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11. 发明授权

US4330662A Ordered copolyestercarbonate resins 失效
标题翻译：有序共聚酯碳酸酯树脂
公开(公告)号：US4330662A
公开(公告)日：1982-05-18
申请号：US200759
申请日：1980-10-27
申请人： Stephen E. Bales
发明人： Stephen E. Bales
IPC分类号： C08G63/00 , C08G63/64 , C08G63/12
CPC分类号： C08G63/64
摘要： Ordered copolyestercarbonate resins having repeating units of the formula: ##STR1## wherein a portion of R.sup.1 is meta-phenylene and a portion of R.sub.1 is para-phenylene and R is independently an aromatic hydrocarbylene or inertly substituted aromatic hydrocarbylene, e.g., ##STR2## exhibit physical properties such as heat resistance, clarity and impact strength that are superior to the comparable properties of corresponding random copolymers. They exhibit melt processability that is superior to the melt processability of corresponding copolyestercarbonates wherein R.sup.1 is entirely para-phenylene. They exhibit heat resistance, notch sensitivity and low temperature impact resistance that are superior to comparable properties of corresponding copolyestercarbonates wherein R.sup.1 is entirely meta-phenylene. Such resins are useful for making transparent tough films and molded articles having high heat resistance.
摘要翻译：具有下式重复单元的有序共聚酯碳酸酯树脂：其中R1的一部分是间亚苯基，R 1的一部分是对亚苯基，R独立地是芳族亚烃基或惰性取代的芳族亚烃基，例如，诸如耐热性，透明度和冲击强度的物理性能优于相应无规共聚物的可比性能。它们表现出优于相应的共聚酯碳酸酯的熔融加工性的熔融加工性，其中R1是完全对亚苯基。它们表现出耐热性，切口灵敏度和耐低温冲击性，其优于相应的共聚酯碳酸酯的性能，其中R1完全是间 - 亚苯基。这种树脂可用于制造具有高耐热性的透明韧性薄膜和模制品。

12. 发明授权

US5837032A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5837032A
公开(公告)日：1998-11-17
申请号：US382032
申请日：1995-02-10
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12
CPC分类号： C01B13/0251 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062
摘要： This invention relates to a method of an apparatus and method for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures at or slightly above the freezing point of any liquid present so as to achieve superior separator of gas components. The composition of certain monomers and polymers are claimed.
摘要翻译： PCT No.PCT / US93 / 07696 Sec。 371日期1995年2月10日 102（e）1995年2月10日PCT PCT 1993年8月13日PCT公布。出版物WO94 / 04250 日本特开1994年3月3日本发明涉及一种使用玻璃状聚合物膜在气体混合物中分离组分气体的装置和方法的方法，所述气体混合物在存在的任何液体的冰点处或稍高于所存在的任何液体的冰点处，以便获得优异的气体分离器组件。要求某些单体和聚合物的组成。

13. 发明授权

US5532331A Thiodiphenol copolycarbonates and their use as components of multilayered polymeric reflective bodies 失效
标题翻译：硫代二苯酚共聚碳酸酯及其作为多层聚合物反射体的组分的用途
公开(公告)号：US5532331A
公开(公告)日：1996-07-02
申请号：US351436
申请日：1994-12-14
申请人： Stephen E. Bales , Charles A. Langhoff , John A. Wheatley
发明人： Stephen E. Bales , Charles A. Langhoff , John A. Wheatley
IPC分类号： C08G64/08 , C08G64/00
CPC分类号： C08G64/081 , Y10T428/31507
摘要： This invention provides novel copolycarbonates that exhibit improvements in glass transition temperature, refractive index, and limiting oxygen index compared to prior art thiodiphenol/bisphenol A copolycarbonates. The copolycarbonates of this invention comprise the reaction products of 4,4'-thiodiphenol and compounds such as 9,9-bis (4-hydroxyphenyl) fluorene with phosgene. They are useful as components of multilayered polymeric reflective bodies.
摘要翻译： PCT No.PCT / US93 / 06074 Sec。 371日期1994年12月15日 102（e）1994年12月15日日期PCT提交1993年6月24日PCT公布。出版物WO94 / 02533 日本1994年2月3日。本发明提供与现有技术的硫代二酚/双酚A共聚碳酸酯相比，显示玻璃化转变温度，折射率和极限氧指数的改进的新型共聚碳酸酯。本发明的共聚碳酸酯包括4,4'-硫代二酚和诸如9,9-双（4-羟基苯基）芴和光气的化合物的反应产物。它们可用作多层聚合物反射体的组分。

14. 发明授权

US5037935A Thermoplastic compositions with nonlinear optical activity 失效
标题翻译：具有非线性光学活性的热塑性组合物
公开(公告)号：US5037935A
公开(公告)日：1991-08-06
申请号：US535210
申请日：1990-06-08
申请人： Robert J. Gulotty , Stephen E. Bales
发明人： Robert J. Gulotty , Stephen E. Bales
IPC分类号： C08G63/64 , C08G64/08 , C08G64/12
CPC分类号： C08G64/08 , C08G63/64 , C08G64/12
摘要： This invention provides thermoplastic polymeric materials comprising polycarbonate and polyestercarbonate resins and oriented polymeric compositions thereof which exhibit nonlinear optical properties.
摘要翻译：本发明提供包含聚碳酸酯和聚酯碳酸酯树脂的热塑性聚合物材料及其取向的聚合物组合物，其显示非线性光学性质。

15. 发明授权

US4994533A Poly(aryl ether)-poly(aryl carbonate) block copolymers and their preparation 失效
标题翻译：聚（芳基醚） - 聚（芳基碳酸酯）嵌段共聚物及其制备方法
公开(公告)号：US4994533A
公开(公告)日：1991-02-19
申请号：US329802
申请日：1989-03-28
申请人： Michael J. Mullins , Steven P. Crain , Edmund P. Woo , Daniel J. Murray , Stephen E. Bales
发明人： Michael J. Mullins , Steven P. Crain , Edmund P. Woo , Daniel J. Murray , Stephen E. Bales
IPC分类号： C08G64/18 , C08G64/42
CPC分类号： C08G64/183 , C08G64/42
摘要： A method for preparing novel poly(aryl ether)-(poly aryl carbonate) block copolymers by the decarboxylation of copolycarbonates prepared by the condensation of two different aromatic dihydroxy compounds and a carbonate precursor such as phosgene. At least one of the aromatic diols must have at least one electron-withdrawing group located in a position ortho or para to at least one of its hydroxy groups and at least one of the diols must not have any electron-withdrawing groups in a position ortho or para to either of its hydroxy groups. The method is particularly effective in making crystalline block copolymers.
摘要翻译：通过使两种不同的芳族二羟基化合物和碳酸酯前体如光气缩合制备的共聚碳酸酯的脱羧来制备新的聚（芳基醚） - （聚芳基碳酸酯）嵌段共聚物的方法。至少一种芳族二醇必须具有位于至少一个羟基的邻位或对位的至少一个吸电子基团，并且至少一个二醇在邻位不能具有任何吸电子基团或对位于其任一羟基。该方法在制备结晶嵌段共聚物中特别有效。

16. 发明授权

US4818254A Semi-permeable membranes consisting predominantly of polycarbonates derived from tetrahalobisphenols 失效
标题翻译：半透膜主要由衍生自四卤双酚的聚碳酸酯组成
公开(公告)号：US4818254A
公开(公告)日：1989-04-04
申请号：US141878
申请日：1988-01-06
申请人： Joginder N. Anand , Darrell C. Feay , Stephen E. Bales , Thomas O. Jeanes
发明人： Joginder N. Anand , Darrell C. Feay , Stephen E. Bales , Thomas O. Jeanes
IPC分类号： B01D71/50 , C01B13/02 , C01B21/04 , C01B32/50 , C07C7/144 , C08G64/10 , B01D53/22
CPC分类号： C08G64/10 , B01D71/50 , C01B13/0255 , C01B21/0444 , C01B31/20 , C07C7/144 , C01B2210/0045 , C01B2210/0046
摘要： The invention is an improved gas separation membrane comprising a thin, discriminating layer consisting predominantly of a carbonate polymer derived from a bisphenol corresponding to Formula I ##STR1## wherein R at each occurrence is independently H, Cl, Br, or C.sub.1 -C.sub.4 alkyl and R.sup.1 is ##STR2## --S--, --SO.sub.2 --, --O--, or a C.sub.1 -C.sub.6 divalent hydrocarbon or a C.sub.1 -C.sub.6 divalent fluorocarbon radical or inertly substituted hydrocarbon radical, with the proviso that at least 25 weight percent of the moieties derived from the bisphenol of Formula I present in the discriminating layer bear R groups which are exclusively Br or Cl, the gas separation membrane exhibiting a separation factor for oxygen and nitrogen at 24.degree. C. of at least 6.1. In another aspect this invention relates to a process for separating oxygen from nitrogen, or a nitrogen-containing gas.
摘要翻译：本发明是一种改进的气体分离膜，其包括主要由衍生自对应于式I的双酚的碳酸酯聚合物组成的薄的鉴别层，其中R在每次出现时独立地为H，Cl，Br或C 1 -C 4烷基， R 1是-S-，-SO 2 - ， - O-或C 1 -C 6二价烃或C 1 -C 6二价氟代烃基或惰性取代的烃基，条件是至少25重量％的部分衍生自鉴别层中存在的式I的双酚的R基团仅具有Br或Cl，气相分离膜在24℃下表现出氧和氮的分离因子至少为6.1。另一方面，本发明涉及从氮气或含氮气体中分离氧气的方法。

17. 发明授权

US5614599A Stilbene-based polyester and polycarbonate compositions 失效
标题翻译：二苯乙烯基聚酯和聚碳酸酯组合物
公开(公告)号：US5614599A
公开(公告)日：1997-03-25
申请号：US542489
申请日：1995-10-13
申请人： Stephen E. Bales , Robert E. Hefner, Jr. , Rina Singh
发明人： Stephen E. Bales , Robert E. Hefner, Jr. , Rina Singh
IPC分类号： C08L67/03 , C08G63/547 , C08G63/64 , C08G64/04 , C08L67/06 , C08L69/00 , C08L101/00 , C08F283/00
CPC分类号： C08G63/547 , C08G63/64 , C08G64/045
摘要： Described is a polycarbonate, polyester, or polyestercarbonate composition prepared from a reaction mixture comprising at least one diol and at least one carbonate precursor or ester precursor, wherein at least about 95 mole percent of the diol present in the reaction mixture consists of one or more aromatic diols, at least about 10 mole percent of which consists of one or more stilbene diols. The composition of the invention advantageously has a relatively high thermal resistance, melting temperature, tensile and flexural properties, and/or resistance to thermal embrittlement. Moreover, the polymers of the invention which are thermotropic liquid crystalline also advantageously possess a broad temperature range for liquid crystallinity, good melt processibility, a low coefficient of thermal expansion, a high ignition resistance, high solvent resistance, and/or good barrier properties.
摘要翻译：描述了由包含至少一种二醇和至少一种碳酸酯前体或酯前体的反应混合物制备的聚碳酸酯，聚酯或聚酯碳酸酯组合物，其中存在于反应混合物中的至少约95摩尔％的二醇由一种或多种芳族二醇，其至少约10摩尔％由一种或多种二苯乙烯二醇组成。本发明的组合物有利地具有相对高的耐热性，熔融温度，拉伸和弯曲性能和/或耐热脆性。此外，作为热致液晶的本发明的聚合物还有利地具有液晶的宽温度范围，良好的熔融加工性，低热膨胀系数，高耐点火性，高耐溶剂性和/或良好的阻隔性能。

18. 发明授权

US5486577A Blends of diaryl fluorene carbonate polymers with bisphenol A carbonate polymers 失效
标题翻译：二芳基芴碳酸酯聚合物与双酚A碳酸酯聚合物的共混物
公开(公告)号：US5486577A
公开(公告)日：1996-01-23
申请号：US407930
申请日：1995-03-21
申请人： Hani Farah , Stephen E. Bales
发明人： Hani Farah , Stephen E. Bales
IPC分类号： C08L69/00
CPC分类号： C08L69/00
摘要： Carbonate polymer compositions are prepared comprising a first diaryl fluorene carbonate polymer component and a second bisphenol A carbonate polymer component, the blend composition preferably comprising from about 1 to about 99 weight percent diaryl fluorene carbonate polymer component based on weight of first and second components. Preferably the first diaryl fluorene carbonate polymer component is a copolymer comprising (a) from about 1 up to and including about 99 mole percent dihydroxyaryl fluorene moiety based on the weight of dihydroxyaryl fluorene compound and additional multihydric monomer compound and (b) moieties of at least one additional condensation copolymerizable multihydric monomer compound remnant. In another embodiment, the invention is an improved process for preparing heat resistant diaryl fluorene carbonate polymer composition comprising the step of combining a first diaryl fluorene carbonate polymer component and a second bisphenol A carbonate polymer component, different from the diaryl fluorene carbonate polymer component. These blends can be prepared by known means such as by solution blending or melt blending. It has surprisingly been found that these blend compositions are miscible and transparent across a range of weight ratios and diaryl fluorene contents.
摘要翻译：制备碳酸酯聚合物组合物，其包含第一二芳基芴碳酸酯聚合物组分和第二双酚A碳酸酯聚合物组分，所述共混组合物优选包含基于第一组分和第二组分重量的约1至约99重量％的二芳基芴碳酸酯聚合物组分。优选地，第一二芳基芴碳酸酯聚合物组分是包含（a）基于二羟基芳基芴化合物和另外的多羟基单体化合物的重量的约1至约99摩尔％的二羟基芳基芴部分的共聚物，和（b）至少一种另外的可共聚的多羟基单体化合物残余物。在另一个实施方案中，本发明是制备耐热二芳基芴碳酸酯聚合物组合物的改进方法，其包括将不同于二芳基芴碳酸酯聚合物组分的第一二芳基芴碳酸酯聚合物组分和第二双酚A碳酸酯聚合物组分组合的步骤。这些共混物可以通过已知的方法制备，例如通过溶液共混或熔融共混。惊奇地发现，这些共混组合物在重量比和二芳基芴含量范围内是可混溶和透明的。

19. 发明授权

US5419957A Low heat release polymeric composites 失效
标题翻译：低放热聚合物复合材料
公开(公告)号：US5419957A
公开(公告)日：1995-05-30
申请号：US245152
申请日：1994-05-17
申请人： Patrick H. Martin , Peter K. Kim , Stephen E. Bales , Ritchie A. Wessling
发明人： Patrick H. Martin , Peter K. Kim , Stephen E. Bales , Ritchie A. Wessling
IPC分类号： B32B27/08 , C08K7/02 , B32B5/24
CPC分类号： B32B27/08 , C08K7/02 , Y10T428/249962 , Y10T428/249964 , Y10T428/249989
摘要： This invention relates to a low heat release, low density, fiber-reinforced composite comprising a matrix comprising a thermoplastic polymer selected from the group consisting of polyarylsulfone, polyethersulfone, polyetheretherketone, polyetherketoneketone, a copolycarbonate of 4,4'-thiodiphenol and at least one member of the group consisting of bisphenol A, 9,9-bis(4-hydroxyphenyl)fluorene, and 1,1-bis(4-hydroxyphenyl)-1-phenyl ethane, a copolycarbonate of bisphenol A and 9,9-bis(4-hydroxyphenyl)fluorene, 1,1-bis(4-hydroxyphenyl)-1-phenyl ethane polycarbonate, bisphenol A polycarbonate, and polyetherimide, and from about 10 to about 70 percent by weight of the composite of randomly oriented reinforcing fibers, less than 0.5 inch in length, distributed throughout the matrix. The matrix has a void volume of from about 20 to about 90 percent by volume. The composite has a thermoplastic skin layer on each of the major surfaces thereof. A process for making the composite is also disclosed.
摘要翻译：本发明涉及一种低放热，低密度纤维增强复合材料，其包含基质，其包含选自聚芳基砜，聚醚砜，聚醚醚酮，聚醚酮酮，4,4'-硫代二酚的共聚碳酸酯和至少一种由双酚A，9,9-双（4-羟基苯基）芴和1,1-双（4-羟基苯基）-1-苯基乙烷组成的组，双酚A的共聚碳酸酯和9,9-双（ 4-羟基苯基）芴，1,1-双（4-羟基苯基）-1-苯基乙烷聚碳酸酯，双酚A聚碳酸酯和聚醚酰亚胺，和约10至约70重量％的无规取向增强纤维的复合材料长度大于0.5英寸，分布在整个矩阵中。基质具有约20至约90体积％的空隙体积。复合材料在其每个主表面上具有热塑性表层。还公开了制备复合材料的方法。

20. 发明授权

US5106936A Thermoplastic compositions with nonlinear optical activity 失效
标题翻译：具有非线性光学活性的热塑性组合物
公开(公告)号：US5106936A
公开(公告)日：1992-04-21
申请号：US695632
申请日：1991-05-03
申请人： Robert J. Gulotty , Stephen E. Bales
发明人： Robert J. Gulotty , Stephen E. Bales
IPC分类号： C08G63/64 , C08G64/08 , C08G64/12
CPC分类号： C08G64/12 , C08G63/64 , C08G64/08
摘要： This invention provides thermoplastic polymeric materials comprising polycarbonate and polyestercarbonte resins and oriented polymeric compositions thereof which exhibit nonlinear optical properties.
摘要翻译：本发明提供包含聚碳酸酯和聚碳酸酯树脂的热塑性聚合物材料及其取向的聚合物组合物，其表现出非线性的光学

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