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11. 发明申请

US20060093850A1 COATING SYSTEMS CONTAINING GAMMA-PRIME NICKEL ALUMINIDE COATING 有权
标题翻译：包含GAMMA-PRIME镍铬铝涂料的涂料体系
公开(公告)号：US20060093850A1
公开(公告)日：2006-05-04
申请号：US10904220
申请日：2004-10-29
申请人： Ramgopal Darolia , Joseph Rigney , William Walston
发明人： Ramgopal Darolia , Joseph Rigney , William Walston
IPC分类号： B32B15/01 , B32B15/04
CPC分类号： F01D5/288 , F05C2201/0466 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944
摘要： An overlay coating for articles used in hostile thermal environments. The coating has a predominantly gamma prime-phase nickel aluminide (Ni3Al) composition suitable for use as an environmental coating and as a bond coat for a thermal barrier coating. The coating has a composition of, by weight, at least 6% to about 15% aluminum, about 2% to about 5% chromium, optionally one or more reactive elements in individual or combined amounts of up to 4%, optionally up to 2% silicon, optionally up to 60% of at least one platinum group metal, and the balance essentially nickel. A thermal-insulating ceramic layer may be deposited on the coating.
摘要翻译：用于敌对热环境中的物品的覆盖涂层。该涂层主要具有适合用作环境涂层和用作热障涂层的粘合涂层的γ初始相铝酸镍（Ni 3 Al 3 Al）组合物。该涂层具有按重量计至少6％至约15％的铝，约2％至约5％的铬，任选的一种或多种反应性元素的组合物，其个体或组合量可达4％，任选至多2 ％硅，任选至多60％的至少一种铂族金属，余量基本上为镍。绝热陶瓷层可以沉积在涂层上。

12. 发明申请

US20060057406A1 THERMAL BARRIER COATING WITH MODULATED GRAIN STRUCTURE AND METHOD THEREFOR 有权
标题翻译：具有调制颗粒结构的热障涂层及其方法
公开(公告)号：US20060057406A1
公开(公告)日：2006-03-16
申请号：US10711364
申请日：2004-09-14
申请人： Ramgopal Darolia , Brett Boutwell , Brian Hazel , Bangalore Nagaraj , Joseph Rigney , Roger Wustman
发明人： Ramgopal Darolia , Brett Boutwell , Brian Hazel , Bangalore Nagaraj , Joseph Rigney , Roger Wustman
IPC分类号： B32B15/04 , B32B9/00 , C23C16/00
CPC分类号： C23C14/226 , C23C14/22 , C23C14/505 , C23C28/321 , C23C28/3215 , C23C28/345 , C23C28/3455 , C23C28/42 , F01D5/288 , F05D2230/90 , F05D2300/611 , Y10T428/24355 , Y10T428/24413
摘要： Thermal barrier coating (TBC) and a method of depositing a TBC having a modulated columnar microstructure that exhibits increased impact resistance. The TBC is deposited to have a columnar microstructure in which columns extend from a substrate surface. The columns having inner regions contacting the surface, outer regions near an outermost surface of the TBC, and interior regions therebetween. The inner regions of the columns are substantially normal to the substrate surface and at least one of the interior and outer regions of the columns are nonaligned with its respective inner regions, so that the columns of the columnar microstructure are continuous but modulated between the inner and outer regions to reduce tensile stresses within the columns resulting from particle impact.
摘要翻译：热屏蔽涂层（TBC）和沉积具有显示出增加的耐冲击性的调制柱状微结构的TBC的方法。沉积TBC以具有柱状微结构，其中柱从衬底表面延伸。具有接触表面的内部区域，靠近TBC的最外表面的外部区域以及它们之间的内部区域的列。柱的内部区域基本上垂直于基底表面，并且柱的内部和外部区域中的至少一个与其相应的内部区域不对齐，使得柱状微结构的列是连续的但是在内部和/ 外部区域以减少由于颗粒撞击引起的柱内的拉伸应力。

13. 发明申请

US20050106315A1 Method for repairing components using environmental bond coatings and resultant repaired components 有权
标题翻译：使用环境粘合剂涂层修补部件的方法以及由此修复的部件
公开(公告)号：US20050106315A1
公开(公告)日：2005-05-19
申请号：US10713938
申请日：2003-11-13
申请人： Joseph Rigney , Ramgopal Darolia
发明人： Joseph Rigney , Ramgopal Darolia
IPC分类号： B23P6/00 , C23C4/02 , C23C4/08 , C23C10/02 , C23C10/08 , C23C10/28 , C23C10/48 , C23C14/16 , C23C16/20 , C23C18/54 , C23C28/00 , C23C28/04 , C23C30/00 , C23F1/00 , C25D3/50 , C25D7/00 , C25D7/04 , F01D5/28 , F01D25/00 , F02C7/00 , C25D5/10 , B32B35/00
CPC分类号： C23C10/02 , C23C18/54 , C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , C25D7/04 , Y10T428/1259 , Y10T428/12736 , Y10T428/12771 , Y10T428/12937 , Y10T428/12944 , Y10T428/265
摘要： According to an embodiment of the invention, a repaired component is disclosed. The repaired component comprises an engine run component having a base metal substrate, a portion of the base metal substrate between about 1-3 mils in thickness and an overlying bond coat having been removed to create a remaining base metal substrate of reduced thickness. The repaired component further comprises a lower growth environmental bond coating comprising an alloy having an aluminum content of about 10-60 atomic percent applied to the remaining base metal substrate so that upon subsequent repair of the component, less than about 1-3 mils in thickness of the remaining base metal substrate is removed because of less environmental coating growth into the substrate than the prior bond coat. Advantageously, the repaired component has extended component life and increased repairability.
摘要翻译：根据本发明的实施例，公开了修理的部件。被修复的部件包括具有贱金属基底的发动机运行部件，贱金属基底的厚度在约1-3密耳之间的部分和已经去除的上覆接合涂层，以产生厚度减小的剩余基底金属基底。修复的部件还包括较低生长环境粘合涂层，其包含施加到剩余的贱金属基底上的约10-60原子百分比的铝含量的合金，使得在随后修复部件时，厚度小于约1-3密耳剩余的贱金属基底被去除，因为比现有的粘合涂层更少的环境涂层生长到基底中。有利地，修复的部件具有延长的部件寿命和增加的可修复性。

14. 发明申请

US20050011593A1 PROCESS FOR A BETA-PHASE NICKEL ALUMINIDE OVERLAY COATING 有权
标题翻译：用于BET相镍镍氧化物覆层涂料的方法
公开(公告)号：US20050011593A1
公开(公告)日：2005-01-20
申请号：US10604368
申请日：2003-07-15
申请人： Theodore Grossman , Ramgopal Darolia , Joseph Rigney
发明人： Theodore Grossman , Ramgopal Darolia , Joseph Rigney
IPC分类号： C23C4/18 , C23C14/16 , C23C14/58 , C23C26/00 , C23C28/00 , C22F1/10
CPC分类号： C23C14/5886 , C23C4/18 , C23C14/16 , C23C26/00 , C23C28/3215 , C23C28/345 , C23C28/3455
摘要： A process for forming a beta-phase nickel aluminide (NiAl) overlay coating that is suitable for use as a bond coat for a thermal barrier coating (TBC). The overlay coating is deposited by a method that produces a generally columnar grain structure in which grains extend through the coating such that at least some grain boundaries are open at the coating surface. The coating is then peened with a particulate media, followed by heating the overlay coating to a temperature sufficient to cause the overlay coating to recrystallize and form new grain boundaries that are not open to the outer surface of the coating and significantly less susceptible to accelerated oxidation than the original grain boundaries. The particulate media is formed of a composition containing nickel and aluminum, such that an oxide scale that forms on the surface of the coating after the peening operation is substantially free of deleterious oxide compounds, notably iron-containing spinels.
摘要翻译：用于形成适合用作热障涂层（TBC）的粘合涂层的β-相镍铝化物（NiAl）覆盖涂层的方法。覆盖涂层通过产生大致柱状晶粒结构的方法沉积，其中晶粒延伸穿过涂层，使得至少一些晶界在涂层表面开口。然后用颗粒介质对涂层进行喷丸处理，然后将覆盖涂层加热至足以使覆盖涂层再结晶并形成不对涂层外表面开放的新晶粒边界，并显着降低易受加速氧化影响的温度比原来的晶界。颗粒介质由包含镍和铝的组合物形成，使得在喷丸操作之后在涂层表面上形成的氧化皮基本上不含有害氧化物化合物，特别是含铁尖晶石。

15. 发明申请

US20060029723A1 METHOD FOR REPAIRING COATED COMPONENTS USING NIAL BOND COATS 有权
标题翻译：使用NIAL BOND COATS修复涂层组件的方法
公开(公告)号：US20060029723A1
公开(公告)日：2006-02-09
申请号：US10714430
申请日：2003-11-13
申请人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
发明人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
IPC分类号： C23C16/52 , B05D3/00
CPC分类号： B23P6/002 , C23C10/02 , C23C10/60 , C23C28/321 , C23C28/3215 , C23C28/345 , C23C28/3455 , C23C28/36 , C25D3/50 , C25D7/00 , C25D7/008 , F05B2230/31 , F05B2230/90 , F05C2253/12
摘要： According to an embodiment of the invention, a method for repairing a coated high pressure turbine blade, which has been exposed to engine operation, to restore coated airfoil contour dimensions of the blade, and improve upon the prior bond coat is disclosed. The method comprises providing an engine run high pressure turbine blade including a base metal substrate made of a nickel-based alloy and having thereon a thermal barrier coating system. The thermal barrier coating system comprises a diffusion bond coat on the base metal substrate and a top ceramic thermal barrier coating comprising a yttria stabilized zirconia material. The top ceramic thermal barrier coating has a nominal thickness t. The method further comprises removing the thermal barrier coating system, wherein a portion of the base metal substrate also is removed, and determining the thickness of the base metal substrate removed. The portion of the base metal substrate removed has a thickness, Δt. The method also comprises applying a β phase NiAl overlay coating to the substrate, and determining the difference in thickness, Δx, between the β phase NiAl overlay coating and the previously removed bond coat. The method further comprises reapplying the top ceramic thermal barrier coating to a nominal thickness of t+Δt-Δx, wherein Δt compensates for the portion of removed base metal substrate. Advantageously, the coated airfoil contour dimensions of the high pressure turbine blade are restored to about the coated dimensions preceding the engine run.
摘要翻译：根据本发明的实施例，公开了一种已经暴露于发动机操作的用于修复涂覆的高压涡轮机叶片以恢复叶片的被覆翼型轮廓尺寸并改进先前的粘结涂层的方法。该方法包括提供一种发动机运行的高压涡轮叶片，其包括由镍基合金制成的基底金属基底并且具有热障涂层系统。热障涂层系统包括在基底金属基底上的扩散粘合涂层和包含氧化钇稳定的氧化锆材料的顶部陶瓷热障涂层。顶部陶瓷热障涂层具有标称厚度t。该方法还包括去除热障涂层系统，其中基底金属衬底的一部分也被去除，并且确定移除的母体金属衬底的厚度。去除的贱金属基材的部分厚度为Deltat。该方法还包括将β相NiAl覆盖涂层施加到基底上，并确定β相NiAl覆盖涂层与先前去除的粘结涂层之间的厚度差异Deltax。该方法还包括将顶部陶瓷热障涂层重新施加到t + Deltat-Deltax的标称厚度，其中Deltat补偿去除的基底金属基底的部分。有利地，高压涡轮机叶片的被覆翼型轮廓尺寸恢复到发动机运行之前的涂层尺寸。

16. 发明申请

US20050271514A1 COATING AND COATING PROCESS INCORPORATING RAISED SURFACE FEATURES FOR AN AIR-COOLED SURFACE 有权
标题翻译：包含空气冷却表面的提高表面特性的涂层和涂层工艺
公开(公告)号：US20050271514A1
公开(公告)日：2005-12-08
申请号：US10906903
申请日：2005-03-11
申请人： Ching-Pang Lee , Robert Schafrik , Ramgopal Darolia , Joseph Rigney
发明人： Ching-Pang Lee , Robert Schafrik , Ramgopal Darolia , Joseph Rigney
IPC分类号： B32B15/16 , C08F2/48 , C23C4/02 , C23C4/08 , C23C14/02 , C23C14/04 , C23C14/16 , C23C16/06 , C23C28/00 , F23M5/00 , F23R3/00 , F28F13/18
CPC分类号： C23C4/02 , C23C4/073 , C23C4/08 , C23C14/025 , C23C14/044 , C23C14/16 , C23C28/021 , C23C28/022 , F05B2240/11 , F05B2250/60 , F05B2260/224 , F05C2253/12 , F23M5/00 , F23M2900/05004 , F23R3/002 , F28F13/18 , F28F13/185 , Y10T428/12063 , Y10T428/12493 , Y10T428/12639 , Y10T428/12646 , Y10T428/12931 , Y10T428/12944 , Y10T428/12993
摘要： A coating and coating process for incorporating surface features on an air-cooled substrate surface of a component for the purpose of promoting heat transfer from the component. The coating process generally comprises depositing a first metallic coating material on the surface of the component using a first set of coating conditions to form a first environmental coating layer, and then depositing a second metallic coating material using a second set of coating conditions that differ from the first set, such that an outer environmental coating layer is formed having raised surface features that cause the surface of the outer environmental coating layer to be rougher than the surface of the first environmental coating layer.
摘要翻译：用于将部件的空气冷却基板表面上的表面特征引入到涂层和涂覆方法中，以促进从部件的热传递。涂覆方法通常包括使用第一组涂覆条件在组件的表面上沉积第一金属涂层材料以形成第一环境涂层，然后使用第二组涂覆条件沉积第二金属涂层材料第一组，使得外部环境涂层形成具有使外部环境涂层的表面比第一环境涂层的表面更粗糙的凸起表面特征。

17. 发明申请

US20050106316A1 Method for repairing coated components 有权
标题翻译：修复涂层部件的方法
公开(公告)号：US20050106316A1
公开(公告)日：2005-05-19
申请号：US10714213
申请日：2003-11-13
申请人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
发明人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
IPC分类号： B23P6/00 , C23C26/00 , C23C28/00 , F01D5/00 , F01D5/14 , F01D5/28 , F01D25/00 , F02C7/00 , B32B35/00
CPC分类号： C23C28/321 , C23C26/00 , C23C28/325 , C23C28/3455 , F01D5/005 , F01D5/288 , F05D2230/80 , F05D2230/90 , F05D2300/501 , Y10T29/49318
摘要： According to an embodiment of the invention, a method for repairing a coated high pressure turbine blade, which has been exposed to engine operation, to restore coated airfoil contour dimensions of the blade, is disclosed. The method comprises providing an engine run high pressure turbine blade including a base metal substrate made of a nickel-based alloy and having thereon a thermal barrier coating system. The thermal barrier coating system comprises a diffusion bond coat on the base metal substrate and a top ceramic thermal barrier coating comprising a yttria stabilized zirconia material. The top ceramic thermal barrier coating has a nominal thickness t. The method further comprises removing the thermal barrier coating system, wherein a portion of the base metal substrate also is removed, and determining the thickness of the base metal substrate removed. The portion of the base metal substrate removed has a thickness, Δt. The method also comprises reapplying the diffusion bond coat to the substrate, wherein the bond coat is reapplied to a thickness, which is about the same as applied prior to the engine operation; and reapplying the top ceramic thermal barrier coating to a nominal thickness of t+Δt, wherein Δt compensates for the portion of removed base metal substrate. Advantageously, the coated airfoil contour dimensions of the high pressure turbine blade are restored to about the coated dimensions preceding the engine run.
摘要翻译：根据本发明的实施例，公开了一种已经暴露于发动机操作的用于修复涂覆的高压涡轮机叶片以恢复叶片的被覆翼型轮廓尺寸的方法。该方法包括提供一种发动机运行的高压涡轮叶片，其包括由镍基合金制成的基底金属基底并且具有热障涂层系统。热障涂层系统包括在基底金属基底上的扩散粘合涂层和包含氧化钇稳定的氧化锆材料的顶部陶瓷热障涂层。顶部陶瓷热障涂层具有标称厚度t。该方法还包括去除热障涂层系统，其中基底金属衬底的一部分也被去除，并且确定移除的母体金属衬底的厚度。去除的贱金属基材的部分厚度为Deltat。该方法还包括将扩散粘合涂层重新施加到基底上，其中粘结涂层重新施加到与发动机操作前相同的厚度; 并将顶部陶瓷热障涂层重新施加到标称厚度t + Deltat，其中Deltat补偿去除的基底金属基底的部分。有利地，高压涡轮机叶片的被覆翼型轮廓尺寸恢复到发动机运行之前的涂层尺寸。

18. 发明申请

US20050019491A1 BETA-PHASE NICKEL ALUMINIDE OVERLAY COATING AND PROCESS THEREFOR 审中-公开
标题翻译： BETA相镍合金镀层及其工艺
公开(公告)号：US20050019491A1
公开(公告)日：2005-01-27
申请号：US10711584
申请日：2004-09-27
申请人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
发明人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
IPC分类号： C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/00 , B05D3/12
CPC分类号： C23C28/321 , C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/345 , C23C28/3455 , Y10T428/12611 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944
摘要： A beta-phase nickel aluminide (NiAl) overlay coating (24) and method for modifying the grain structure of the coating (24) to improve its oxidation resistance. The coating (24) is deposited by a method that produces a grain structure characterized by grain boundaries (44) exposed at the outer coating surface (36). The grain boundaries (44) may also contain precipitates (40) as a result of the alloyed chemistry of the coating (24). During or after deposition, the overlay coating (24) is caused to form new grain boundaries (34) that, though open to the outer surface (36) of the coating (24), are free of precipitates or contain fewer precipitates (40) than the as-deposited grain boundaries (44). New grain boundaries (34) are preferably produced by causing the overlay coating (24) to recrystallize during coating deposition or after deposition as a result of a surface treatment followed by heat treatment.
摘要翻译： β相镍铝化合物（NiAl）覆盖层（24）以及用于改变涂层（24）的晶粒结构以提高其抗氧化性的方法。通过产生以在外涂层表面（36）处暴露的晶界（44）为特征的晶粒结构的方法沉积涂层（24）。作为涂层（24）的合金化学的结果，晶界（44）也可以含有沉淀物（40）。在沉积期间或之后，使覆盖涂层（24）形成新的晶粒边界（34），其尽管向涂层（24）的外表面（36）开口，但没有沉淀物或含有较少的沉淀物（40）比沉积的晶界（44）。优选通过在涂布沉积期间或沉积后的覆盖涂层（24）进行再结晶，然后进行热处理后的表面处理，来制造新的晶界（34）。

19. 发明授权

US06884476B2 Ceramic masking material and application method for protecting turbine airfoil component surfaces during vapor phase aluminiding 有权
标题翻译：陶瓷掩模材料及其在汽相铝化过程中保护涡轮机翼部件表面的应用方法
公开(公告)号：US06884476B2
公开(公告)日：2005-04-26
申请号：US10281544
申请日：2002-10-28
申请人： Jeff Pfaendtner , James Ruud , Ted Grossman , Peter Meschter , Joseph Rigney
发明人： Jeff Pfaendtner , James Ruud , Ted Grossman , Peter Meschter , Joseph Rigney
IPC分类号： C23C8/04 , C23C14/04 , C23C14/30
CPC分类号： C23C8/04 , C23C14/04 , Y02T50/67
摘要： A masking material and a method for applying the masking material to preselected surfaces of a component to protect the surfaces to which the masking material is applied from exposure to a vapor phase of aluminum gas while a protective environmental coating is applied to other surfaces of the component. The component, such as found in the hot section of a gas turbine engine, typically has intricate internal passageways. A ceramic material is applied as a mask over preselected surfaces while leaving remaining surfaces of a component exposed. The component typically is a superalloy component, and the exposed surfaces are to be coated with an environmental protective coating. The surfaces are preselected on the basis of whether coating is desired on the surface. The ceramic material forms a continuous, crack-free mask on these preselected surfaces without obstructing the internal passageways. The ceramic material which forms a mask is stable at the elevated temperatures of environmental coating application. The ceramic mask material must be continuous and substantially crack-free to prevent the penetration of the aggressive gas phase of the environmental coating material onto the surface of the component where it would otherwise undesirably be deposited. The ceramic material does not react with either the surface of the superalloy component or the gaseous vapors of the coating composition. At the conclusion of the coating operation, the ceramic coating applied as a mask can be easily and completely removed from the surface of the substrate by simple mechanical means, which surface is free of any coating from the coating operation.
摘要翻译：掩模材料和将掩蔽材料施加到部件的预选表面上以将保护掩模材料施加的表面暴露于铝气体的气相的方法，同时将保护性环境涂层施加到部件的其它表面。诸如在燃气涡轮发动机的热段中发现的部件通常具有复杂的内部通道。将陶瓷材料作为掩模施加在预选表面上，同时使元件的剩余表面露出。组分通常是超合金组分，并且暴露的表面将被涂覆有环境保护涂层。基于是否需要在表面上涂布来预选表面。陶瓷材料在这些预选表面上形成连续的，无裂纹的掩模，而不会阻碍内部通道。形成掩模的陶瓷材料在环境涂料应用的高温下是稳定的。陶瓷掩模材料必须是连续的且基本无裂纹的，以防止环境涂层材料的腐蚀性气相渗透到组件的表面上，否则其将不希望地沉积。陶瓷材料不与超合金组分的表面或涂料组合物的气体蒸气反应。在涂布操作结束时，作为掩模施加的陶瓷涂层可以通过简单的机械装置容易且完全地从基板的表面去除，该表面没有涂层操作的任何涂层。

20. 发明申请

US20050084706A1 Method of selective region vapor phase aluminizing 有权
标题翻译：选择性区域气相镀铝的方法
公开(公告)号：US20050084706A1
公开(公告)日：2005-04-21
申请号：US10685637
申请日：2003-10-15
申请人： Nripendra Das , Joseph Rigney , Jeffrey Pfaendtner , Matthew Saylor
发明人： Nripendra Das , Joseph Rigney , Jeffrey Pfaendtner , Matthew Saylor
IPC分类号： C23C10/02 , C23C10/06 , C23C10/14 , B32B15/10
CPC分类号： C23C10/06 , C23C10/02 , C23C10/14 , Y02T50/67 , Y10T428/12736
摘要： The present invention is process for forming diffusion aluminide coatings on an uncoated surface of a substrate, without interdiffusing a sufficient amount of aluminum into a coating layer to adversely affect the coating growth potential and mechanical properties of said coating layer. A metal substrate is provided comprising an external surface and an internal passage therein defined by an internal surface, at least a portion of the external surface of the substrate being coated with a coating layer selected from the group consisting of β-NiAl-base, MCrAlX, a line-of-sight diffusion aluminide, a non-line-of-sight diffusion aluminide, a pack diffusion aluminide, and a slurry diffusion aluminide on said substrate. The external surface of the substrate is cleaned. The metal substrate is subjected to a aluminum vapor phase deposition process performed using a fluorine-containing activator selected from the group consisting of AlF3, CrF3, NH4F, and combinations thereof, at a rate in the range of about 0.036 mols of fluorine per ft3/hr of transport gas to about 0.18 mols of fluorine per ft3/hr of transport gas, at a temperature in the range of about 1350° F. (730° C.) to about 1925° F. (1050° C.), using a transport gas selected from the group consisting of argon, nitrogen, hydrogen, and combinations thereof, the transport gas being provided at a flow rate in the range of about 20 ft3/hr to about 120 ft3/hr for a period of time in the range of about 2 hours to about 10 hours. The substrate is then cooled. The present invention is also a superalloy article coated with a diffusion aluminide layer using the diffusion aluminide coating process of the present invention.
摘要翻译：本发明是在基材的未涂覆表面上形成扩散铝化物涂层的方法，而不会将足够量的铝相互扩散到涂层中，从而不利地影响涂层生长电位和所述涂层的机械性能。提供了一种金属基底，其包括由内表面限定的外表面和内部通道，所述基底的外表面的至少一部分被涂覆有选自β-NiAl基，MCrAlX ，视线扩散铝化物，非视线扩散铝化物，包层扩散铝化物和在所述衬底上的浆料扩散铝化物。清洁基板的外表面。对金属基板进行铝蒸气相沉积工艺，该方法使用选自AlF 3 N 3，CrF 3 N，NH 4的含氟活化剂 F和它们的组合，以约0.036摩尔氟/ ft 3 /小时的运输气体至约0.18摩尔氟/ ft 3的范围内的速率，在约1350°F（730℃）至约1925°F（1050℃）的温度范围内使用选自以下的输送气体：氩气，氮气，氢气及其组合，输送气体的流速为约20ft 3 / hr至约120ft 3 / hr 一段时间在约2小时至约10小时的范围内。然后将衬底冷却。本发明也是使用本发明的扩散铝化物涂覆方法涂覆有扩散铝化物层的超级合金制品。

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