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11. 发明申请

WO2002103825A1 METHOD FOR PRODUCING COMPOSITE MATERIAL FOR ELECTRODE COMPRISING QUINOXALINE BASED POLYMER, SUCH MATERIAL, ELECTRODE AND BATTERY USING THE SAME 审中-公开
标题翻译：用于生产包含基于喹啉基的聚合物的电极的复合材料的方法，使用其的这种材料，电极和电池
公开(公告)号：WO2002103825A1
公开(公告)日：2002-12-27
申请号：PCT/JP2002/005784
申请日：2002-06-11
申请人： SHOWA DENKO K.K. , TAKEUCHI, Masataka , YASUDA, Hiroshi , MIZUGUCHI, Junko
发明人： TAKEUCHI, Masataka , YASUDA, Hiroshi , MIZUGUCHI, Junko
IPC分类号： H01M4/60
CPC分类号： H01M4/137 , C08G61/122 , C08G73/0694 , H01G11/56 , H01M4/60 , H01M4/606 , H01M4/608 , H01M4/625 , H01M10/36 , H01M2300/0011 , H01M2300/0065 , H01M2300/0082 , Y02E60/13
摘要： The present invention relates to a method for producing a polymer/conductive carbon composite electrode comprising dehydration condensation polymerization of a tetramine derivative and a tetracarbonyl compound in the presence of an electrically conductive carbon material. The synthetized polymer comprises quinoxaline structural units such as polyphenyl quinoxaline (PPQ) and serves as an active material having proton conductivity. The composite material for electrode obtained by the method has a large capacity of inserting/releasing a proton and excellent in durability. An electrode comprising the composite material and a secondary battery comprising the electrode is excellent in safety and reliability high-speed current characteristics, has a longer life and a larger gravimetric energy density (Wh/kg).
摘要翻译：本发明涉及一种聚合物/导电性碳复合电极的制造方法，其特征在于，在导电性碳材料的存在下，包括四胺衍生物和四羰基化合物的脱水缩聚。合成的聚合物包括喹喔啉结构单元如聚苯基喹喔啉（PPQ），并且用作具有质子传导性的活性材料。通过该方法获得的电极用复合材料具有大的插入/释放质子的能力，并且耐久性优异。包含复合材料的电极和包含电极的二次电池具有优异的安全性和可靠性的高速电流特性，具有更长的寿命和更大的重量能量密度（Wh / kg）。

12. 发明申请

WO2010100764A1 COMPOSITE GRAPHITE PARTICLES AND LITHIUM SECONDARY BATTERY USING THE SAME 审中-公开
标题翻译：使用该复合石墨颗粒和锂二次电池
公开(公告)号：WO2010100764A1
公开(公告)日：2010-09-10
申请号：PCT/JP2009/054356
申请日：2009-03-02
申请人： SHOWA DENKO K.K. , LS MTRON Ltd. , SOTOWA, Chiaki , SUDOH, Akinori , TAKEUCHI, Masataka , HAN, Kyung-hee , HAN-Jung-min , OH, Jung-hun
发明人： SOTOWA, Chiaki , SUDOH, Akinori , TAKEUCHI, Masataka , HAN, Kyung-hee , HAN-Jung-min , OH, Jung-hun
IPC分类号： C01B31/04
CPC分类号： H01M4/587 , C01B32/20 , H01M4/133 , H01M4/1393 , H01M10/052
摘要： The present invention provides composite graphite particles, which are useful for a negative electrode in a secondary battery having high capacitance, good charge- discharge characteristics and good charge-discharge cycle characteristics; and a paste for negative electrode, a negative electrode and a lithium secondary battery which use the composite graphite particles. The composite graphite particles of the present invention comprises a core material consisting of graphite having a interlayer distance d(002) of 0.337 nm or less in which the intensity ratio I D /I G (R value) between the peak intensity (I D ) in a range of 1300 to 1400 cm -1 and the peak intensity ( I G ) in a range of 1580 to 1620 cm -1 as measured by Raman spectroscopy spectra is from 0.01 to 0.1 and a carbonaceous surface layer in which the intensity ratio I D /I G (R value) between the peak intensity (I D ) in a range of 1300 to 1400 cm -1 and the peak intensity ( I G ) in a range of 1580 to 1620 cm -1 as measured by Raman scattering spectroscopy is 0.2 or higher; wherein the peak intensity ratio I 110 /I 004 between the peak intensity (I 004 ) of face (110) and the peak intensity (I 004 ) of face (004) obtained by XRD measurement on the graphite crystal is 0.2 or higher when the particles are mixed with a binder and pressure-molded to a density of 1.55 to 1.65 g/cm 3 .
摘要翻译：本发明提供了复合石墨粒子，其可用于具有高电容，良好的充放电特性和良好的充放电循环特性的二次电池中的负极; 以及使用该复合石墨粒子的负极，负极和锂二次电池用糊料。本发明的复合石墨粒子包括由石墨构成的芯材，其中层间距离d（002）为0.337nm以下，其中峰强度（ID）在一定范围内的强度比ID / IG（R值）为1300〜1400cm -1，通过拉曼光谱测定的1580〜1620cm -1范围内的峰强度（IG）为0.01〜0.1，强度比ID / IG（R 通过拉曼散射光谱法测定的在1300〜1400cm -1范围内的峰强度（ID）与1580〜1620cm -1范围内的峰强度（IG）之差为0.2以上; 其中，当将所述颗粒与所述石墨晶体的XRD测量得到的在所述石墨晶体上通过XRD测量获得的面（110）的峰强度（I004）和所述面（004）的峰强度（I004）之间的峰强度比I110 / I004为0.2以上时，粘合剂，并以1.55-1.65g / cm3的密度进行压塑。

13. 发明申请

WO2009105863A1 COMPOSITE ELECTRODE MATERIAL 审中-公开
标题翻译：复合电极材料
公开(公告)号：WO2009105863A1
公开(公告)日：2009-09-03
申请号：PCT/CA2009/000188
申请日：2009-02-24
申请人： HYDRO-QUEBEC , SHOWA DENKO K.K. , ZAGHIB, Karim , SOTOWA, Chiaki , CHAREST, Patrick , TAKEUCHI, Masataka , GUERFI, Abdelbast
发明人： ZAGHIB, Karim , SOTOWA, Chiaki , CHAREST, Patrick , TAKEUCHI, Masataka , GUERFI, Abdelbast
IPC分类号： H01M4/36 , H01M4/04 , H01M4/48
CPC分类号： H01M4/131 , H01B1/20 , H01M4/02 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/366 , H01M4/485 , H01M4/5825 , H01M4/623 , H01M4/625 , H01M10/052 , H01M2004/021 , H01M2004/028
摘要： The invention relates to a composite electrode material consisting of a carbon coated complex oxide, fibrous carbon and a binder. Said material is prepared by a method which comprises co-grinding an active electrode material and fibrous carbon, and adding a binder to the co-grinded mixture to lower the viscosity of the mixture. The fibrous carbon is preferably vapor grown carbon fibers.
摘要翻译：本发明涉及由碳涂复合氧化物，纤维状碳和粘结剂组成的复合电极材料。所述材料通过包括共同研磨活性电极材料和纤维状碳的方法以及向共磨碎的混合物中加入粘合剂以降低混合物的粘度的方法制备。纤维状碳优选为气相生长碳纤维。

14. 发明申请

WO2007004728A1 METHOD FOR PRODUCING ANODE FOR LITHIUM SECONDARY BATTERY AND ANODE COMPOSITION, AND LITHIUM SECONDARY BATTERY 审中-公开
标题翻译：生产锂二次电池和阳极组合物的阳极的方法和锂二次电池
公开(公告)号：WO2007004728A1
公开(公告)日：2007-01-11
申请号：PCT/JP2006/313630
申请日：2006-07-03
申请人： SHOWA DENKO K.K. , TAKEUCHI, Masataka , SOTOWA, Chiaki
发明人： TAKEUCHI, Masataka , SOTOWA, Chiaki
IPC分类号： H01M4/02 , H01M4/58 , H01M4/62 , H01M4/66 , H01M10/40 , C01B31/02
CPC分类号： H01M4/133 , H01M4/0433 , H01M4/139 , H01M4/364 , H01M4/587 , H01M4/62 , H01M4/621 , H01M4/661 , H01M10/0569 , H01M2004/021 , H01M2004/027 , Y02E60/122 , Y02P70/54 , Y10T428/2971
摘要： The invention relates to an anode for lithium secondary battery comprising vapor grown carbon fiber uniformly dispersed without forming an agglomerate of 10 µm or larger in an anode active material using natural graphite or artificial graphite, which anode is excellent in long cycle life and large current characteristics. Composition used for production for the anode can be produced, for example, by mixing a thickening agent solution containing an anode active material, a thickening agent aqueous solution and styrene butadiene rubber as binder with a composition containing carbon fiber dispersed in a thickening agent with a predetermined viscosity or by mixing an anode active material with vapor grown carbon fiber in dry state and then adding polyvinylidene difluoride thereto.
摘要翻译：本发明涉及一种锂二次电池用阳极，其包括使用天然石墨或人造石墨在阳极活性物质中形成均匀分散的气相生长碳纤维，而阳极活性物质的长周期性优异，电流特性大。用于阳极生产的组合物可以例如通过将含有负极活性物质，增稠剂水溶液和丁苯橡胶作为粘合剂的增稠剂溶液与分散在增稠剂中的含有碳纤维的组合物混合，通过将阳极活性材料与干燥状态下的气相生长碳纤维混合，然后向其中加入聚偏二氟乙烯。

15. 发明申请

WO2005067081A1 NEGATIVE ELECTRODE MATERIAL FOR LITHIUM BATTERY, AND LITHIUM BATTERY 审中-公开
标题翻译：用于锂电池的负极电极材料和锂电池
公开(公告)号：WO2005067081A1
公开(公告)日：2005-07-21
申请号：PCT/JP2004/019835
申请日：2004-12-28
申请人： SHOWA DENKO K.K. , ZEON CORPORATION , SOTOWA, Chiaki , TAKEUCHI, Masataka , MORI, Hidekazu , YAMAKAWA, Msahiro
发明人： SOTOWA, Chiaki , TAKEUCHI, Masataka , MORI, Hidekazu , YAMAKAWA, Msahiro
IPC分类号： H01M4/02
CPC分类号： H01M4/0433 , H01M4/133 , H01M4/587 , H01M4/621 , H01M4/622 , H01M4/661 , H01M2004/021 , Y10T29/49108 , Y10T29/49115
摘要： The present invention relates to a negative electrode material for a lithium battery characterized by comprising a carbonaceous negative electrode active substance having a specific surface area of 1 m 2 /g or more, a binder formed of styrene-butadiene rubber and a carbon fiber having a fiber diameter of 1 to 1,000 nm; and to a lithium battery using the negative electrode material, which has excellent characteristics, i.e., low electrode resistance, high electrode strength, excellent electrolytic solution permeability, high energy density, and good high-speed charging/discharging performance. The negative electrode material contains carbon fiber in the amount of 0.05 to 20 mass% and the binder formed of styrene-butadiene rubber in 0.1 to 6.0 mass%, and may further contain a thickner such as carboxymethyl cellulose in the amount of 0.3 to 3 mass%.
摘要翻译：本发明涉及一种锂电池用负极材料，其特征在于，包括比表面积为1m 2 / g以上的碳质负极活性物质，由苯乙烯 - 丁二烯橡胶和碳纤维形成的粘合剂纤维直径为1〜1000nm; 并且使用具有优异的特性，即低电极电阻，高电极强度，优异的电解液渗透性，高能量密度和良好的高速充电/放电性能的负极材料的锂电池。负极材料含有0.05〜20质量％的碳纤维和0.1〜6.0质量％的苯乙烯 - 丁二烯橡胶形成的粘合剂，还可以含有0.3〜3质量％的羧甲基纤维素等增稠剂％。

16. 发明申请

WO1996026234A1 SOLID POLYMER ELECTROLYTE, BATTERY AND SOLID-STATE ELECTRIC DOUBLE LAYER CAPACITOR USING THE SAME AS WELL AS PROCESSES FOR THE MANUFACTURE THEREOF 审中-公开
标题翻译：固体聚合物电解质，电池和固态电动双层电容器使用相同的方法作为其制造方法
公开(公告)号：WO1996026234A1
公开(公告)日：1996-08-29
申请号：PCT/JP1996000384
申请日：1996-02-21
申请人： SHOWA DENKO K.K.
发明人： SHOWA DENKO K.K. , TAKEUCHI, Masataka , OOGA, Kazuhiko
IPC分类号： C08G65/32
CPC分类号： H01G9/038 , C08F290/062 , C08F290/142 , C08G18/283 , C08G18/2835 , C08G18/4833 , C08G18/4837 , C08G18/4883 , C08G18/8116 , C08G65/329 , C08G65/3322 , C08G65/33348 , H01B1/122 , H01G9/025 , H01G11/56 , H01M4/13 , H01M4/137 , H01M4/621 , H01M4/622 , H01M6/181 , H01M6/40 , H01M10/052 , H01M10/0565 , Y02E60/13 , Y02T10/7011 , Y02T10/7022
摘要： A solid polymer electrolyte comprising a composite of: (a) a polymer obtainable from at least one compound which contains a structure derived from a polyhydric alcohol having three or more hydroxyl groups, at least two hydrogen atoms of said alcoholic hydroxyl groups being each replaced by a unit represented by a general formula (1): CH2=C(R )C(=O)[O(CH2)x(CH(CH3))y]zNHC(=O)OR - wherein R represents a hydrogen or a methyl group; R represents a divalent organic group containing at least one oxyalkylene group; x and y each represents a number of 0 to 5; z represents a number of 0 to 10; and (b) at least one electrolyte salt. The solid polymer electrolyte has good film strength and processability as well as high ionic conductivity, and is useful for fabricating thin electrodes, batteries and electric double layer capacitors which are free from the leakage of any solution.
摘要翻译：一种固体聚合物电解质，其包含以下复合物：（a）可从至少一种含有衍生自具有三个或更多个羟基的多元醇的结构的化合物获得的聚合物，所述醇羟基的至少两个氢原子各自被由通式（1）表示的单元：CH 2 = C（R 1）C（= O）[O（CH 2）x（CH（CH 3））y] z NHC（= O）OR 2 - R 1表示氢或甲基; R 2表示含有至少一个氧化烯基的二价有机基团; x和y各自表示0〜5的数; z表示0〜10的数; 和（b）至少一种电解质盐。固体聚合物电解质具有良好的膜强度和加工性以及高离子导电性，并且可用于制造没有任何溶液泄漏的薄电极，电池和双电层电容器。

17. 发明授权

EP1961700B1 METHOD FOR PRODUCING GRAPHITE MATERIAL 有权转让
公开(公告)号：EP1961700B1
公开(公告)日：2019-06-26
申请号：EP06834048.8
申请日：2006-12-05
申请人： SHOWA DENKO K.K.
发明人： SUDOH, Akinori , TAKEUCHI, Masataka
IPC分类号： C01B32/205 , H01M4/587 , H01M10/0525

18. 发明公开

EP2908366A1 COMPOSITE CARBON PARTICLE AND LITHIUM-ION SECONDARY CELL USING SAME 审中-公开
标题翻译：碳复合粒子和锂离子二次电池，其
公开(公告)号：EP2908366A1
公开(公告)日：2015-08-19
申请号：EP13844916.0
申请日：2013-10-11
申请人： Showa Denko K.K.
发明人： TAKEUCHI, Masataka , YOKOYAMA, Yoshihito , SOTOWA, Chiaki
IPC分类号： H01M4/587 , H01M4/36 , H01M10/052 , H01M10/0565 , H01M10/0569
CPC分类号： H01M4/366 , H01M4/0402 , H01M4/0471 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M10/0525 , H01M10/0565 , H01M10/0569 , H01M2004/027 , H01M2300/0028 , H01M2300/0082 , Y02P70/54 , Y02T10/7011
摘要： A composite carbon particle for use in a negative electrode of a lithium-ion secondary battery, the composite carbon particle comprising a core particle composed of a carbon material obtained by heating, at not higher than 2500 °C, petroleum coke having a Hardgrove grindability index (HGI value) of 30 to 60 (defined by ASTM D409), and a covering layer composed of a carbonaceous material obtained by heating an organic compound at 1000 °C to 2000 °C, wherein the composite carbon particle has a 50 % particle diameter (D50) of 1 µm to 30 µm in a volume-based cumulative particle size distribution as measured by laser diffraction method.

19. 发明授权

EP2282366B1 CARBON NEGATIVE ELECTRODE MATERIAL FOR LITHIUM SECONDARY BATTERY, PRODUCTION METHOD THEREOF AND LITHIUM SECONDARY BATTERY USING THE SAME 有权
标题翻译：碳负极材料用于锂二次电池，工艺用于生产和锂二次电池
公开(公告)号：EP2282366B1
公开(公告)日：2013-12-11
申请号：EP09734880.9
申请日：2009-04-16
申请人： Posco Chemtech , Showa Denko K.K.
发明人： HAN, Kyung-Hee , OH, Jeong-Hun , KIM, Jong-Sung , YOUM, Chul , HAN, Jung-Min , TAKEUCHI, Masataka , SUDOH, Akinori , SOTOWA, Chiaki
IPC分类号： H01M4/36 , H01M4/587 , H01M4/133
CPC分类号： H01M4/587 , H01M4/133 , H01M4/362 , H01M10/052 , Y02E60/122 , Y02P70/54

20. 发明公开

EP2403802A1 COMPOSITE GRAPHITE PARTICLES AND LITHIUM SECONDARY BATTERY USING THE SAME 审中-公开
标题翻译： GRAPHITVERBUNDTEILCHEN UND LITHIUM-SEKUNDÄRBATTERIEDAMIT
公开(公告)号：EP2403802A1
公开(公告)日：2012-01-11
申请号：EP09841126.7
申请日：2009-03-02
申请人： Showa Denko K.K. , LS Mtron, Ltd.
发明人： SOTOWA, Chiaki , SUDOH, Akinori , TAKEUCHI, Masataka , HAN, Kyung-hee , HAN-Jung-min , OH, Jung-hun
IPC分类号： C01B31/04
CPC分类号： H01M4/587 , C01B32/20 , H01M4/133 , H01M4/1393 , H01M10/052
摘要： The present invention provides composite graphite particles, which are useful for a negative electrode in a secondary battery having high capacitance, good charge- discharge characteristics and good charge-discharge cycle characteristics; and a paste for negative electrode, a negative electrode and a lithium secondary battery which use the composite graphite particles. The composite graphite particles of the present invention comprises a core material consisting of graphite having a interlayer distance d(002) of 0.337 nm or less in which the intensity ratio I
D /I
G (R value) between the peak intensity (I
D ) in a range of 1300 to 1400 cm
-1 and the peak intensity ( I
G ) in a range of 1580 to 1620 cm
-1 as measured by Raman spectroscopy spectra is from 0.01 to 0.1 and a carbonaceous surface layer in which the intensity ratio I
D /I
G (R value) between the peak intensity (I
D ) in a range of 1300 to 1400 cm
-1 and the peak intensity ( I
G ) in a range of 1580 to 1620 cm
-1 as measured by Raman scattering spectroscopy is 0.2 or higher; wherein the peak intensity ratio I
110 /I
004 between the peak intensity (I
004 ) of face (110) and the peak intensity (I
004 ) of face (004) obtained by XRD measurement on the graphite crystal is 0.2 or higher when the particles are mixed with a binder and pressure-molded to a density of 1.55 to 1.65 g/cm
3 .
摘要翻译：本发明提供了复合石墨粒子，其对具有高电容，良好的充放电特性和良好的充放电循环特性的二次电池中的负极是有用的; 以及使用该复合石墨粒子的负极，负极和锂二次电池用糊料。本发明的复合石墨粒子包括由层间距离d（002）为0.337nm以下的石墨构成的芯材，其中峰强度（ID）在一定范围内的强度比ID / IG（R值）为1300〜1400cm -1，通过拉曼光谱测定的1580〜1620cm -1范围内的峰强度（IG）为0.01〜0.1，强度比ID / IG（R 通过拉曼散射光谱法测定的在1300〜1400cm -1范围内的峰强度（ID）与1580〜1620cm -1范围内的峰强度（IG）之差为0.2以上; 其中，当将颗粒与石墨晶体的XRD测量获得的面（110）的峰强度（I110）和面（004）的峰强度（I004）之间的峰强度比I110 / I004与粘合剂，并以1.55-1.65g / cm3的密度加压成型。

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