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11. 发明授权

US09550961B2 Lipase powder compositions 有权
标题翻译：脂肪酶粉末组合物
公开(公告)号：US09550961B2
公开(公告)日：2017-01-24
申请号：US12000032
申请日：2007-12-07
申请人： Satoshi Negishi , Junko Suzuki , Isamu Takahashi , Hans Christian Holm
发明人： Satoshi Negishi , Junko Suzuki , Isamu Takahashi , Hans Christian Holm
IPC分类号： C12N11/12 , C11C3/10 , C12N9/20 , C12N11/14 , C12P7/64
CPC分类号： C11C3/10 , C12N9/20 , C12N11/14 , C12P7/6436 , C12P7/6454 , Y02P20/52
摘要： The present invention provides a lipase powder composition which comprises a filter aid(s) and a product obtained by pulverizing a Thermomyces sp.-derived lipase immobilized to a silica carrier(s) into the average particle diameter of 1 μm or more and less than 300 μm. This lipase powder composition improves the lipase activity and operability and, therefore, can be suitably used in the methods for exchanging esters of fats and oils and for esterification.
摘要翻译：本发明提供一种脂肪酶粉末组合物，其包含助滤剂和通过将固定于二氧化硅载体上的嗜热链球菌来源的脂肪酶粉碎成平均粒径为1μm以上且小于 300μm。这种脂肪酶粉末组合物改善了脂肪酶活性和可操作性，因此可以适用于脂肪和油的酯交换方法和酯化反应。

12. 发明授权

US5696299A Optical resolution for producing optically active alcohol 失效
标题翻译：用于制造光学活性醇的光学分辨率
公开(公告)号：US5696299A
公开(公告)日：1997-12-09
申请号：US529059
申请日：1995-09-15
申请人： Satoshi Negishi , Seiichi Shirasawa , Junko Suzuki , Yukie Masuda
发明人： Satoshi Negishi , Seiichi Shirasawa , Junko Suzuki , Yukie Masuda
IPC分类号： C12P7/62 , C12P41/00 , C07C33/18 , C07C33/46
CPC分类号： C12P7/62 , C12P41/004
摘要： A process for producing an optically active alcohol comprising carrying out interesterification between a racemic alcohol and an ester selected from the group consisting of (a) a diester between a lower monohydric alcohol and a saturated dicarboxylic acid having 14 or more carbon atoms, (b) a triglyceride of a saturated fatty acid having 16 or more carbon atoms, and (c) a monoester between a lower monohydric alcohol and a saturated fatty acid having 18 or more carbon atoms in the presence of lipase, preferably heat-resistant lipase, and in the presence or absence of a solvent, preferably in the absence of a solvent, under a substantially water-free condition, separating an optically active alcohol rich in either one of R- and S-forms from the reaction mixture, and adding an optically inactive non-racemic alcohol to the residue of the previous step to carry out interesterification under the same conditions as in the previous reaction to separate the other enantiomer. According to the present invention a racemic alcohol can easily be resolved into each enantiomer with high purity in good yield.
摘要翻译：一种光学活性醇的制造方法，其包括在外消旋醇与选自（a）低级一元醇和具有14个或更多个碳原子的饱和二羧酸之间的二酯的酯中进行酯交换，（b）具有16个或更多个碳原子的饱和脂肪酸的甘油三酯，和（c）在脂肪酶，优选耐热脂肪酶存在下，具有18个或更多个碳原子的低级一元醇和饱和脂肪酸之间的单酯，以及在基本无水条件下，优选在不存在溶剂的情况下存在或不存在溶剂，从反应混合物中分离富含R-和S-形式的任何一种的光学活性醇，并加入光学惰性将非外消旋醇与前述步骤的残余物进行酯交换，在与之前反应相同的条件下进行酯交换以分离另一种对映异构体。根据本发明，外消旋醇可以容易地以良好的产率分离成高纯度的每种对映异构体。

13. 发明授权

US5480787A Transesterification method using lipase powder with a particle diameter of 20-50 microns 失效
标题翻译：使用粒径为20-50微米的脂肪酶粉末的酯交换方法
公开(公告)号：US5480787A
公开(公告)日：1996-01-02
申请号：US296921
申请日：1994-08-31
申请人： Satoshi Negishi , Seiichi Shirasawa , Junko Suzuki , Tateo Murui
发明人： Satoshi Negishi , Seiichi Shirasawa , Junko Suzuki , Tateo Murui
IPC分类号： C12N9/20 , C12N11/14 , C12P7/62 , C12P7/64 , C12R1/05
CPC分类号： C12P7/6454 , C12N11/14
摘要： The transesterification method is conducted with a powdery lipase wherein the powdery lipase is dispersed in ester-containing starting materials in the presence or absence of an inert organic solvent, and the diameter of at least 90% of the dispersed lipase particles is kept in the range of 1 to 100 .mu.m in the course of the trans-esterification reaction. A reactivity higher than that realized by the conventional transesterification method with a powdery lipase is obtained and the lipase can be easily recovered and reused, without causing a loss of the lipase activity, lowering of the conversion due to the residence of the substrate on the immobilizing carrier and side reactions caused by water introduced into the reaction system by the immobilizing carrier.
摘要翻译：酯交换方法用粉状脂肪酶进行，其中在存在或不存在惰性有机溶剂的情况下将粉状脂肪酶分散在含酯原料中，并且至少90％的分散的脂肪酶颗粒的直径保持在在反式酯化反应过程中为1〜100微米。获得比通过常规酯交换法用粉末脂肪酶实现的更高的反应性，并且可以容易地回收和再利用脂肪酶，而不会引起脂肪酶活性的丧失，由于底物停留在固定化上的转化率降低由固定载体引入反应体系的水引起的载体和副反应。

14. 发明授权

US08580550B2 Lipase powder, method for manufacture thereof, and use thereof 失效
标题翻译：脂肪酶粉末，其制造方法及其用途
公开(公告)号：US08580550B2
公开(公告)日：2013-11-12
申请号：US11716580
申请日：2007-03-12
申请人： Tomomi Suganuma , Tadashiro Hirose , Junko Suzuki , Shin Arimoto , Hideaki Maki , Satoshi Negishi
发明人： Tomomi Suganuma , Tadashiro Hirose , Junko Suzuki , Shin Arimoto , Hideaki Maki , Satoshi Negishi
IPC分类号： C12N9/20
CPC分类号： C12P7/6454 , C12N9/20 , C12P7/62 , C12P7/6436
摘要： There is provided a lipase powder which is a granulated material comprising a lipase and at least one member selected from the group consisting of fatty acids having 8 to 12 carbon atoms, alcohol esters thereof, and a mixture thereof. This lipase powder has an increased lipase activity.
摘要翻译：提供了脂肪酶粉末，其是包含脂肪酶和至少一种选自碳原子数为8〜12的脂肪酸，其醇酯及其混合物的颗粒状物质。该脂肪酶粉末具有增加的脂肪酶活性。

15. 发明申请

US20090104680A1 Lipase powder, methods for producing the same and use thereof 有权
标题翻译：脂肪酶粉末，其制造方法及其用途
公开(公告)号：US20090104680A1
公开(公告)日：2009-04-23
申请号：US12314473
申请日：2008-12-11
申请人： Junko Suzuki , Satoshi Negishi , Yuri Arai , Chika Sakurai
发明人： Junko Suzuki , Satoshi Negishi , Yuri Arai , Chika Sakurai
IPC分类号： C12N9/20
CPC分类号： C12P7/6454 , C12N9/20 , C12N9/96 , C12N9/98
摘要： A lipase powder which is a granulated substance containing a lipase and a solid content of animal milk, a lipase composition wherein said lipase powder is immersed or impregnated in fatty oil, and a method for producing the lipase powder which comprises the step of adding animal milk or cream derived from the animal milk to an aqueous solution containing a lipase, and the step of spray-drying, freeze-drying or solvent-precipitating the mixture thereof are provided. According to the present invention, a lipase powder of which lipase activity and stability are improved can be provided.
摘要翻译：一种脂肪酶粉末，其是含有脂肪酶和动物乳固体含量的粒状物质，其中所述脂肪酶粉末浸渍或浸渍在脂肪油中的脂肪酶组合物，以及包含添加动物乳的步骤的方法或来自动物乳的乳膏至含有脂肪酶的水溶液，并且提供其喷雾干燥，冷冻干燥或溶剂沉淀其混合物的步骤。根据本发明，可以提供脂肪酶活性和稳定性提高的脂肪酶粉末。

16. 发明申请

US20080102500A1 Lipase powder compositions 有权
标题翻译：脂肪酶粉末组合物
公开(公告)号：US20080102500A1
公开(公告)日：2008-05-01
申请号：US12000032
申请日：2007-12-07
申请人： Satoshi Negishi , Junko Suzuki , Isamu Takahashi , Hans Holm
发明人： Satoshi Negishi , Junko Suzuki , Isamu Takahashi , Hans Holm
IPC分类号： C12P7/64 , C12N9/14
CPC分类号： C11C3/10 , C12N9/20 , C12N11/14 , C12P7/6436 , C12P7/6454 , Y02P20/52
摘要： The present invention provides a lipase powder composition which comprises a filter aid(s) and a product obtained by pulverizing a Thermomyces sp.-derived lipase immobilized to a silica carrier(s) into the average particle diameter of 1 μm or more and less than 300 μm. This lipase powder composition improves the lipase activity and operability and, therefore, can be suitably used in the methods for exchanging esters of fats and oils and for esterification.
摘要翻译：本发明提供了一种脂肪酶粉末组合物，其包含助滤剂和通过将固定于二氧化硅载体上的嗜热链球菌来源的脂肪酶粉碎成平均粒径为1μm以上且小于 300个妈妈这种脂肪酶粉末组合物改善了脂肪酶活性和可操作性，因此可以适用于脂肪和油的酯交换方法和酯化反应。

17. 发明申请

US20060105935A1 Lipase powder, methods for producing the same and use thereof 审中-公开
公开(公告)号：US20060105935A1
公开(公告)日：2006-05-18
申请号：US11320756
申请日：2005-12-30
申请人： Junko Suzuki , Satoshi Negishi , Yuri Arai , Chika Sakurai
发明人： Junko Suzuki , Satoshi Negishi , Yuri Arai , Chika Sakurai
IPC分类号： C11D17/00
CPC分类号： C12P7/6454 , C12N9/20 , C12N9/96 , C12N9/98
摘要： A lipase powder which is a granulated substance containing a lipase and a solid content of animal milk, a lipase composition wherein said lipase powder is immersed or impregnated in fatty oil, and a method for producing the lipase powder which comprises the step of adding animal milk or cream derived from the animal milk to an aqueous solution containing a lipase, and the step of spray-drying, freeze-drying or solvent-precipitating the mixture thereof are provided. According to the present invention, a lipase powder of which lipase activity and stability are improved can be provided.

18. 发明授权

US5600027A Process for producing optically active alcohol containing phenyl group 失效
标题翻译：含苯基的光学活性醇的方法
公开(公告)号：US5600027A
公开(公告)日：1997-02-04
申请号：US529071
申请日：1995-09-15
申请人： Junko Suzuki , Satoshi Negishi , Seiichi Shirasawa , Yukie Masuda
发明人： Junko Suzuki , Satoshi Negishi , Seiichi Shirasawa , Yukie Masuda
IPC分类号： C12P7/62 , C12P41/00 , C07C29/74
CPC分类号： C12P7/62 , C12P41/004
摘要： A process for producing an optically active alcohol having a phenyl group is disclosed, comprising the step of carrying out interesterification between (a) a monoester between a racemic alcohol having a phenyl group and a fatty acid or a diester between a racemic alcohol having a phenyl group and a dibasic acid and (b) an optically inactive non-racemic alcohol having 16 or more carbon atoms in the presence of heat-resistant lipase and in the absence of a solvent under a substantially water-free condition at a temperature of not lower than 81.degree. C. under atmospheric pressure or reduced pressure and the step of separating an optically active alcohol having a phenyl group rich in either one of R- and S-forms from the reaction mixture. Use of heat-resistant lipase makes it possible to use high-melting point materials without using any solvent therefor and to perform interesterification at a high temperature thereby completing the reaction in a reduced time. Further, use of a high-melting point and high-boiling point starting material makes it possible to separate an optically active alcohol from the reaction mixture with high purity in high yield by means of a simple purification step taking advantage of a difference in physical properties.
摘要翻译：公开了一种制备具有苯基的光学活性醇的方法，包括以下步骤：在（a）具有苯基的外消旋醇与脂肪酸之间的单酯或具有苯基的外消旋醇之间的二酯之间进行酯交换基和二元酸，和（b）在耐热脂肪酶存在下具有16个或更多个碳原子的光学非活性的非外消旋醇，并且在不存在溶剂的条件下，在基本上无水条件下，温度不低于在大气压或减压下的温度为81℃，并且从反应混合物中分离具有富R和S-形式的苯基的光学活性醇的步骤。使用耐热脂肪酶使得可以使用高熔点材料而不使用任何溶剂，并在高温下进行酯交换，从而在缩短的时间内完成反应。此外，使用高熔点和高沸点原料可以通过利用物理性质的差异的简单纯化步骤以高产率从反应混合物中分离光学活性醇。

19. 发明授权

US08535749B2 Oil-and-fat composition, process for production of the composition, chocolate, and process for production of the chocolate 失效
标题翻译：油脂组合物，生产组合物的方法，巧克力和生产巧克力的方法
公开(公告)号：US08535749B2
公开(公告)日：2013-09-17
申请号：US12810705
申请日：2008-12-12
申请人： Akira Akahane , Yoshiyuki Hatano , Hirofumi Haruna , Hidetaka Uehara , Satoshi Negishi , Yuka Kikuchi
发明人： Akira Akahane , Yoshiyuki Hatano , Hirofumi Haruna , Hidetaka Uehara , Satoshi Negishi , Yuka Kikuchi
IPC分类号： A23G1/00 , A23D9/00
CPC分类号： A23D9/00 , A23D9/02 , A23G1/36 , A23G3/343 , A23G3/40 , A23L29/10 , A23V2002/00 , A23V2200/244
摘要： Disclosed is an oil-and-fat composition suitable for the coating with a tempered chocolate, particularly suitable for the enrobing with the chocolate. Also disclosed is a low-fat tempered chocolate suitable for coating, particularly enrobing. Specifically disclosed is an oil-and-fat composition which has a content of an oleoyldipalmitin (P2O) component of 70 to 85% by mass, which contains a symmetric triglyceride 1,3-dipalmitoyl-2-oleoylglycerin (POP) in the oleoyldipalmitin (P2O) component at a ratio of the amount of 1,3-dipalmitoyl-2-oleoylglycerin (POP) to the amount of the oleoyldipalmitin (P2O) component [(POP)/(P2O)] of 0.95 or more by mass, and which has a content of tripalmitin (PPP) of 2 to 6% by mass. The oil-and-fat composition is added to a tempered chocolate.
摘要翻译：公开了一种适用于用柔软巧克力涂覆的油脂组合物，特别适用于巧克力的包衣。还公开了一种适用于涂层的低脂温和巧克力，特别是包被。具体公开了油酰基二头孢霉素（P2O）成分含量为70〜85质量％的含油脂组合物，其含有油酰基黑霉素（对照甘油三酯，甘油三酯，甘油三酯，甘油三酯， P2O）组分，其中1,3-二棕榈酰基-2-油酰甘油（POP）的量与油酰基二头孢霉多糖（P2O）组分[（POP）/（P2O）]的量的比例为0.95以上，具有2〜6质量％的三棕榈酸（PPP）含量。将油脂组合物加入调味巧克力中。

20. 发明申请

US20120021214A1 FUNCTIONAL FILM AND LAMINATE 审中-公开
标题翻译：功能膜和层压板
公开(公告)号：US20120021214A1
公开(公告)日：2012-01-26
申请号：US13260350
申请日：2010-03-09
申请人： Takeshi Hasegawa , Satoshi Negishi , Susumu Kurishima
发明人： Takeshi Hasegawa , Satoshi Negishi , Susumu Kurishima
IPC分类号： B32B27/00 , C09J7/02 , B32B7/12
CPC分类号： C09J7/29 , C09J2201/622 , C09J2205/31 , Y10T428/2813 , Y10T428/31504
摘要： A functional film that does not show decrease of surface hardness even when an adhesive layer for adhering it to another member is provided, and does not generate separation nor delamination at the time of die cutting, and a laminate thereof are provided. The functional film can include a plastic film having a functional layer constituted by a cured film on one surface and an adhesive layer on the other surface. The adhesive layer contains a curable adhesive that can be cured by irradiation of ionizing radiation or heating, and is constituted so that the adhesive layer after cured by irradiation of ionizing radiation or heating shows a Martens hardness of 260 N/mm2 or lower, and the following relational expression is satisfied. Martens hardness of the adhesive layer after curing≧Martens hardness of the functional layer×0.25
摘要翻译：即使提供粘附到另一个部件上的粘合剂层，也没有显示表面硬度的降低的功能膜，并且在切割时不产生分离或分层，并且提供其层压体。功能膜可以包括具有由一个表面上的固化膜和另一个表面上的粘合剂层构成的功能层的塑料膜。粘合剂层含有可通过电离辐射照射或加热而固化的可固化粘合剂，并且构成为通过照射电离辐射或加热固化后的粘合剂层的马氏体硬度为260N / mm 2以下，满足关系表达式。固化后粘合层的马氏硬度≧功能层的马氏硬度×0.25

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