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11. 发明授权

US5385753A Process for reactively coating particles 失效
标题翻译：反应性地涂覆颗粒的方法
公开(公告)号：US5385753A
公开(公告)日：1995-01-31
申请号：US114028
申请日：1993-08-30
申请人： Patrick C. Hu , Richard I. Leavitt
发明人： Patrick C. Hu , Richard I. Leavitt
IPC分类号： B01J2/00 , C09C1/40 , B05D7/00
CPC分类号： C09C1/405 , B01J2/006 , C01P2004/61 , C01P2004/62 , C01P2004/80 , C01P2004/84 , C01P2006/60
摘要： Coated particles having properties such as to make them suitable as replacements for titanium dioxide particles can be obtained by reacting a titanium or zirconium halide, ether, or ester with zeolite hydrate particles so as to coat the zeolite particles with titania or zirconia. The reaction is preferably conducted between a titanium compound, such as titanium tetrachloride, and the zeolite in an inert medium, such as anhydrous or substantially anhydrous air or a hydrocarbon.
摘要翻译：可以通过使钛或卤化锆，醚或酯与沸石水合物颗粒反应，以便用二氧化钛或氧化锆涂覆沸石颗粒来获得具有如二氧化钛颗粒替代物的性质的涂层颗粒。该反应优选在诸如四氯化钛的钛化合物和惰性介质如无水或基本无水的空气或烃中的沸石之间进行。

12. 发明授权

US5256390A Biocidal zeolite particles 失效
标题翻译：杀生物沸石颗粒
公开(公告)号：US5256390A
公开(公告)日：1993-10-26
申请号：US548484
申请日：1990-07-03
申请人： Patrick C. Hu
发明人： Patrick C. Hu
IPC分类号： A01N25/08 , C01B39/02 , C01B33/34
CPC分类号： C01B39/026 , A01N25/08 , Y10S423/24
摘要： A method of producing zeolite particles with reduced carbonate species so that the zeolite particles are ion exchangeable with biocidal metal ions.
摘要翻译：制备具有降低碳酸盐物质的沸石颗粒的方法，使得沸石颗粒可与杀生物金属离子进行离子交换。

13. 发明授权

US08940329B2 High ibuprofen content granules and their preparation and their use in pharmaceutical dosage forms 有权
标题翻译：高布洛芬含量颗粒及其制备及其在药物剂型中的应用
公开(公告)号：US08940329B2
公开(公告)日：2015-01-27
申请号：US11260662
申请日：2005-10-28
申请人： Patrick C. Hu , Gregory H. Lambeth , Arcelio J. Malcolm
发明人： Patrick C. Hu , Gregory H. Lambeth , Arcelio J. Malcolm
IPC分类号： A61K9/20 , A01N37/10 , A61K31/19 , A61K9/16 , A61K31/192
CPC分类号： A61K9/2077 , A61K9/1652 , A61K9/1688 , A61K9/1694 , A61K9/2059 , A61K31/192
摘要： Described are granules composed at least of a substantial amount of ibuprofen, at least one pharmaceutically-acceptable super disintegrant, and at least one pharmaceutically-acceptable binder different from the super disintegrant(s), the super disintegrant(s) being substantially uniformly dispersed throughout the granules. The methods for preparing such granules are described. The granules are useful in forming solid dosage forms such as filled capsules or compressed solid dosage forms.
摘要翻译：描述了至少包含大量布洛芬，至少一种药学上可接受的超级崩解剂和至少一种不同于超级崩解剂的药学上可接受的粘合剂的颗粒，所述超级崩解剂基本均匀地分散在整个颗粒。描述了制备这种颗粒的方法。颗粒可用于形成固体剂型，例如填充胶囊或压缩固体剂型。

14. 发明授权

US5487882A Process for preparation of zeolite "X" 失效
标题翻译：沸石“X”的制备方法
公开(公告)号：US5487882A
公开(公告)日：1996-01-30
申请号：US275722
申请日：1994-07-19
申请人： Patrick C. Hu , Eric W. Liimatta
发明人： Patrick C. Hu , Eric W. Liimatta
IPC分类号： C01B39/22
CPC分类号： C01B39/22 , Y10S423/21
摘要： A method for producing crystalline synthetic faujasite of the zeolite "X" type is disclosed. The method comprises (a) separately preparing a sodium silicate solution and a sodium aluminate solution, (b) admixing the sodium silicate solution and the sodium aluminate solution at high shear until a mixture results having a ratio of sodium oxide to silica of 0.4:1 to 2:1, silica to alumina of 2.2:1 to 3.5:1, and water to sodium oxide of 20:1 to 70:1, (c) heating said mixture to a temperature of about 80.degree. to 120.degree. C. in the absence of any further mixing for a period of time sufficient to produce the desired crystalline faujasite of the zeolite "X" type, and (d) recovering said zeolite "X".
摘要翻译：公开了一种生产沸石“X”型结晶合成八面沸石的方法。该方法包括（a）分别制备硅酸钠溶液和铝酸钠溶液，（b）以高剪切力混合硅酸钠溶液和铝酸钠溶液，直到混合物的氧化钠与二氧化硅的比例为0.4:1 至2:1，二氧化硅与氧化铝的比例为2.2:1至3.5:1，水至氧化钠的比例为20:1至70:1，（c）将所述混合物加热至约80℃至120℃的温度没有任何进一步混合足以产生沸石“X”型所需的结晶八面沸石的时间段，和（d）回收所述沸石“X”。

15. 发明授权

US5183061A Silicon compounds in bone treatment 失效
标题翻译：硅化合物在骨治疗
公开(公告)号：US5183061A
公开(公告)日：1993-02-02
申请号：US692778
申请日：1991-04-26
申请人： Karl E. Wiegand , Patrick C. Hu
发明人： Karl E. Wiegand , Patrick C. Hu
IPC分类号： A61K31/695 , A61K31/70 , C07F7/04 , C07H23/00
CPC分类号： A61K31/7004 , A61K31/695 , A61K31/70 , C07F7/045 , C07H23/00
摘要： Organic silicon compounds such as tetraloweralkylorthosilicates, silicon tetracarboxylates, and silicon-containing reaction products derived from carbohydrates, such as glucose, sucrose, and ascorbic acid are useful in treating, preventing, or delaying the onset of bone disease in warm blooded vertebrates, including man and domesticated animals of economic importance, such as poultry, house pets, and horses, cattle, swine, and sheep.
摘要翻译：诸如葡萄糖，蔗糖和抗坏血酸等碳水化合物衍生的有机硅化合物，例如四氢二烷基硅酸盐，四羧酸硅酸盐和含硅反应产物，可用于治疗，预防或延迟温血脊椎动物以及家禽，家养宠物，马，牛，猪，羊等具有经济意义的驯养动物。

16. 发明授权

US4917045A Silicon compounds in poultry hatching 失效
标题翻译：家禽孵化中的硅化合物
公开(公告)号：US4917045A
公开(公告)日：1990-04-17
申请号：US223020
申请日：1988-07-22
申请人： Karl E. Wiegand , Patrick C. Hu
发明人： Karl E. Wiegand , Patrick C. Hu
IPC分类号： A01K45/00 , C07H23/00
CPC分类号： C07H23/00 , A01K45/007
摘要： Organic silicon compounds in which silicon is solely bonded to oxygen, fluorine, chlorine or bromine such that not less than one-fourth of the silicon valences are satisfied by bonding to oxygen, stimulate the deposition of bone in bird embryos. Preferred birds are domestic fowl, such as chickens and turkeys. The silicon compounds are administered to the bird eggs by such means as injecting the eggs, or spraying or soaking them.
摘要翻译：有机硅化合物，其中硅仅与氧，氟，氯或溴结合，使得不少于四分之一的硅价通过结合氧来满足，刺激骨在鸟胚中的沉积。首选的鸟类是家禽，如鸡和火鸡。硅化合物通过诸如注射鸡蛋或喷洒或浸泡的方式施用于鸡蛋。

17. 发明授权

US4731196A Process for making bleach activator 失效
标题翻译：制备漂白活化剂的方法
公开(公告)号：US4731196A
公开(公告)日：1988-03-15
申请号：US923891
申请日：1986-10-28
申请人： James S. Staton , Patrick C. Hu
发明人： James S. Staton , Patrick C. Hu
IPC分类号： C11D3/39 , C09K3/00
CPC分类号： C11D3/3935 , C11D3/3932
摘要： A manganese exchanged Zeolite A laundry bleach activator is made in a single reaction vessel by mixing dry Zeolite A with an inorganic acid in an amount to lower the pH to 8.0-10.5, adding and mixing in an aqueous manganese (II) salt, adding and mixing in a chelating agent such as sodium tripolyphosphate, adding and mixing in a binding agent such as carboxymethylcellulose, mixing and adding water to cause the Mn-exchanged Zeolite A, chelating agent and binder to agglomerate to form small granules and drying the resulting small granules for use as a bleach activator in laundry detergent compositions.
摘要翻译：通过将干燥的沸石A与无机酸混合，将pH降低至8.0-10.5，在单一的反应容器中制备锰交换的沸石A洗衣漂白活化剂，在含水锰酸盐（II）中加入和混合，在螯合剂如三聚磷酸钠中混合，在粘合剂如羧甲基纤维素中加入并混合，混合并加水，使Mn交换的沸石A，螯合剂和粘合剂结块形成小颗粒并干燥得到的小颗粒用作洗衣洗涤剂组合物中的漂白活化剂。

18. 发明授权

US09629806B2 High content sodium ibuprofen granules, their preparation and their use in preparing non-effervescent solid dosage forms 有权
公开(公告)号：US09629806B2
公开(公告)日：2017-04-25
申请号：US13054369
申请日：2009-07-13
申请人： Patrick C. Hu
发明人： Patrick C. Hu
IPC分类号： A61K9/16 , A61K9/20
CPC分类号： A61K31/192 , A61K9/1611 , A61K9/1635 , A61K9/1652 , A61K9/1694 , A61K9/2009 , A61K9/2027 , A61K9/2054
摘要： Granules of racemic sodium ibuprofen dihydrate formed from components specified herein have very desirable properties and can be effectively used in conventional rotary press tableting equipment without operational difficulties often encountered in actual practice. Their preparation by a wet granulation process, the wet granule compositions, formulations adapted for preparation of solid dosage forms utilizing a rotary press, solid dosage forms, and methods of preparing solid dosage forms in a rotary press are also described.

19. 发明授权

US06357678B1 Process for producing ultra finely-divided zeolite powder 失效
标题翻译：用于生产超细粉末沸石粉末的方法
公开(公告)号：US06357678B1
公开(公告)日：2002-03-19
申请号：US09430856
申请日：1999-10-29
申请人： Patrick C. Hu , Conrad J. Langlois, Jr. , Ronald L. Camp
发明人： Patrick C. Hu , Conrad J. Langlois, Jr. , Ronald L. Camp
IPC分类号： B02C1700
CPC分类号： C01B39/026
摘要： Particulate synthetic zeolite is micronized in a liquid organic medium to form a micronized zeolite product having an average (mean) particle size of about 2 microns or less and containing at least 90% by weight, based on the dry weight of the zeolite product, if isolated, of particles no larger than about 5 microns. Preferably, the micronized zeolite product has a mean particle size of 1 micron or less, and at least 90% by weight of the zeolite product, based on the dry weight of the zeolite product, if isolated, has a particle size of 2 microns or less. The liquid organic medium used is (a) inert or substantially inert, (b) devoid or substantially devoid of water, and (c) devoid of a dispersant.
摘要翻译：颗粒状合成沸石在液体有机介质中微粉化以形成平均（平均）粒度为约2微米或更小并且基于沸石产物的干重至少包含90重量％的微粉化沸石产物，如果分离的不大于约5微米的颗粒。优选地，微粉化的沸石产物具有1微米或更小的平均粒度，并且基于沸石产物的干重，至少90重量％的沸石产物，如果分离，其粒径为2微米，或减。所使用的液体有机介质是（a）惰性或基本上惰性的，（b）不含或基本上不含水，和（c）不含分散剂。

20. 发明授权

US6035869A Dish-washing method 失效
标题翻译：洗碗方式
公开(公告)号：US6035869A
公开(公告)日：2000-03-14
申请号：US182749
申请日：1998-10-29
申请人： Deborah A. Quebedeaux , Joe D. Sauer , Conrad J. Langlois, Jr. , Patrick C. Hu
发明人： Deborah A. Quebedeaux , Joe D. Sauer , Conrad J. Langlois, Jr. , Patrick C. Hu
IPC分类号： C11D1/14 , C11D1/75 , C11D1/83 , C11D3/02 , C11D11/00 , C11D17/00 , B08B3/08
CPC分类号： C11D3/046 , C11D1/75 , C11D1/83 , C11D11/0023 , C11D17/0065 , C11D1/143
摘要： Dishes are cleaned by washing them with a cleaning implement which has been charged with the detergent in a solid block made from a formulation having a water-soluble alkali metal salt content of 15-60% by weight and a surfactant content of 10-70% by weight, said surfactant comprising 15-100% by weight of at least one amine oxide corresponding to the formula RR'R"NO .multidot.nH.sub.2 O in which R and R' are independently selected from methyl, ethyl, and 2-hydroxyethyl, R" is a primary alkyl group containing 12-16 carbons, and n represents 0, 1, or 2.
摘要翻译：通过用已经装有洗涤剂的清洁工具清洗碟子，该清洁工具由固体块组成，该固体块由水溶性碱金属盐含量为15-60重量％，表面活性剂含量为10-70重量％所述表面活性剂包含15-100重量％的至少一种对应于式RR'R'NO x·6H 2 O的氧化胺，其中R和R'独立地选自甲基，乙基和2-羟基乙基，R' '是含有12-16个碳原子的伯烷基，n代表0,1或2。

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