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11. 发明授权

US10369547B2 Composition based on oxides of cerium, of zirconium and of another rare earth metal with high reducibility, preparation process and use in the field of catalysis 有权
公开(公告)号：US10369547B2
公开(公告)日：2019-08-06
申请号：US14125639
申请日：2012-06-13
申请人： Simon Ifrah , Emmanuel Rohart , Julien Hernandez , Dominique Horbez , Lama Itani
发明人： Simon Ifrah , Emmanuel Rohart , Julien Hernandez , Dominique Horbez , Lama Itani
IPC分类号： B01J23/10 , C01G25/00 , B01D53/94 , B01J37/03 , B01J37/06 , B01J37/34 , B01J23/34 , B01J23/83 , B01J35/02 , B01J35/10 , B01J37/00
摘要： The composition of the invention is based on oxides of cerium, of zirconium and of at least one rare earth metal other than cerium, with a cerium oxide content of greater than 50% by weight and it has, after calcination at 1000° C. for 4 hours, a specific surface area of at least 20 m2/g and an amount of mobile oxygen between 200° C. and 400° C. of at least 0.8 ml O2/g. It is prepared by a process in which, in a reactor, a mixture of compounds of cerium, of zirconium and of the other rare earth metal is reacted continuously with a basic compound with a residence time of the reaction medium in the mixing zone of the reactor of at most 100 milliseconds; the precipitate is heated then brought into contact with a surfactant before being calcined.

12. 发明授权

US10125333B2 Organic dispersion of iron-based particles in crystallized form 有权
公开(公告)号：US10125333B2
公开(公告)日：2018-11-13
申请号：US13995798
申请日：2011-12-19
申请人： Lauriane D'Alencon , Julien Hernandez , Virginie Harle , Michael Lallemand
发明人： Lauriane D'Alencon , Julien Hernandez , Virginie Harle , Michael Lallemand
IPC分类号： C10L1/12 , C10L10/06 , C10L1/10 , C10L10/02 , C10L1/16 , C10L1/188
摘要： A dispersion includes an apolar organic phase, at least one amphiphilic agent, and solid objects based on particles of an iron compound in crystallized form of small size.

13. 发明申请

US20050004297A1 Diene rubber composition for tire comprising a specific silica as reinforcing filler 有权
标题翻译：用于轮胎的二烯橡胶组合物，其包含特定二氧化硅作为增强填料
公开(公告)号：US20050004297A1
公开(公告)日：2005-01-06
申请号：US10777075
申请日：2004-02-13
申请人： Olivier Durel , Arnaud Lapra , Julien Hernandez , Remi Valero
发明人： Olivier Durel , Arnaud Lapra , Julien Hernandez , Remi Valero
IPC分类号： B60C1/00 , C01B33/143 , C01B33/193 , C08K3/36 , C08K5/548 , C08L9/00 , C08K3/34
CPC分类号： B82Y30/00 , B60C1/0016 , C01B33/193 , C01P2004/50 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C08K3/36 , C08K5/548 , Y10T152/10495 , C08L21/00
摘要： Diene rubber compositions are described containing a diene elastomer, a reinforcing inorganic filler, and a coupling agent wherein the inorganic filler includes a silica having the following characteristics: (a) a BET specific surface area between 45 and 400 m2/g; (b) a CTAB specific surface area between 40 and 380 m2/g; (c) an average particle size (by mass), dw, of 20 to 300 nm; and at least one of the following characteristics, preferably two and more preferably all three: (d) a particle size distribution such that dw≧/CTAB)−30; (e) a porosity which meets the criterion L/FI≧−0.0025 CTAB+0.85; (f) an amount of silanols per unit of surface area, NSiOH/nm2; NSiOH/nm2≦−0.027 CTAB+10.5. These diene rubber compositions can be used for the manufacture of tires or of semi-finished products intended for tires.
摘要翻译：描述了含有二烯弹性体，增强无机填料和偶联剂的二烯橡胶组合物，其中无机填料包括具有以下特性的二氧化硅：（a）BET比表面积为45-400m 2 / g; （b）CTAB比表面积在40和380m 2 / g之间; （c）平均粒径（质量百分比）dw为20〜300nm; 和以下特征中的至少一个，优选两个，更优选全部三个：（d）使得dw> = / CTAB）-30的粒度分布; （e）满足标准L / FI> = - 0.0025 CTAB + 0.85的孔隙率; （f）每单位表面积的硅烷醇量，NSiOH / nm 2; NSiOH / nm 2 = 0.027 CTAB + 10.5。这些二烯橡胶组合物可用于制造轮胎或用于轮胎的半成品。

14. 发明申请

US20140013659A1 ORGANIC DISPERSION OF IRON-BASED PARTICLES IN CRYSTALLIZED FORM 审中-公开
标题翻译：在结晶形式中的基于有机碳的颗粒的有机分散
公开(公告)号：US20140013659A1
公开(公告)日：2014-01-16
申请号：US13995798
申请日：2011-12-19
申请人： Lauriane D'Alencon , Julien Hernandez , Virginie Harle , Michael Lallemand
发明人： Lauriane D'Alencon , Julien Hernandez , Virginie Harle , Michael Lallemand
IPC分类号： C10L10/06
CPC分类号： C10L10/06 , C10L1/10 , C10L1/1608 , C10L1/1616 , C10L1/1881 , C10L1/1883 , C10L10/02
摘要： A dispersion includes an apolar organic phase, at least one amphiphilic agent, and solid objects based on particles of an iron compound in crystallized form of small size.
摘要翻译：分散体包括非极性有机相，至少一种两亲性试剂和基于小型结晶形式的铁化合物颗粒的固体物质。

15. 发明授权

US07884153B2 Method for preparing anisotropic silica aggregates 有权
标题翻译：制备各向异性二氧化硅聚集体的方法
公开(公告)号：US07884153B2
公开(公告)日：2011-02-08
申请号：US10563792
申请日：2004-07-07
申请人： Lionel Ventelon , Julien Hernandez , Françoise Lafuma , Christophe Chassenieux , Christelle Perreur
发明人： Lionel Ventelon , Julien Hernandez , Françoise Lafuma , Christophe Chassenieux , Christelle Perreur
IPC分类号： C08K3/36 , C01B33/18
CPC分类号： B82Y30/00 , C01B33/12 , C01B33/16 , C01P2004/32 , C01P2004/50 , C01P2004/64 , C01P2006/12 , C09C1/3036 , C09C1/3072 , C09K3/1409
摘要： The invention concerns a method for preparing anisotropic silica aggregates comprising the following steps: a) contacting at least one polymer with non-aggregated silica particles and/or highly dispersed in an aqueous medium, with a ratio R, polymer weight to silica particle surface, ranging between 0.03 and 2 mg/m; 2; and whereof the electrostatic value of the silica particle surface is not less than the value of the charge of the silica particle surface measured in an aqueous phase without added salts at a pH not less than 7; b) consolidating the aggregates obtained at step a) either by heat treatment, or by precipitation of a mineral compound. The invention also concerns a silica aggregate comprising a chaining of elementary particles whereof the number of particles ranges between 5 and 15, whereof 80% of elementary particles are in contact with not more than 2 particles and whereof the greatest distance measurable between 2 points of the aggregate is not more than 5 times the average size of one elementary particle.
摘要翻译：本发明涉及一种制备各向异性二氧化硅聚集体的方法，包括以下步骤：a）使至少一种聚合物与非聚集的二氧化硅颗粒接触和/或高度分散在水性介质中，R与聚合物重量与二氧化硅颗粒表面的比率，范围在0.03至2mg / m; 2; 并且二氧化硅颗粒表面的静电值不小于在不低于7的pH下在没有添加盐的情况下在水相中测量的二氧化硅颗粒表面的电荷的值; b）通过热处理或通过沉淀矿物化合物来固化在步骤a）获得的聚集体。本发明还涉及一种二氧化硅聚集体，其包含基本粒子的连接，其中粒子数目在5至15之间，其中80％的基本粒子与不超过2个粒子接触，并且其中2个点之间的最大距离可以测量聚集体不超过一个基本粒子的平均尺寸的5倍。

16. 发明授权

US08974764B2 Composition including a lanthanum perovskite on an alumina or aluminium oxyhydroxide substrate, preparation method and use in catalysis 有权
标题翻译：在氧化铝或羟基氧化铝基体上的钙钛矿型镧的组成，其制备方法和催化剂的用途
公开(公告)号：US08974764B2
公开(公告)日：2015-03-10
申请号：US13254151
申请日：2010-02-25
申请人： Simon Ifrah , Olivier Larcher , Rui Jorge Coelho Marques , Michael Lallemand , Julien Hernandez
发明人： Simon Ifrah , Olivier Larcher , Rui Jorge Coelho Marques , Michael Lallemand , Julien Hernandez
IPC分类号： C01B13/00 , C01C1/00 , C01D1/02 , C01G49/00 , C01G45/12 , C01F7/00 , B01J23/00 , B01J23/10 , B01J23/83 , B01J23/34 , B01J35/00 , B01J37/03 , B82Y30/00 , C04B35/26
CPC分类号： B01J35/026 , B01J21/04 , B01J23/002 , B01J23/10 , B01J23/34 , B01J23/83 , B01J35/006 , B01J37/031 , B01J2523/00 , B82Y30/00 , C01G45/1264 , C01G49/0054 , C01P2002/34 , C01P2002/72 , C01P2004/64 , C04B35/2675 , C04B2235/3208 , C04B2235/3227 , C04B2235/3229 , Y02C20/10 , B01J2523/3706 , B01J2523/842 , B01J2523/72 , B01J2523/23 , B01J2523/3712
摘要： A composition is described that includes a perovskite of the formula LaMO3, where M is at least one element selected from among iron, aluminum or manganese, in the form of particles dispersed on an alumina or aluminum oxyhydroxide substrate, wherein after calcination at 700° C. for 4 hours, the perovskite is in the form of a pure crystallographic phase, and in that the size of the perovskite particles does not exceed 15 nm. The described composition can be used in the field of catalysis.
摘要翻译：描述了一种组合物，其包括式LaMO 3的钙钛矿，其中M是选自铁，铝或锰中的至少一种元素，分散在氧化铝或羟基氧化铝基质上的颗粒形式，其中在700℃下煅烧 4小时，钙钛矿为纯晶相，形成钙钛矿颗粒的尺寸不超过15nm。所述组合物可用于催化领域。

17. 发明申请

US20110178227A1 NOVEL PRECIPITATED SILICA HAVING PARTICULAR MORPHOLOGY, GRADING AND POROSITY, PREPARATION THEREOF AND REINFORCING OF POLYMERS THEREWITH 有权
标题翻译：具有特殊形态，分级和多孔性的新型沉淀二氧化硅，其制备和聚合物的增强
公开(公告)号：US20110178227A1
公开(公告)日：2011-07-21
申请号：US12921423
申请日：2009-03-09
申请人： Emmanuelle Allain , Julien Hernandez , Lionel Ventelon , Laurent Guy , Marc Airiau
发明人： Emmanuelle Allain , Julien Hernandez , Lionel Ventelon , Laurent Guy , Marc Airiau
IPC分类号： C08K3/36 , C01B33/12 , C08L55/00
CPC分类号： C01B33/193 , C01B33/12 , Y10T428/2982
摘要： Precipitated silicas including clusters of large primary silica particles having at the surface thereof small primary silica particles, have a specific surface area CTAB (SCTAB) ranging from 60 to 400 m2/g; a cluster average size d50, as measured by XDC grading after ultrasound deagglomeration, such that d50 (nm)>(6214/SCTAB (m2/g)+23; a pore volume distribution such that V(d5-d50)/V(d5-d100)>0.906−(0.0013×SCATB (m2/g)); and a pore size distribution such that Mode (nm)>(4166/SCTAB (m2/g))−9.2; such silicas are useful reinforcing fillers for polymers.
摘要翻译：沉淀二氧化硅，其表面具有小的一次二氧化硅颗粒的具有大的初级二氧化硅颗粒的簇，其比表面积CTAB（SCTAB）为60-400m2 / g; 通过超声解聚后的XDC分级测定，使得d50（nm）>（6214 / SCTAB（m2 / g）+23;孔径分布为V（d5-d50）/ V（d5））的簇平均尺寸d50 -d100）> 0.906-（0.0013×SCATB（m2 / g））;孔径分布使得Mode（nm）>（4166 / SCTAB（m2 / g））-2.9）;这样的二氧化硅是聚合物的增强填料。

18. 发明申请

US20070219305A1 Method for Preparing Anisotropic Silica Aggregates 有权
标题翻译：各向异性二氧化硅聚集体的制备方法
公开(公告)号：US20070219305A1
公开(公告)日：2007-09-20
申请号：US10563792
申请日：2004-07-07
申请人： Lionel Ventelon , Julien Hernandez , Francoise Lafuma
发明人： Lionel Ventelon , Julien Hernandez , Francoise Lafuma
IPC分类号： B60C1/00
CPC分类号： B82Y30/00 , C01B33/12 , C01B33/16 , C01P2004/32 , C01P2004/50 , C01P2004/64 , C01P2006/12 , C09C1/3036 , C09C1/3072 , C09K3/1409
摘要： The invention concerns a method for preparing anisotropic silica aggregates comprising the following steps: a) contacting at least one polymer with non-aggregated silica particles and/or highly dispersed in an aqueous medium, with a ratio R, polymer weight to silica particle surface, ranging between 0.03 and 2 mg/m; 2; and whereof the electrostatic value of the silica particle surface is not less than the value of the charge of the silica particle surface measured in an aqueous phase without added salts at a pH not less than 7; b) consolidating the aggregates obtained at step a) either by heat treatment, or by precipitation of a mineral compound. The invention also concerns a silica aggregate comprising a chaining of elementary particles whereof the number of particles ranges between 5 and 15, whereof 80% of elementary particles are in contact with not more than 2 particles and whereof the greatest distance measurable between 2 points of the aggregate is not more than 5 times the average size of one elementary particle.
摘要翻译：本发明涉及一种制备各向异性二氧化硅聚集体的方法，包括以下步骤：a）使至少一种聚合物与非聚集的二氧化硅颗粒接触和/或高度分散在水性介质中，R与聚合物重量与二氧化硅颗粒表面的比率，范围在0.03至2mg / m; 2; 并且二氧化硅颗粒表面的静电值不小于在不低于7的pH下在没有添加盐的情况下在水相中测量的二氧化硅颗粒表面的电荷的值; b）通过热处理或通过沉淀矿物化合物来固化在步骤a）获得的聚集体。本发明还涉及一种二氧化硅聚集体，其包含基本粒子的连接，其中粒子数目在5至15之间，其中80％的基本粒子与不超过2个粒子接触，并且其中2个点之间的最大距离可以测量聚集体不超过一个基本粒子的平均尺寸的5倍。

19. 发明授权

US09359215B2 Precipitated silica having particular morphology, grading and porosity, preparation thereof and reinforcing of polymers therewith 有权
标题翻译：沉淀二氧化硅具有特定的形态，分级和孔隙率，其制备和聚合物的增强
公开(公告)号：US09359215B2
公开(公告)日：2016-06-07
申请号：US12921423
申请日：2009-03-09
申请人： Emmanuelle Allain , Julien Hernandez , Lionel Ventelon , Laurent Guy , Marc Airiau
发明人： Emmanuelle Allain , Julien Hernandez , Lionel Ventelon , Laurent Guy , Marc Airiau
IPC分类号： C01B33/12 , C01B33/193
CPC分类号： C01B33/193 , C01B33/12 , Y10T428/2982
摘要： Precipitated silicas including clusters of large primary silica particles having at the surface thereof small primary silica particles, have a specific surface area CTAB (SCTAB) ranging from 60 to 400 m2/g; a cluster average size d50, as measured by XDC grading after ultrasound deagglomeration, such that d50 (nm)>(6214/SCTAB (m2/g)+23; a pore volume distribution such that V(d5-d50)/V(d5-d100)>0.906−(0.0013×SCATB (m2/g)); and a pore size distribution such that Mode (nm)>(4166/SCTAB (m2/g))−9.2; such silicas are useful reinforcing fillers for polymers.
摘要翻译：沉淀二氧化硅，其表面具有小的一次二氧化硅颗粒的大的一次二氧化硅颗粒簇，其比表面积CTAB（SCTAB）为60-400m2 / g; 通过超声解聚后的XDC分级测定，使得d50（nm）>（6214 / SCTAB（m2 / g）+23;孔径分布为V（d5-d50）/ V（d5））的簇平均尺寸d50 -d100）> 0.906-（0.0013×SCATB（m2 / g））;孔径分布使得Mode（nm）>（4166 / SCTAB（m2 / g））-2.9）;这样的二氧化硅是聚合物的增强填料。

20. 发明授权

US09333802B2 Diene rubber composition for tire including a silica as a reinforcing filler 有权
标题翻译：用于轮胎的二烯橡胶组合物，其包括二氧化硅作为增强填料
公开(公告)号：US09333802B2
公开(公告)日：2016-05-10
申请号：US12921540
申请日：2009-03-09
申请人： Damien Thomasson , Emmanuelle Allain , Julien Hernandez
发明人： Damien Thomasson , Emmanuelle Allain , Julien Hernandez
IPC分类号： B60C1/00 , C08K3/36 , C08K5/548 , C08K9/02
CPC分类号： B60C1/0016 , C08K3/36 , C08K5/548 , C08K9/02 , C08L21/00
摘要： A diene rubber composition for tires based on at least (i) one diene elastomer, (ii) one reinforcing inorganic filler and (iii) one coupling agent which provides the bonding between the inorganic filler and the elastomer. The inorganic filler comprises at least one silica capable of being obtained by the preparation process of the type comprising the reaction of a silicate with an acidifying agent, whereby a silica suspension is obtained, followed by the separation and the drying of this suspension. The reaction of the silicate with the acidifying agent is carried out according to the following successive stages: (i) an aqueous suspension of precipitated silica, exhibiting a pH of between 2.5 and 5.3, is brought into contact (mixing) with acidifying agent and silicate, in such a way that the pH of the reaction medium is maintained between 2.5 and 5.3, (ii) silicate is added to the reaction medium obtained, so as to increase the pH of the reaction medium up to a value of between 4.7 and 6.3.
摘要翻译：一种用于轮胎的二烯橡胶组合物，其至少基于（i）一种二烯弹性体，（ii）一种增强无机填料和（iii）提供无机填料和弹性体之间的结合的偶联剂。无机填料包含至少一种能够通过包括硅酸盐与酸化剂的反应的制备方法获得的二氧化硅，由此获得二氧化硅悬浮液，然后分离和干燥该悬浮液。硅酸盐与酸化剂的反应根据以下连续阶段进行：（i）沉淀二氧化硅的水性悬浮液，其pH值介于2.5和5.3之间，与酸化剂和硅酸盐接触（混合）以使反应介质的pH保持在2.5和5.3之间的方式，（ii）将硅酸盐加入到所获得的反应介质中，以使反应介质的pH升高至4.7-6.3之间。

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