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11. 发明申请

US20080269435A1 Polymerization Process 有权
标题翻译：聚合过程
公开(公告)号：US20080269435A1
公开(公告)日：2008-10-30
申请号：US10585199
申请日：2004-12-27
申请人： Kalle Kallio , Janne Maaranen , Eija Lappi , Marina Surakka
发明人： Kalle Kallio , Janne Maaranen , Eija Lappi , Marina Surakka
IPC分类号： C08F2/00 , B01J19/00
CPC分类号： C08F10/02 , B01J8/0015 , B01J19/2435 , B01J2208/00283 , B01J2208/00707 , C08F210/16 , Y10S526/905 , C08F2/00 , C08F2/06 , C08F2/42 , C08F2/14 , C08F210/14
摘要： A process for the polymerisation of ethylene and optionally at least one C3-20 alpha olefin comonomer in the slurry or solution phase in a reactor having a polymer outlet stream, a procatalyst or catalyst feed stream and a hydrogen feed stream, said polymerisation being effected in the presence of a metallocene catalyst, a diluent and hydrogen, wherein said diluent is recycled from said outlet stream to said hydrogen feed stream, said procatalyst or catalyst feed stream is free of hydrogen, said hydrogen feed stream is free of procatalyst or catalyst and said procatalyst or catalyst feed stream does not comprise recycled diluent.
摘要翻译：在具有聚合物出口流，原催化剂或催化剂进料流和氢气的反应器中，在淤浆或溶液相中使乙烯和任选的至少一种C 3-20α-烯烃共聚单体聚合的方法所述聚合在茂金属催化剂，稀释剂和氢气存在下进行，其中所述稀释剂从所述出口流再循环到所述氢气进料流中，所述前催化剂或催化剂进料流不含氢气，所述氢气进料流不含主催化剂或催化剂，并且所述原催化剂或催化剂进料流不包含再循环稀释剂。

12. 发明授权

US06284849B1 Method of catalyst transitions in olefin polymerizations 失效
标题翻译：烯烃聚合中催化剂转变的方法
公开(公告)号：US06284849B1
公开(公告)日：2001-09-04
申请号：US09142402
申请日：1999-01-11
申请人： Vidar Almquist , Tone Aastad , Ingrid Sorum Melaaen , Harri Hokkanen , Kalle Kallio
发明人： Vidar Almquist , Tone Aastad , Ingrid Sorum Melaaen , Harri Hokkanen , Kalle Kallio
IPC分类号： C08F238
CPC分类号： C08F10/00 , Y10S526/943 , C08F2/42
摘要： A method for transitioning between two different catalysts in olefin polymerizations, a first catalyst and a second catalyst, comprising the steps of: discontinuing the feed of the first catalyst into the polymerization reactor, and introducing the second catalyst into the reactor, wherein the transition is performed between a chromium-based catalyst and a metallocene catalyst.
摘要翻译：一种用于在烯烃聚合中的两种不同催化剂之间转化的方法，第一催化剂和第二催化剂，包括以下步骤：将第一催化剂进料停止进入聚合反应器，并将第二催化剂引入反应器，其中转变为在铬基催化剂和茂金属催化剂之间进行。

13. 发明授权

US08962509B2 Preparation of a solid catalyst system 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US08962509B2
公开(公告)日：2015-02-24
申请号：US13695884
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
IPC分类号： C08F4/602 , C08F4/642 , C08F4/6592 , C08F10/00 , C08F4/76 , C07F5/06 , C08F4/52 , B01J31/12 , B01J31/14 , B01J31/22 , B01J31/26
CPC分类号： C08F4/76 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/46 , B01J2531/48 , B01J2531/49 , B01J2531/90 , B01J2531/94 , C07F5/068 , C08F4/52 , C08F4/6028 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , Y10S526/943 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system (CS) comprising the steps of preparing a liquid clathrate (LC) comprising (a) a lattice (L) being the reaction product of (i) aluminoxane (A), (ii) an organometallic compound (O) of a transition metal (M) of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and (i) a compound (B) being effective to form with the aluminoxane (A) and the organometallic compound (O) the lattice (L), and (b) a guest (G) being an hydrocarbon compound (HC), and subsequently precipitating said liquid clathrate (LC) obtaining said solid catalyst system (SC).
摘要翻译：制备固体催化剂体系（CS）的方法，包括以下步骤：制备液体包合物（LC），其包含（a）格子（L），其为（i）铝氧烷（A），（ii）有机金属（IUPAC 2007）第3至10族的过渡金属（M）或锕系元素或镧系元素的化合物（O）和（i）与铝氧烷（A）形成有效的化合物（B）和有机金属化合物（O），晶格（L）和（b）作为烃化合物（HC）的客体（G），随后沉淀得到所述固体催化剂体系（SC）的所述液体包合物（LC）。

14. 发明授权

US08409681B2 Multi-stage process for producing multi-modal linear low density polyethylene 有权
标题翻译：生产多模式线性低密度聚乙烯的多阶段工艺
公开(公告)号：US08409681B2
公开(公告)日：2013-04-02
申请号：US13126496
申请日：2010-02-22
申请人： Thomas Garoff , Paivi Waldvogel , Kalle Kallio , Virginie Eriksson , Aki Aittola , Esa Kokko
发明人： Thomas Garoff , Paivi Waldvogel , Kalle Kallio , Virginie Eriksson , Aki Aittola , Esa Kokko
IPC分类号： B32B1/08 , C08F2/14 , C08F2/34 , C08F210/14 , C08F4/685
CPC分类号： C08F10/00 , C08F110/02 , C08F210/16 , C08F2410/03 , Y10T428/139 , C08F4/6357 , C08F4/685 , C08F2/001 , C08F2500/07 , C08F2500/12 , C08F2500/05 , C08F2500/18 , C08F210/14 , C08F2500/08
摘要： A process is disclosed for producing a multi-modal linear low density polyethylene in at least two staged reactors connected in series, comprising (i) polymerizing in a first slurry phase stage ethylene monomers with a Ziegler-Natta polymerization catalyst system to obtain a first polyethylene fraction component (A); and (ii) polymerizing in a second gas or slurry phase stage ethylene monomers with a Ziegler-Natta polymerization catalyst system to obtain a second polyethylene fraction component (B). The Ziegler-Natta polymerization catalyst system comprises: 1) a solid procatalyst formed by contacting at least: a) a Mg-alcoholate complex of formula (I) b) an aluminum compound of formula (II); and c) a vanadium compound and a titanium compound having a molar ratio (V:Ti) from 10:90 to 90:10; and 2) one or more organometallic cocatalvsts of formula (III). The linear low density polyethylene shows an improved comonomer composition distribution Formulas (I), (II), and (III) are described herein.
摘要翻译：公开了一种用于在至少两个分级反应器中串联生产多模式线性低密度聚乙烯的方法，其包括（i）在第一浆液阶段中聚合乙烯单体与齐格勒 - 纳塔聚合催化剂体系以获得第一聚乙烯级分组分（A）; 和（ii）在齐格勒 - 纳塔聚合催化剂体系中在第二气体或浆料相阶段中聚合乙烯单体以获得第二聚乙烯级分组分（B）。齐格勒 - 纳塔聚合催化剂体系包括：1）通过使至少a）使式（I）的Mg-醇合物络合物b）式（II）的铝化合物与式和c）钒化合物和摩尔比（V:Ti）为10:90至90:10的钛化合物; 和2）式（III）的一种或多种有机金属助催化剂。线性低密度聚乙烯显示改进的共聚单体组成分布本文描述了式（I），（II）和（III）。

15. 发明授权

US07291655B2 Polymerisation method and device for carrying out a polymerisation method 失效
标题翻译：用于进行聚合方法的聚合方法和装置
公开(公告)号：US07291655B2
公开(公告)日：2007-11-06
申请号：US10479384
申请日：2002-05-29
申请人： Karl-Heinz Reichert , Annette Wittebrock , Kalle Kallio
发明人： Karl-Heinz Reichert , Annette Wittebrock , Kalle Kallio
IPC分类号： C08F2/46 , C08F2/50
CPC分类号： B01J31/14 , B01J8/20 , B01J8/24 , B01J19/12 , B01J19/123 , B01J19/128 , B01J31/143 , B01J31/2295 , B01J31/38 , B01J31/4084 , B01J38/00 , B01J2219/0879 , B01J2219/0886 , B01J2219/0892 , B01J2231/10 , B01J2231/12 , B01J2231/20 , B01J2531/48 , B01J2531/49 , C08F2/46 , C08F4/65912 , C08F4/65916 , C08F4/65922 , C08F4/65925 , C08F4/65927 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/00 , C08F210/02 , C08F291/00 , Y02P20/584 , Y10S522/912 , Y10S522/915 , C08F2/48 , C08F2500/03 , C08F2500/07 , C08F2500/12 , C08F2500/15 , C08F220/10
摘要： A polymerization process with elevated productivity using a coordination catalyst, wherein electromagnetic radiation is applied during polymerization. The irradiation of light greatly increases the activity of the coordination catalyst.
摘要翻译：使用配位催化剂提高生产率的聚合方法，其中在聚合过程中施加电磁辐射。光的照射大大增加了配位催化剂的活性。

16. 发明授权

US06730756B1 Catalyst and process for olefin polymerization 失效
标题翻译：催化剂和烯烃聚合方法
公开(公告)号：US06730756B1
公开(公告)日：2004-05-04
申请号：US09857370
申请日：2001-10-09
申请人： Ove Andell , Kalle Kallio , Hikka Knuuttitila
发明人： Ove Andell , Kalle Kallio , Hikka Knuuttitila
IPC分类号： C08F444
CPC分类号： C08F10/02 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F110/02 , C08F210/16 , Y10S526/943 , C08F4/65927 , C08F4/65925 , C08F2500/03 , C08F2500/18 , C08F210/14 , C08F2500/12
摘要： Olefin polymerization may be catalysed by a wide range of catalytic materials. Described herein is a heterogeneous olefin polymerization catalyst comprising a porous paniculate support material having impregnated therein a metallocene catalyst the metal atom whereof is bound to an amide group which is not bound to an &eegr;-ligand of the metallocene, or the reaction product of a said metallocene catalyst and a co-catalyst.
摘要翻译：烯烃聚合可以由各种催化材料催化。本文描述的是一种异质烯烃聚合催化剂，其包含多孔颗粒载体材料，其中浸渍有茂金属催化剂，其金属原子结合到不与茂金属的η - 配位体结合的酰胺基，或所述金属茂催化剂的反应产物茂金属催化剂和助催化剂。

17. 发明授权

US08829128B2 Preparation of polypropylene in the presence of a single-site catalyst 有权
标题翻译：在单中心催化剂存在下制备聚丙烯
公开(公告)号：US08829128B2
公开(公告)日：2014-09-09
申请号：US13516378
申请日：2010-06-16
申请人： Lauri Huhtanen , Kalle Kallio , Pascal Castro
发明人： Lauri Huhtanen , Kalle Kallio , Pascal Castro
IPC分类号： C08F4/642 , C08F4/6592 , C08F10/06
CPC分类号： C08F10/00 , C08F4/65927 , C08F110/06 , C08F4/65912
摘要： Process for the preparation of a polypropylene, wherein propylene is polymerized optionally with a comonomer selected from the group consisting of ethylene, a C4-C20 α-olefin and mixtures thereof, in the presence of a catalyst system comprising solid catalyst particles, wherein the solid catalyst particles (a) comprise a transition metal compound of formula (I) LmRnMXq (I) wherein “M” is a transition metal of anyone of the groups 3 to 10 of the periodic table (IUPAC), each “X” is independently a monovalent anionic σ-ligand, each “L” is independently an organic ligand which coordinates to the transition metal (M), each “R” is a bridging group linking two organic ligands (L), “m” is 2 or 3, preferably 2, “n” is 0, 1 or 2, preferably 1, “q” is 1, 2 or 3, preferably 2, m+q is equal to the valency of the transition metal (M), (c) comprise a cocatalyst (Co) comprising an element (E) of group 13 of the periodic table (IUPAC), preferably a cocatalyst (Co) comprising a compound of A1, wherein further the loss of activity of the solid catalyst particles during polymerization is at most 20%.
摘要翻译：制备聚丙烯的方法，其中在包含固体催化剂颗粒的催化剂体系的存在下，丙烯任选地与选自乙烯，C 4 -C 20α-烯烃及其混合物的共聚单体聚合，其中固体催化剂颗粒（a）包含式（I）的过渡金属化合物LmRnMXq（I）其中“M”是元素周期表（IUPAC）中任何3至10族的过渡金属，每个“X”独立地为每个“L”独立地是与过渡金属（M）配位的有机配体，每个“R”是连接两个有机配体（L）的桥连基团，“m”是2或3，优选2，“n”为0,1或2，优选为1，“q”为1,2或3，优选2，m + q等于过渡金属（M）的化合价，（c）包含包括元素周期表第13族元素（I）的助催化剂（Co）（IUPAC），优选助催化剂（Co）是A1的化合物，其中在聚合期间固体催化剂颗粒的活性进一步降低至多20％。

18. 发明申请

US20130253152A1 PREPARATION OF A SOLID CATALYST SYSTEM 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US20130253152A1
公开(公告)日：2013-09-26
申请号：US13695884
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
IPC分类号： C08F4/76 , C08F4/52
CPC分类号： C08F4/76 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/46 , B01J2531/48 , B01J2531/49 , B01J2531/90 , B01J2531/94 , C07F5/068 , C08F4/52 , C08F4/6028 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , Y10S526/943 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system (CS) comprising the steps of preparing a liquid clathrate (LC) comprising (a) a lattice (L) being the reaction product of (i) aluminoxane (A), (ii) an organometallic compound (O) of a transition metal (M) of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and (i) a compound (B) being effective to form with the aluminoxane (A) and the organometallic compound (O) the lattice (L), and (b) a guest (G) being an hydro-carbon compound (HC), and subsequently precipitating said liquid clathrate (LC) obtaining said solid catalyst system (SC).
摘要翻译：制备固体催化剂体系（CS）的方法，包括以下步骤：制备液体包合物（LC），其包含（a）格子（L），其为（i）铝氧烷（A），（ii）有机金属（IUPAC 2007）第3至10族的过渡金属（M）或锕系元素或镧系元素的化合物（O）和（i）与铝氧烷（A）形成有效的化合物（B）和有机金属化合物（O），晶格（L）和（b）作为氢碳化合物（HC）的客体（G），随后沉淀得到所述固体催化剂体系（SC）的所述液体包合物（LC）。

19. 发明申请

US20120277384A1 PREPARATION OF POLYPROPYLENE IN THE PRESENCE OF A SINGLE-SITE CATALYST 有权
标题翻译：单壁催化剂存在下聚丙烯的制备
公开(公告)号：US20120277384A1
公开(公告)日：2012-11-01
申请号：US13516378
申请日：2010-06-16
申请人： Lauri Huhtanen , Kalle Kallio , Pascal Castro
发明人： Lauri Huhtanen , Kalle Kallio , Pascal Castro
IPC分类号： C08F4/6592 , C08F2/01 , C08F210/06 , C08F110/06
CPC分类号： C08F10/00 , C08F4/65927 , C08F110/06 , C08F4/65912
摘要： Process for the preparation of a polypropylene, wherein propylene is polymerised optionally with a comonomer selected from the group consisting of ethylene, a C4-C20 α-olefin and mixtures thereof, in the presence of a catalyst system comprising solid catalyst particles, wherein the solid catalyst particles (a) comprise a transition metal compound of formula (I) LmRnMXq (I) wherein “M” is a transition metal of anyone of the groups 3 to 10 of the periodic table (IUPAC), each “X” is independently a monovalent anionic σ-ligand, each “L” is independently an organic ligand which coordinates to the transition metal (M), each “R” is a bridging group linking two organic ligands (L), “m” is 2 or 3, preferably 2, “n” is 0, 1 or 2, preferably 1, “q” is 1, 2 or 3, preferably 2, m+q is equal to the valency of the transition metal (M), (c) comprise a cocatalyst (Co) comprising an element (E) of group 13 of the periodic table (IUPAC), preferably a cocatalyst (Co) comprising a compound of Al, wherein further the loss of activity of the solid catalyst particles during polymerization is at most 20%.
摘要翻译：制备聚丙烯的方法，其中在包含固体催化剂颗粒的催化剂体系的存在下，丙烯任选地与选自乙烯，C 4 -C 20α-烯烃及其混合物的共聚单体聚合，其中固体催化剂颗粒（a）包含式（I）的过渡金属化合物LmRnMXq（I）其中M是周期表（IUPAC）中第3至10族中的任何一个的过渡金属，每个X独立地是一价阴离子＆每个L独立地是与过渡金属（M）配位的有机配体，每个R是连接两个有机配体（L）的桥连基团，m是2或3，优选2，n是0,1或2 ，优选1，q为1,2或3，优选2，m + q等于过渡金属（M）的化合价，（c）包含助催化剂（Co），其包含第13族元素（E）周期表（IUPAC），优选包含Al的化合物的助催化剂（Co），其中，在聚合过程中固体催化剂颗粒的活性降低至多20％。

20. 发明授权

US08828901B2 Preparation of a solid catalyst system 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US08828901B2
公开(公告)日：2014-09-09
申请号：US13696184
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
IPC分类号： C08F4/642 , C08F4/6592
CPC分类号： C08F4/76 , B01J31/0239 , B01J31/0268 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/90 , C08F4/52 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system comprising the steps of generating an emulsion by dispersing a liquid clathrate in a solution wherein (i) the solution constitutes the continuous phase of the emulsion and (ii) the liquid clathrate constitutes in form of droplets the dispersed phase of the emulsion, solidifying said dispersed phase to convert said droplets to solid particles and optionally recovering said particles to obtain said catalyst system, wherein the liquid clathrate comprises a lattice being the reaction product of aluminoxane, an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and a further compound being effective to form with the aluminoxane and the organometallic compound the lattice, and a guest being an hydrocarbon compound, and the solution comprises a silicon fluid and a hydrocarbon solvent.
摘要翻译：制备固体催化剂体系的方法，包括以下步骤：通过将液体包合物分散在溶液中产生乳液，其中（i）溶液构成乳液的连续相，和（ii）液体包合物以液滴的形式构成分散相，固化所述分散相，将所述液滴转化为固体颗粒，任选地回收所述颗粒以获得所述催化剂体系，其中所述液体包合物包含格子，其为铝氧烷，过渡金属的有机金属化合物周期表第3至10组（IUPAC 2007）或锕系元素或镧系元素，以及有效与铝氧烷和有机金属化合物形成晶格的另外的化合物，以及作为烃化合物的客体，该溶液包含硅液和烃溶剂。

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