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    • 12. 发明授权
    • Ceramic material and method of manufacture
    • 陶瓷材料及其制造方法
    • US4711644A
    • 1987-12-08
    • US926849
    • 1986-11-03
    • Russel L. YeckleyBernard North
    • Russel L. YeckleyBernard North
    • C04B35/597C04B35/58
    • C04B35/597
    • A dual phase silicon aluminum oxynitride material comprising a first phase Si-Al-O-N, commonly referred to as .beta.--Si--Al--O--N, and a second phase Si-Al-O-N referred to as .alpha.--Si--Al--O--N. In addition to the double phase Si-Al-O-Ns, there is included a glassy type material which can formulate up to ten percent by weight of the total composition. The material may be manufactured by forming a polytype material made from reacted alumina, aluminum nitride and silicon nitride. The polytype material may be mixed with further powders of silicon nitride and an oxide of yttrium, lithium or calcium and finally reacted to a double phase Si-Al-O-N material where hardness is increased by the additional .alpha.-Si-Al-O-N is increased significantly affecting its strength.The material may be formed in situ by mixing aluminum nitride, alumina, silicon nitride, together with an oxide of yttrium, lithium or calcium. These materials can then be sintered to a final product containing a double phase Si-Al-O-N. Control of the alumina content in the polytype or in situ methods affects the percentage of .alpha.-Si-Al-O-N produced in the final product. The hardness of the material increases with the .alpha.-Si-Al-O-N content without significantly affecting its transverse rupture strength.
    • 包括通常称为β-Si-Al-O-N的第一相Si-Al-O-N和称为α-Si-Al-O-N的第二相Si-Al-O-N的双相硅铝氧氮化物材料。 除了双相Si-Al-O-N之外,还包括一种玻璃状材料,其可以配制成总组合物的10重量%。 该材料可以通过形成由反应的氧化铝,氮化铝和氮化硅制成的多型材制造。 多型材料可以与氮化硅和钇,锂或钙的氧化物的另外的粉末混合,并最终与双相Si-Al-ON材料反应,其中硬度通过额外的α-Si-Al-ON增加而增加 显着影响其实力。 材料可以通过将氮化铝,氧化铝,氮化硅与钇,锂或钙的氧化物一起混合而原位形成。 然后将这些材料烧结成含有双相Si-Al-O-N的最终产品。 控制聚合物或原位方法中的氧化铝含量会影响最终产品中产生的α-Si-Al-O-N的百分比。 材料的硬度随着α-Al-O-N含量的增加而不会明显影响其横向断裂强度。
    • 16. 发明授权
    • Ceramic material and method of manufacture
    • 陶瓷材料及其制造方法
    • US4563433A
    • 1986-01-07
    • US466716
    • 1983-02-15
    • Russell L. YeckleyBernard North
    • Russell L. YeckleyBernard North
    • C04B35/597C04B35/58
    • C04B35/597
    • A dual phase silicon aluminum oxynitride material comprising a first phase Si-Al-O-N, commonly referred to as .beta.-Si-Al-O-N, and a second phase Si-Al-O-N referred to as .alpha.-Si-Al-O-N. In addition to the double phase Si-Al-O-Ns, there is included a glassy type material which can formulate up to ten percent by weight of the total composition. The material may be manufactured by forming a polytype material made from reacted alumina, aluminum nitride and silicon nitride. The polytype material may be mixed with further powders of silicon nitride and an oxide of yttrium, lithium or calcium and finally reacted to a double phase Si-Al-O-N material where hardness is increased as the additional .alpha.-Si-Al-O-N is increased without significantly affecting its strength.The material may be formed in situ by mixing aluminum nitride, alumina, silicon nitride, together with an oxide of yttrium, lithium or calcium. These materials can then be sintered to a final product containing a double phase Si-Al-O-N. Control of the alumina content in the polytype or in situ methods affects the percentage of .alpha.-Si-Al-O-N produced in the final product. The hardness of the material increases with the .alpha.-Si-Al-O-N content without significantly affecting its transverse rupture strength.
    • 包括通常称为β-Si-Al-O-N的第一相Si-Al-O-N和称为α-Si-Al-O-N的第二相Si-Al-O-N的双相硅铝氧氮化物材料。 除了双相Si-Al-O-N之外,还包括一种玻璃状材料,其可以配制成总组合物的10重量%。 该材料可以通过形成由反应的氧化铝,氮化铝和氮化硅制成的多型材制造。 多型材料可以与另外的氮化硅粉末和钇,锂或钙的氧化物混合,并最终与另外的α-Al-ON增加硬度的双相Si-Al-ON材料反应 没有显着影响其实力。 材料可以通过将氮化铝,氧化铝,氮化硅与钇,锂或钙的氧化物一起混合而原位形成。 然后将这些材料烧结成含有双相Si-Al-O-N的最终产品。 控制聚合物或原位方法中的氧化铝含量会影响最终产品中产生的α-Si-Al-O-N的百分比。 材料的硬度随着α-Al-O-N含量的增加而不会明显影响其横向断裂强度。