（a）具有保护基的上述含氟聚合物（B），（b）光致酸产生剂和（c）溶剂，（IV）形成步骤在基板上或基板上的给定层上包含上述抗蚀剂组合物的抗蚀剂膜，（V）通过用能量射线选择性地照射抗蚀剂膜的给定区域来曝光的步骤，以及（VI）使曝光的抗蚀剂膜显影以选择性地除去抗蚀剂膜的暴露部分，从而形成精细图案。

20. 发明授权

US07649118B2 Process for preparing fluorine-containing norbornene derivative 失效
标题翻译：含氟降冰片烯衍生物的制备方法
公开(公告)号：US07649118B2
公开(公告)日：2010-01-19
申请号：US11649265
申请日：2007-01-04
申请人： Takayuki Araki , Takuji Ishikawa , Takuji Kume , Akinori Yamamoto
发明人： Takayuki Araki , Takuji Ishikawa , Takuji Kume , Akinori Yamamoto
IPC分类号： C07C45/00
CPC分类号： G03F7/0395 , C07C33/44 , C07C43/313 , C07C45/45 , C07C49/567 , C07C61/28 , C07C69/96 , C07C2602/42 , C07C2603/86 , G03F7/0046 , G03F7/0382
摘要： There are provided a novel norbornene derivative which is a material for a chemically amplifying type photoresist for F2 laser, possesses excellent transparency and improved dry etching resistivity and has a fluorine-containing ketone unit or fluorine-containing tertiary alcohol unit directly bonded to the norbornene backbone; a fluorine-containing polymer obtained by using the norbornene derivative as a copolymerizable monomer; and a chemically amplifying type photoresist composition comprising the fluorine-containing polymer, a photoacid generator and a solvent.
摘要翻译：提供了一种新型的降冰片烯衍生物，它是用于F2激光的化学放大型光致抗蚀剂的材料，具有优异的透明性和改善的干蚀刻电阻率，并且具有直接键合在降冰片烯骨架上的含氟酮单元或含氟叔醇单元 ; 通过使用降冰片烯衍生物作为可共聚单体得到的含氟聚合物; 以及包含含氟聚合物，光致酸产生剂和溶剂的化学放大型光致抗蚀剂组合物。

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