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11. 发明授权

US5026791A Aromatic carbonate polymer composition 失效
标题翻译：芳香族碳酸酯聚合物组合物
公开(公告)号：US5026791A
公开(公告)日：1991-06-25
申请号：US407371
申请日：1989-09-14
申请人： Christopher M. Hawkins , Robert R. Gallucci , John S. Razzano
发明人： Christopher M. Hawkins , Robert R. Gallucci , John S. Razzano
IPC分类号： C08K3/00 , C08G64/00 , C08G64/18 , C08G77/42 , C08G77/448 , C08K3/10 , C08K5/36 , C08K5/42 , C08L69/00 , C08L83/04 , C08L83/10
CPC分类号： C08G64/186 , C08G77/448
摘要： A composition comprising an aromatic carbonate polymer wherein in the backbone of said polymer there is a siloxane unit of the structure below ##STR1## wherein n is an integer of one to about 100, R and R' are each selected from the group consisting of alkyl of one to twelve carbon atoms, inclusive, cycloalkyl of four to eight carbon atoms, inclusive, aryl or six to twenty carbon atoms, inclusive, aryl substituted alkyl of seven to twenty two carbon atoms, inclusive, and A ##STR2## wherein p is an integer of zero to about 4, R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5, are the same or different and are selected from hydrogen, alkyl of one to six carbon atoms, inclusive, and with the proviso that there is sufficient A present that the flame retardance of the polymer is enhanced compared to the polymer without the said siloxane unit.

12. 发明申请

US20080090985A1 PROCESS FOR PRODUCING CONTROLLED VISCOSITY FLUOROSILICONE POLYMERS 审中-公开
公开(公告)号：US20080090985A1
公开(公告)日：2008-04-17
申请号：US11549139
申请日：2006-10-13
申请人： Nancy E. Gosh , John S. Razzano , Anping Wang
发明人： Nancy E. Gosh , John S. Razzano , Anping Wang
IPC分类号： C08G77/06
CPC分类号： C08G77/06 , C08G77/24
摘要： A process for making a fluorosilicone M″DaDFbM′ with M″=(OH)R6R7SiO1/2 or (OH)R4R5SiO1/2 and is chosen independently of M′; M′=(OH)R6R7SiO1/2 or (OH)R4R5SiO1/2 and is chosen independently of M″; D=R4R5SiO2/2; and DF=R6R7SiO2/2; where the subscript a is zero or positive, the subscript b is positive and the subscripts a and b satisfy the following relationship: b>0.4(a+b) and R1 is selected from the group of 1 to 20 carbon atom monovalent alkyl, aryl, or alkaryl hydrocarbon radicals and terminally unsaturated alkenyl groups of from 2 to 10 carbon atoms; R2, R3 are each independently any monovalent hydrocarbon radical: alkyl, aryl, or alkaryl of from 1 to 20 carbon atoms or R1 and each R4 and R5 are any monovalent hydrocarbon radical: alkyl, aryl, alkenyl, or alkaryl of from 1 to 20 carbon atoms, and R6 is a fluorine substituted 3 to 20 carbon atom monovalent hydrocarbon radical having no fluorine substitution on the alpha or beta carbon atoms of the radical and R7 is any monovalent hydrocarbon radical: alkyl, aryl, or alkaryl of from 1 to 20 carbon atoms or R6 by reacting 1) b moles of (R6R7SiO)3, with 2) a moles of (R4R5SiO)3, 3) water and 4) an oxygenated promoter. Compositions made by the process and articles of manufacture made from the compositions.

13. 发明授权

US06492479B2 Process for producing fluorosilicon polymers 失效
标题翻译：制备氟硅聚合物的方法
公开(公告)号：US06492479B2
公开(公告)日：2002-12-10
申请号：US09935317
申请日：2001-08-22
申请人： John S. Razzano , Nancy E. Gosh
发明人： John S. Razzano , Nancy E. Gosh
IPC分类号： C08G7708
CPC分类号： C08G77/24 , C08G77/08
摘要： The invention comprises a method for producing fluorosilicone oil by reacting a fluorosilicone trimer with a triorganosilanol in the presence of an alkali silanolate. The polymer may be condensed to increase viscosity and decrease the silanol content of the polymer, and volatiles may be removed by stripping. The method provides a high yield of fluorosilicone oil of narrow viscosity ranges in an efficient reaction, and produces small amounts of waste.
摘要翻译：本发明包括在碱性硅铝酸盐存在下使氟硅酮三聚体与三有机硅烷醇反应生产氟硅油的方法。可以将聚合物缩合以增加聚合物的粘度和降低硅烷醇含量，并且挥发物可以通过汽提除去。该方法在有效的反应中提供了具有窄粘度范围的高产率的氟硅油，并且产生少量的废物。

14. 发明授权

US5739370A Process the production of octaphenylcyclotetrasiloxane 失效
标题翻译：处理八苯基环四硅氧烷的生产
公开(公告)号：US5739370A
公开(公告)日：1998-04-14
申请号：US825863
申请日：1997-04-29
申请人： John S. Razzano
发明人： John S. Razzano
IPC分类号： C07F7/08 , C07F7/21
CPC分类号： C07F7/0874 , C07F7/21
摘要： A base catalyzed hydrolysis of dialkoxydiphenylsilanes or dialkoxymethylphenylsilanes in a solvent or solvent mixture wherein dialkoxydiphenylsilanes or dialkoxymethylphenylsilanes are soluble but in which octaphenylcyclotetrasiloxane or tetramethyltetraphenyl-cyclotetrasiloxane is sparingly soluble or insoluble provides for a process to prepare octaphenylcyclotetrasiloxane or sym-tetramethyltetraphenyl-cyclotetrasiloxane in high yield.
摘要翻译：二烷氧基二苯基硅烷或二烷氧基甲基苯基硅烷在溶剂或溶剂混合物中的碱催化水解，其中二烷氧基二苯基硅烷或二烷氧基甲基苯基硅烷是可溶的，但其中八苯基环四硅氧烷或四甲基四苯基四环四硅氧烷是微溶或不溶的，提供了以高产率制备八苯基环四硅氧烷或对四甲基四苯基四环四硅氧烷的方法。

15. 发明授权

US5670596A Production of low molecular weight linear hydrogen siloxanes 失效
标题翻译：生产低分子线性氢硅氧烷
公开(公告)号：US5670596A
公开(公告)日：1997-09-23
申请号：US623340
申请日：1996-03-27
申请人： John S. Razzano , Patricia P. Anderson , Robert J. Perry
发明人： John S. Razzano , Patricia P. Anderson , Robert J. Perry
IPC分类号： C08G77/10 , C07F7/08 , C08G77/04 , C08G77/06 , C08G77/08 , C08G77/12 , C08G77/22
CPC分类号： C08G77/10 , C07F7/0874 , C08G77/045 , C08G77/08 , C08G77/12 , Y02P20/582
摘要： A batch or continuous process for the production of low molecular weight hydrogen siloxanes catalyzed by soluble phosphonitrilic halides or solid acid catalysts such as acid washed clays, zeolites and ion exchange resins.
摘要翻译：用于生产低分子量氢硅氧烷的分批或连续方法，由可溶性三氯化鏻或固体酸催化剂如酸洗的粘土，沸石和离子交换树脂催化。

16. 发明授权

US4028338A Fluorosiloxydiphenylsiloxy block copolymers 失效
标题翻译：氟硅氧基二苯基甲硅烷氧基嵌段共聚物
公开(公告)号：US4028338A
公开(公告)日：1977-06-07
申请号：US621032
申请日：1975-10-09
申请人： John S. Razzano
发明人： John S. Razzano
IPC分类号： C08G77/00 , C08G77/06 , C08G77/22 , C08G77/24 , C08G77/42 , C08G77/44 , C08G77/04
CPC分类号： C08G77/22 , C08G77/24 , C08G77/44
摘要： There is provided by the present invention a solvent resistant block copolymer having desirable processability comprising a copolymer of the formula, ##STR1## WHERE R is an alkyl radical of 1 to 3 carbon atoms, R.sup.1 is a perfluoroalkyl radical of 1 to 8 carbon atoms, Vi is vinyl, B is selected from the class consisting of lithium and hydrogen, x varies from 20 to 400 and y varies from 700 to 6000 and z varies from 0 to 100.There is also provided by the present invention an advantageous process for producing the above block copolymer.
摘要翻译：本发明提供了具有所需加工性的耐溶剂嵌段共聚物，其包含下式的共聚物，其中R是1至3个碳原子的烷基，R1是1至8个碳原子的全氟烷基， Vi是乙烯基，B选自锂和氢组成的组，x从20变化到400，y从700变化到6000，z从0变化到100。

17. 发明申请

US20120046488A1 SOLVENTLESS PROCESS TO PRODUCE AROMATIC GROUP-CONTAINING ORGANOSILANES 审中-公开
标题翻译：无溶剂工艺生产含芳族基团的有机硅
公开(公告)号：US20120046488A1
公开(公告)日：2012-02-23
申请号：US13211777
申请日：2011-08-17
申请人： Paul R. Willey , John S. Razzano
发明人： Paul R. Willey , John S. Razzano
IPC分类号： C07F7/08
CPC分类号： C07F7/122 , C07F7/0827
摘要： Disclosed herein is a process for producing an aromatic group-containing organosilane, The process includes reacting a reaction mixture comprising an aromatic organic compound of the formula R1X and a halosilane or alkoxysilane represented by the formula R2aSiZ4-a in the presence of magnesium metal in order to produce the organosilane with the proviso that said reaction mixture is essentially free of any organic solvent, wherein R1 is an aryl group, each R2 is independently a phenyl group, a vinyl group or a C1-C4 alkyl group, X is chlorine or bromine, Z is chlorine, bromine or alkoxy, and a has a value of 0, 1, 2, or 3.
摘要翻译：本发明公开了含有芳基的有机硅烷的制备方法，该方法包括在镁金属存在下使包含式R 1 X的芳族有机化合物和由式R 2aSiZ 4-a表示的卤代硅烷或烷氧基硅烷反应的反应混合物反应以产生有机硅烷，条件是所述反应混合物基本上不含任何有机溶剂，其中R 1是芳基，每个R 2独立地是苯基，乙烯基或C 1 -C 4烷基，X是氯或溴 Z为氯，溴或烷氧基，a为0,1,2或3。

18. 发明授权

US07671161B2 Process for producing controlled viscosity fluorosilicone polymers 有权
标题翻译：生产受控粘度氟硅氧烷聚合物的方法
公开(公告)号：US07671161B2
公开(公告)日：2010-03-02
申请号：US11549137
申请日：2006-10-13
申请人： Nancy E. Gosh , John S. Razzano , Anping Wang
发明人： Nancy E. Gosh , John S. Razzano , Anping Wang
IPC分类号： C08G77/24
CPC分类号： C08G77/24
摘要： A process for making a fluorosilicone MDaDFbM′ where M=R1R2R3SiO1/2; M′=(OH)R6R7SiO1/2 or (OH)R4R5SiO1/2; D=R4R5SiO2/2; and DF=R6R7SiO2/2; where the subscript a is zero or positive, the subscript b is positive and the subscripts a and b satisfy the following relationship: b>0.4(a+b) and R1 is selected from the group of 1 to 20 carbon atom monovalent alkyl, aryl, or alkaryl hydrocarbon radicals and terminally unsaturated alkenyl groups of from 2 to 10 carbon atoms; R2, R3 are each independently any monovalent hydrocarbon radical: alkyl, aryl, or alkaryl of from 1 to 20 carbon atoms or R1 and each R4 and R5 are any monovalent hydrocarbon radical: alkyl, aryl, alkenyl, or alkaryl of from 1 to 20 carbon atoms, and R6 is a fluorine substituted 3 to 20 carbon atom monovalent hydrocarbon radical having no fluorine substitution on the alpha or beta carbon atoms of the radical and R7 is any monovalent hydrocarbon radical: alkyl, aryl, or alkaryl of from 1 to 20 carbon atoms or R6 by reacting 1) b moles of (R6R7SiO)3, with 2) a moles of (R4R5SiO)3, 3) R1R2R3SiOH and 4) an oxygenated promoter. Compositions made by the process and articles of manufacture made from the compositions.
摘要翻译：制备氟硅酮MDaDFbM的方法，其中M = R 1 R 2 R 3 SiO 1/2; M'=（OH）R6R7SiO1 / 2或（OH）R4R5SiO1 / 2; D = R4R5SiO2 / 2; DF = R6R7SiO2 / 2; 其中下标a为零或正，下标b为正，下标a和b满足以下关系：b> 0.4（a + b），R1选自1至20个碳原子的一价烷基，芳基或烷芳基烃基和具有2-10个碳原子的末端不饱和烯基; R 2，R 3各自独立地为任何一价烃基：具有1-20个碳原子的烷基，芳基或烷芳基或R 1，并且每个R 4和R 5是任何一价烃基：1至20的烷基，芳基，链烯基或烷芳基碳原子，R6是氟取代的3〜20个碳原子，在基团的α或β碳原子上不具有氟取代的一价烃基，R 7是任何一价烃基：1至20的烷基，芳基或烷芳基碳原子或R6通过使1）b摩尔的（R6R7SiO）3与2）摩尔的（R 4 R 5 SiO）3,3）R 1 R 2 R 3 SiOH和4）含氧促进剂反应。由组合物制成的方法和制品制成的组合物。

19. 发明授权

US06433204B1 Process for making silanol stopped oligomeric materials 失效
标题翻译：制备硅烷醇停止的低聚物的方法
公开(公告)号：US06433204B1
公开(公告)日：2002-08-13
申请号：US10055199
申请日：2002-01-23
申请人： Nancy E. Gosh , John S. Razzano , Slawomir Rubinsztajn
发明人： Nancy E. Gosh , John S. Razzano , Slawomir Rubinsztajn
IPC分类号： C07F708
CPC分类号： C07F7/0876
摘要： A process for the production of linear silanol stopped siloxanes comprising: a) conducting a ring opening polymerization of a hexaorganocyclotrisiloxane having the formula: D3=(R1R2SiO)3 where R1 and R2 are independently selected from the group of one to forty carbon atom monovalent radicals, in a solvent comprising a mixture of water and a volatile polar aprotic organic solvent in the presence of catalytic amounts of a strong base; b) neutralizing the catalytic amount of the strong base with a partially neutralized salt of a polybasic acid wherein the pH ranges from about 6 to about 8; and c) washing with water.
摘要翻译：一种制备线性硅烷醇封端硅氧烷的方法，包括：a）进行下式的六有机环三硅氧烷的开环聚合：其中R1和R2独立地选自一至四十个碳原子的一价基团，在包含在催化量的强碱存在下，水与挥发性极性非质子有机溶剂的混合物; b）用多碱的部分中和盐中和强碱的催化量，其中pH范围为约6至约8; 和c）用水洗涤。

20. 发明授权

US4755370A Purification of silicon halides 失效
标题翻译：卤化硅的纯化
公开(公告)号：US4755370A
公开(公告)日：1988-07-05
申请号：US712913
申请日：1985-03-18
申请人： William D. Kray , John S. Razzano
发明人： William D. Kray , John S. Razzano
IPC分类号： C01B33/107
CPC分类号： C01B33/10778
摘要： A method for the selective removal of boron halides and other Lewis acid-type impurities from silicon halides is disclosed. Treatment of contaminated silicon halides with siloxanes, which react with the impurities, allow the distillation of silicon halide which is virtually free from contamination within extremely low limits of detectability.
摘要翻译：公开了从卤化硅中选择性除去卤化硼和其它路易斯酸型杂质的方法。使用与杂质反应的硅氧烷处理受污染的硅卤化物，允许在极低的可检测限度内实际上没有污染的卤化硅蒸馏。

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