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11. 发明授权

US5079323A Polysiloxazanes, silicon oxynitride fibers and processes for producing same 失效
标题翻译：聚硅氧烷，硅氧烷纤维及其生产方法
公开(公告)号：US5079323A
公开(公告)日：1992-01-07
申请号：US555067
申请日：1990-07-18
申请人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
IPC分类号： D01F9/10 , C04B35/589 , C08G77/48 , C08G77/54
CPC分类号： C04B35/589 , C08G77/54
摘要： Novel polysiloxazanes comprising --SiH.sub.2).sub.n NH] and --SiH.sub.2).sub.m O] as the main repeating units are provided. The polysiloxazanes are produced by reacting a dihalosilane or an adduct thereof with a Lewis base, with ammonia and water vapor or oxygen. From the polysiloxazane, novel silicon oxynitride shapes can be produced and the silicon oxynitride shapes are essentially composed of silicon, nitride (5 mol % or more) and oxygen (5 mol % or more).

12. 发明授权

US4975512A Reformed polysilazane and method of producing same 失效
标题翻译：改性聚硅氮烷及其制备方法
公开(公告)号：US4975512A
公开(公告)日：1990-12-04
申请号：US230422
申请日：1988-08-10
申请人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
IPC分类号： C04B35/589 , C08G77/62
CPC分类号： C04B35/589 , C08G77/62
摘要： A novel, reformed polysilazane obtained by reacting a polysilazane with a compound selected from ammonia, primary and secondary amines, hydrazine and mono-, di- and tri-substituted hydrazines to cross-link the polysilazane with the compound serving as a cross-linking agent or to link the compound to the polysilazane.

13. 发明授权

US4869858A Processes for producing polysiloxazanes and silicon oxynitride fibers 失效
标题翻译：生产聚硅氮烷和氮氧化硅纤维的方法
公开(公告)号：US4869858A
公开(公告)日：1989-09-26
申请号：US13680
申请日：1987-02-12
申请人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
IPC分类号： D01F9/10 , C04B35/589 , C08G77/48 , C08G77/54
CPC分类号： C04B35/589 , C08G77/54
摘要： Novel polysiloxazanes comprising [(SiH.sub.2).sub.n NH] and [(SiH.sub.2).sub.m O] as the main repeating units are provided. The polysiloxazanes are produced by reacting a dihalosilane or an adduct thereof with a Lewis base, with ammonia and water vapor or oxygen. From the polysiloxazane, novel silicon oxynitride shapes can be produced and the silicon oxynitride shapes are essentially composed of silicon, nitride (5 mol % or more) and oxygen (5 mol % or more).
摘要翻译：提供了包含[（SiH 2）nNH]和[（SiH 2）m O]作为主要重复单元的新型聚硅氧氮烷。聚硅氧烷是通过使二氯硅烷或其加合物与路易斯碱反应，与氨和水蒸汽或氧气反应制备的。从聚硅氮烷可以制造新的氮氧化硅形状，氮氧化硅形状主要由硅，氮化物（5摩尔％以上）和氧（5摩尔％以上）组成。

14. 发明授权

US4861569A Reformed, inorganic polysilazane and method of producing same 失效
标题翻译：改性无机聚硅氮烷及其制备方法
公开(公告)号：US4861569A
公开(公告)日：1989-08-29
申请号：US230421
申请日：1988-08-10
申请人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
IPC分类号： C08G77/62
CPC分类号： C08G77/62
摘要： A novel, reformed, inorganic polysilazane which is liquid or solid at room temperature and soluble in o-xylene at room temperature and which has (a) a number-average molecular weight of 200-500,000, (b) contents of Si, N and H of 50-70% by weight, 20-34% by weight and 5-9% by weight, respectively; and (c) --SiH.sub.2 -- and --SiH.sub.3 groups, the molar ratio of the --SiH.sub.2 -- groups to the --SiH.sub.3 groups being 2.0:1 to 8.4:1. The reformed polysilazane is obtained by reaction of a solution of a polysilazane in an organic base-containing solvent to polycondense the polysilazane.

15. 发明授权

US5292830A Thermosetting copolymers, silicon carbide-based fiber and processes for producing same 失效
标题翻译：热固性共聚物，碳化硅基纤维及其制备方法
公开(公告)号：US5292830A
公开(公告)日：1994-03-08
申请号：US900843
申请日：1992-06-18
申请人： Osamu Funayama , Tomohiro Kato , Rika Takatsu , Yuuji Tashiro , Toshihide Kishi , Takayuki Date , Takeshi Isoda
发明人： Osamu Funayama , Tomohiro Kato , Rika Takatsu , Yuuji Tashiro , Toshihide Kishi , Takayuki Date , Takeshi Isoda
IPC分类号： C04B35/571 , C08G77/60 , C08G79/00 , C08L83/16 , C08G77/56
CPC分类号： C08L83/16 , C04B35/571 , C08G77/60 , C08G79/00 , Y10T428/2913 , Y10T428/2916
摘要： A thermoplastic silicon-containing polymer, which may be a precursor of SiC, and which can be transformed to a thermosetting polymer by copolymerizing it with a thermosetting perhydropolysilazane or polyborosilazane.
摘要翻译：一种热塑性含硅聚合物，其可以是SiC的前体，并且可以通过使其与热固性全氢聚硅氮烷或聚硼硅氮烷共聚而转变成热固性聚合物。

16. 发明授权

US4795622A Method for producing silicon-imide 失效
标题翻译：生产硅酰亚胺的方法
公开(公告)号：US4795622A
公开(公告)日：1989-01-03
申请号：US855453
申请日：1986-04-24
申请人： Takeshi Isoda , Mikiro Arai
发明人： Takeshi Isoda , Mikiro Arai
IPC分类号： C01B21/068 , C01B21/082
CPC分类号： C01B21/068 , C01P2002/82 , C01P2002/88
摘要： A silicon halide, preferably SiCl.sub.4, is reacted with an excess of a base, e.g. a Lewis base or Bronsted base with steric hindrance group to produce an adduct. The adduct, which need not be separated, is treated with ammonia gas to produce the imide of silicon. A light organic solvent is used. The temperature used is -78.degree. C. to 100.degree. C. and the reaction is rapid.Byproduct ammonium halide is removed, and the imide is heated at 1000.degree. C. to 1600.degree. C. in an oven in an atmosphere containing nitrogen, to produce silicon nitride of good sintering characteristics and more than 70 wt % of which is of the .alpha.-crystal form.
摘要翻译：将卤化硅，优选SiCl 4与过量的碱反应，例如，路易斯碱或具有空间位阻基团的布朗斯台德碱，以产生加合物。不需要分离的加合物用氨气处理以产生硅的酰亚胺。使用轻质有机溶剂。使用的温度为-78℃至100℃，反应快。除去副产物卤化铵，并将酰亚胺在含氮气氛中的烘箱中在1000℃加热至1600℃，以产生具有良好烧结特性的氮化硅，其中70重量％以上为α 晶体形式。

17. 发明授权

US4840778A Inorganic polysilazane and method of producing the same 失效
标题翻译：无机聚硅氮烷及其制备方法
公开(公告)号：US4840778A
公开(公告)日：1989-06-20
申请号：US801884
申请日：1985-11-26
申请人： Mikiro Arai , Takeshi Isoda , Takuji Itoh
发明人： Mikiro Arai , Takeshi Isoda , Takuji Itoh
IPC分类号： C01B21/068 , C01B21/082 , C01B21/087 , C04B35/589 , C04B35/622 , C07F7/02 , C08G77/62
CPC分类号： C08G77/62 , C01B21/068 , C01B21/087 , C04B35/589 , C04B35/62227 , C07F7/025 , C01P2002/82 , C01P2002/86 , C01P2004/10
摘要： Novel primarily chain inorganic polysilazanes of average molecular weight of 690 to 2000 are prepared from novel adducts of a halosilane and a base by reacting the adducts with ammonia in unreactive solvents. Silicon nitride is prepared by heating the polysilazanes at 1000.degree. to 1600.degree. C., preferably below 1300.degree. C., most preferably 1000.degree. to 1100.degree. C.
摘要翻译：新型的无机聚硅氮烷平均分子量为690〜2000的新型无机聚硅氮烷由卤代硅烷和碱的新加成物通过使加合物与氨在非反应性溶剂中反应而制备。通过在1000℃至1600℃，优选低于1300℃，最优选1000℃至1100℃下加热聚硅氮烷来制备氮化硅。

18. 发明授权

US5494978A Modified polysilazane and process for preparation thereof 失效
标题翻译：改性聚硅氮烷及其制备方法
公开(公告)号：US5494978A
公开(公告)日：1996-02-27
申请号：US346845
申请日：1994-11-30
申请人： Yasuo Shimizu , Yuuji Tashiro , Hiroyuki Aoki , Masaaki Ichiyama , Hayato Nishii , Toshihide Kishi , Kouji Okuda , Takeshi Isoda
发明人： Yasuo Shimizu , Yuuji Tashiro , Hiroyuki Aoki , Masaaki Ichiyama , Hayato Nishii , Toshihide Kishi , Kouji Okuda , Takeshi Isoda
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62 , C08F283/12
CPC分类号： C08G77/62 , C04B35/589
摘要： A stabilized polysilazane obtained by reacting an inorganic polysilazane having a number average molecular weight of about 100 to about 100,000 with an alcohol, an organic acid, an ester, a ketone, an aldehyde, a mercaptan, or an alkysilazane preferably at a molar ratio of from 50/50 to 99.99/0.01 is described.
摘要翻译：将数均分子量为约100〜约100,000的无机聚硅氮烷与醇，有机酸，酯，酮，醛，硫醇或烷基硅氮烷反应得到的稳定化聚硅氮烷，优选摩尔比为从50/50至99.99 / 0.01。

19. 发明授权

US5436398A Polymetalosilazane, process of producing same, silicon nitride based ceramic, and process of preparing same 失效
标题翻译：聚甲硅氮烷，其制备方法，氮化硅基陶瓷及其制备方法
公开(公告)号：US5436398A
公开(公告)日：1995-07-25
申请号：US223866
申请日：1994-04-06
申请人： Yasuo Shimizu , Hirohiko Nakahara , Tomoko Aoki , Osamu Funayama , Takeshi Isoda
发明人： Yasuo Shimizu , Hirohiko Nakahara , Tomoko Aoki , Osamu Funayama , Takeshi Isoda
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62 , C08G79/00 , D01F9/10 , C08L83/04
CPC分类号： D01F9/10 , C04B35/589 , C08G77/62 , C08G79/00
摘要： A preceramic polymetalosilazane substantially free of Si-O groups is produced by reacting a polysilazane with a metal alkoxide in the presence of an alkylsilazane or alkylsilane. The preceramic polymer gives a high strength and heat resistant ceramic body which remains amorphous when calcined at 1,600.degree. C. for 10 hours in the atmosphere of nitrogen.
摘要翻译：通过在烷基硅氮烷或烷基硅烷的存在下使聚硅氮烷与金属醇盐反应来制备基本上不含Si-O基的预陶瓷聚金属硅氮烷。陶瓷聚合物提供了一种高强度和耐热的陶瓷体，当在氮气气氛中在1600℃下煅烧10小时时，其保持无定形。

20. 发明授权

US5905130A Process for the production of polysilazane 失效
标题翻译：聚硅氮烷生产工艺
公开(公告)号：US5905130A
公开(公告)日：1999-05-18
申请号：US894663
申请日：1997-08-25
申请人： Hirohiko Nakahara , Osamu Funayama , Takeshi Isoda
发明人： Hirohiko Nakahara , Osamu Funayama , Takeshi Isoda
IPC分类号： C08G77/62 , C08G77/08
CPC分类号： C08G77/62
摘要： Disclosed is a process for the production of a polysilazane containing Si--N linkages in the main chain thereof. According to the present invention, the polysilazane is produced by reacting a polyaminosilane compound with a polyhydrogenated nitrogen-containing compound in the presence of a basic catalyst or by reacting a polyhydrogenated silicon compound with a polyhydrogenated nitrogen-containing compound in the presence of a basic solid oxide catalyst.
摘要翻译： PCT No.PCT / JP97 / 00005 Sec。 371日期1997年8月25日第 102（e）日期1997年8月25日PCT 1997年1月6日PCT PCT。出版物WO97 / 24391 日期1997年7月10日公开是在其主链中生产含有Si-N键的聚硅氮烷的方法。根据本发明，聚硅氮烷是在碱性催化剂的存在下使聚氨基硅烷化合物与多氢化含氮化合物反应制备的，或者是通过使多氢化硅化合物与多氢化含氮化合物在碱性固体氧化物催化剂。

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