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11. 发明申请

US20140157987A1 Fe(II)-SUBSTITUTED BETA TYPE ZEOLITE, GAS ADSORBENT CONTAINING SAME AND METHOD FOR PRODUCING SAME, AND METHOD FOR REMOVING NITROGEN MONOXIDE AND HYDROCARBON 有权
标题翻译： Fe（II） - 沸石型沸石，含有它们的气体吸附剂及其生产方法，以及除去一氧化氮和氢氧化碳的方法
公开(公告)号：US20140157987A1
公开(公告)日：2014-06-12
申请号：US13979670
申请日：2012-01-17
申请人： Masaru Ogura , Keiji Itabashi , Tatsuya Okubo , Shanmugam Palani Elangovan
发明人： Masaru Ogura , Keiji Itabashi , Tatsuya Okubo , Shanmugam Palani Elangovan
IPC分类号： B01J20/30 , B01J20/28 , B01D53/02
CPC分类号： B01J20/3085 , B01D53/02 , B01D2253/108 , B01D2253/1085 , B01D2253/306 , B01D2253/311 , B01D2257/404 , B01D2257/702 , B01D2258/01 , B01J20/28061 , B01J20/28071 , C01B39/065 , C01B39/46 , C01P2006/12 , C01P2006/14 , F01N3/0835 , F01N3/0842
摘要： To provide an Fe(II)-substituted beta type zeolite which has been ion-exchanged with Fe(II) ions and can effectively adsorb and remove nitrogen monoxide or hydrocarbon contained in gas to be cleaned, even if oxygen is present in the gas at a high concentration or the temperature of the gas is low. In the Fe(II)-substituted beta type zeolite, a ratio of SiO2/Al2O3 is preferably 10 to 18, a BET specific surface area is preferably 400 m2/g to 700 m2/g, a micropore specific surface area is preferably 290 m2/g to 500 m2/g, and a micropore volume is preferably 0.15 cm3/g to 0.25 cm3/g. The amount of Fe(II) supported is preferably 0.01% by mass to 6.5% by mass based on the Fe(II)-substituted beta type zeolite.
摘要翻译：为了提供与Fe（II）离子进行离子交换的Fe（II） - 取代的β型沸石，并且即使在气体中存在氧气也可以有效地吸附和去除待清洁的气体中所含的一氧化氮或烃。高浓度或气体的温度低。在Fe（II）取代的β型沸石中，SiO 2 / Al 2 O 3的比例优选为10〜18，BET比表面积优选为400m 2 / g〜700m 2 / g，微孔比表面积优选为290m 2 g〜500m 2 / g，微孔体积优选为0.15cm 3 / g〜0.25cm 3 / g。相对于Fe（II）取代的β型沸石，Fe（II）的量优选为0.01质量％〜6.5质量％。

12. 发明申请

US20130343986A1 METHOD FOR PRODUCING MTW-TYPE ZEOLITE 有权
标题翻译：生产MTW型沸石的方法
公开(公告)号：US20130343986A1
公开(公告)日：2013-12-26
申请号：US13980765
申请日：2012-01-17
申请人： Keiji Itabashi , Yoshihiro Kamimura , Tatsuya Okubo
发明人： Keiji Itabashi , Yoshihiro Kamimura , Tatsuya Okubo
IPC分类号： C01B39/46
CPC分类号： C01B39/46 , C01B39/42
摘要： Provided is a method for producing an MTW-type zeolite. The reaction mixture contains a silica source, an alumina source, an alkali source, and water is reacted with a seed crystal of a zeolite to produce an MTW-type zeolite. The reaction mixture has a composition, which makes a synthesized zeolite contain an MFI-type zeolite when the zeolite is synthesized solely from the reaction mixture, is used. As the seed crystal, a beta-type zeolite which has a ratio of SiO2/Al2O3 of 8 to 50 and does not contain a structure direction agent is used. The seed crystal is added to the reaction mixture, in a proportion of 0.1% by mass to 20% by mass based on a silica component in the reaction mixture. The reaction mixture to which the seed crystal has been added is heated at 100° C. to 200° C. in a sealed state.
摘要翻译：提供了一种MTW型沸石的制造方法。反应混合物含有二氧化硅源，氧化铝源，碱源，水与沸石晶种反应生成MTW型沸石。反应混合物具有组合物，当使用沸石仅由反应混合物合成时，其使合成的沸石含有MFI型沸石。作为晶种，使用SiO 2 / Al 2 O 3的比例为8〜50，不含结构方向试剂的β型沸石。相对于反应混合物中的二氧化硅成分，将该晶种以0.1质量％〜20质量％的比例添加到反应混合物中。已加入晶种的反应混合物在密封状态下在100℃加热至200℃。

13. 发明授权

US4466812A Zeolite encapsulating material 失效
标题翻译：沸石封装材料
公开(公告)号：US4466812A
公开(公告)日：1984-08-21
申请号：US404034
申请日：1982-08-02
申请人： Tetsuo Takaishi , Keiji Itabashi , Satoru Morishita , Hisashi Hatotani
发明人： Tetsuo Takaishi , Keiji Itabashi , Satoru Morishita , Hisashi Hatotani
IPC分类号： B01J20/18 , B01J39/14 , C01B3/00 , C01B23/00 , C01B39/02 , C01B39/14 , G21F9/02 , B01D53/04
CPC分类号： C01B3/001 , B01J20/18 , B01J39/14 , C01B23/00 , C01B39/026 , G21F9/02 , Y02E60/327 , Y10S95/902
摘要： A zeolite encapsulating material composed of an A-type zeolite expressed by a typical unit cell (CsxMII.sub.y Naz)(AlO.sub.2.SiO.sub.2).sub.12 .multidot.(NaAlO.sub.2).delta..multidot..omega.H.sub.2 O wherein MII represents a divalent metal; O.ltoreq..delta..ltoreq.1; and .omega. represents a positive number. Further, in the above stated unit cell, x, y and z which respectively represent the numbers of Cs, M and Na within the unit cell are in a relation:x+2y+z=123.ltoreq.x
摘要翻译：由典型的单元电池（CsxMIIyNaz）（AlO 2·SiO 2）12x（NaAlO 2）δ×ωH2 O表示的A型沸石构成的沸石包封材料，其中MII表示二价金属; O

14. 发明授权

US09333495B2 Method for producing MTW-type zeolite 有权
标题翻译：生产MTW型沸石的方法
公开(公告)号：US09333495B2
公开(公告)日：2016-05-10
申请号：US13509677
申请日：2010-11-19
申请人： Keiji Itabashi , Tatsuya Okubo , Kenta Iyoki
发明人： Keiji Itabashi , Tatsuya Okubo , Kenta Iyoki
IPC分类号： C01B39/42 , B01J29/70 , B01J20/30
CPC分类号： C01B39/42 , B01J20/3078 , B01J29/7034
摘要： A method for producing an MTW-type zeolite, comprising (1) mixing an alumina source, an alkali source, a lithium source, and water so as to obtain a reaction mixture (2) Adding a seed crystal of an MTW-type zeolite before or while a silica source is added to the reaction mixture in a proportion of 0.1 to 20% by weight relative to the silica component in the reaction mixture. Mixing and stirring the reaction mixture. Wherein the MTW-type zeolite of the seed crystal has a SiO2/Al2O3 ratio of 10 to 500 and does not contain an organic compound. The reaction mixture has a composition represented by the following molar ratios: SiO2/Al2O3=12 to 200, Na2O/SiO2=0.1 to 0.3, Li2O/(Na2O+Li2O)=0.05 to 0.5 and H2O/SiO2=10 to 50. (3) Air tightly heating the reaction mixture, to which the seed crystal of the MTW type zeolite has been added, at 100 to 200° C.
摘要翻译：一种生产MTW型沸石的方法，包括（1）将氧化铝源，碱源，锂源和水混合以获得反应混合物（2）在MTW型沸石之前加入MTW型沸石的晶种或者相对于反应混合物中的二氧化硅组分，以0.1至20重量％的比例将二氧化硅源加入到反应混合物中。混合搅拌反应混合物。其中晶种的MTW型沸石的SiO 2 / Al 2 O 3比例为10〜500，不含有机化合物。反应混合物具有以下摩尔比表示的组成：SiO 2 / Al 2 O 3 = 12〜200，Na 2 O / SiO 2 = 0.1〜0.3，Li 2 O /（Na 2 O + Li 2 O）= 0.05〜0.5，H 2 O / SiO 2 = 10〜50 3）在100〜200℃下，将加入MTW型沸石的晶种的反应混合物气密加热

15. 发明授权

US08834836B2 Method for producing MTW-type zeolite 有权
标题翻译：生产MTW型沸石的方法
公开(公告)号：US08834836B2
公开(公告)日：2014-09-16
申请号：US13980765
申请日：2012-01-17
申请人： Keiji Itabashi , Yoshihiro Kamimura , Tatsuya Okubo
发明人： Keiji Itabashi , Yoshihiro Kamimura , Tatsuya Okubo
IPC分类号： C01B33/36 , C01B39/00 , C01B39/42 , C01B39/46
CPC分类号： C01B39/46 , C01B39/42
摘要： Provided is a method for producing an MTW-type zeolite. The reaction mixture contains a silica source, an alumina source, an alkali source, and water is reacted with a seed crystal of a zeolite to produce an MTW-type zeolite. The reaction mixture has a composition, which makes a synthesized zeolite contain an MFI-type zeolite when the zeolite is synthesized solely from the reaction mixture, is used. As the seed crystal, a beta-type zeolite which has a ratio of SiO2/Al2O3 of 8 to 50 and does not contain a structure direction agent is used. The seed crystal is added to the reaction mixture, in a proportion of 0.1% by mass to 20% by mass based on a silica component in the reaction mixture. The reaction mixture to which the seed crystal has been added is heated at 100° C. to 200° C. in a sealed state.
摘要翻译：提供了一种MTW型沸石的制造方法。反应混合物含有二氧化硅源，氧化铝源，碱源，水与沸石晶种反应生成MTW型沸石。反应混合物具有组合物，当使用仅由反应混合物合成沸石时，使合成的沸石含有MFI型沸石。作为晶种，使用SiO 2 / Al 2 O 3的比例为8〜50，不含结构方向试剂的β型沸石。相对于反应混合物中的二氧化硅成分，将该晶种以0.1质量％〜20质量％的比例添加到反应混合物中。已加入晶种的反应混合物在密封状态下在100℃加热至200℃。

16. 发明申请

US20130156689A1 METHOD FOR PRODUCING MTW-TYPE ZEOLITE 有权
标题翻译：生产MTW型沸石的方法
公开(公告)号：US20130156689A1
公开(公告)日：2013-06-20
申请号：US13509677
申请日：2010-11-19
申请人： Keiji Itabashi , Tatsuya Okubo , Kenta Iyoki
发明人： Keiji Itabashi , Tatsuya Okubo , Kenta Iyoki
IPC分类号： B01J29/70 , B01J20/30
CPC分类号： C01B39/42 , B01J20/3078 , B01J29/7034
摘要： The method for producing an MTW-type zeolite according to the present invention includes: mixing a silica source, an alumina source, an alkali source, a lithium source, and water so as to obtain a reaction mixture having a composition represented by specific molar ratios; (2) adding an MTW-type zeolite which has a SiO2/Al2O3 ratio of 10 to 500 and does not contain an organic compound, as a seed crystal, to the reaction mixture in a proportion of 0.1 to 20% by weight relative to the silica component in the reaction mixture; and (3) airtightly heating the reaction mixture, to which the seed crystal has been added, at 100 to 200° C.
摘要翻译：根据本发明的MTW型沸石的制造方法包括：将二氧化硅源，氧化铝源，碱源，锂源和水混合，得到具有以比摩尔比表示的组成的反应混合物 ; （2）将SiO 2 / Al 2 O 3比例为10〜500，并且不含作为晶种的有机化合物的MTW型沸石相对于反应混合物的比例为0.1〜20重量％反应混合物中的二氧化硅组分; 和（3）在100〜200℃下将加入了晶种的反应混合物气密加热

17. 发明申请

US20120190534A1 ZEOLITE BETA AND PROCESS FOR PRODUCING THE SAME 有权
标题翻译：沸石BETA及其生产方法
公开(公告)号：US20120190534A1
公开(公告)日：2012-07-26
申请号：US13387631
申请日：2010-07-21
申请人： Keiji Itabashi , Tatsuya Okubo , Yoshihiro Kamimura , Watcharop Chaikittisilp , Shanmugam Palani Elangovan
发明人： Keiji Itabashi , Tatsuya Okubo , Yoshihiro Kamimura , Watcharop Chaikittisilp , Shanmugam Palani Elangovan
IPC分类号： B01J29/70 , C01B39/02 , B82Y30/00 , B82Y40/00
CPC分类号： C01B39/46 , B01D53/945 , B01D2255/502 , B01D2255/912 , B01D2255/9205 , B01D2255/9207 , B01D2258/012 , B01D2258/014 , B01J29/7007 , B01J2229/36 , Y02T10/22
摘要： A zeolite beta according to the present invention has a SiO2/Al2O3 ratio of 10 to 16 and is aluminum-rich. The zeolite beta has a BET specific surface area measured in the state of a sodium type of 500 to 700 m2/g, a micropore specific surface area of 350 to 500 m2/g, and a micropore volume of 0.15 to 0.25 cm3/g.
摘要翻译：本发明的沸石β的SiO 2 / Al 2 O 3比为10〜16，富铝。沸石β具有在500至700m 2 / g的钠类型，微孔比表面积为350至500m 2 / g，微孔体积为0.15至0.25cm 3 / g的状态下测量的BET比表面积。

18. 发明申请

US20070004591A1 Adsorbing agent comprising zeolite for heat pump and method for preparation thereof and use thereof 审中-公开
标题翻译：含有热泵沸石的吸附剂及其制备方法及其应用
公开(公告)号：US20070004591A1
公开(公告)日：2007-01-04
申请号：US10565960
申请日：2004-07-29
申请人： Keiji Itabashi , Masashi Harada , Koichi Sato
发明人： Keiji Itabashi , Masashi Harada , Koichi Sato
IPC分类号： B01J20/00
CPC分类号： B01J20/186 , F24F2203/1036 , F25B17/08
摘要： An adsorbent comprising zeolite exhibiting a moisture adsorption of at least 28 wt. % at 25° C. under a partial pressure of water vapor of 5 Torr, and exhibiting a moisture adsorption difference of 15-25 wt. % between a moisture adsorption at 25° C. under a partial pressure of water vapor of 5 Torr and a moisture adsorption at 100° C. under a partial pressure of water vapor of 15 Torr. This adsorbent is produced by ion-exchanging an exchangeable cation in a zeolite, and then, heat-treating the cation-exchanged zeolite in an air or nitrogen stream, or with steam. The adsorbent exhibits a large moisture adsorption at ordinary temperature under a relatively low partial pressure of water vapor and a small moisture adsorption at a relatively low regeneration temperature, and thus, has an enhanced effective moisture adsorption, and is used for a zeolite-water heat pump system and an open cycle moisture adsorption-desorption system.
摘要翻译：含有至少28重量％水分吸附的沸石的吸附剂％，在25°C的水蒸汽分压为5乇下，表现出15-25wt。％的吸湿差。在25乇的水分吸附下，在5乇的水蒸气的分压下，在100乇的水分吸附下，在15乇的水蒸汽的分压下进行吸湿。该吸附剂通过在沸石中离子交换可交换阳离子，然后在空气或氮气流中或与蒸汽热处理阳离子交换的沸石来制备。吸附剂在相对较低的水蒸气分压和较低的再生温度下的吸湿性较小的情况下，在常温下表现出大的吸湿性，因此具有增强的有效吸湿性，并用于沸石 - 水热泵系统和开放循环水分吸附 - 解吸系统。

19. 发明授权

US09670068B2 Zeolite production method 有权
公开(公告)号：US09670068B2
公开(公告)日：2017-06-06
申请号：US13807080
申请日：2011-06-28
申请人： Keiji Itabashi , Tatsuya Okubo , Yoshihiro Kamimura , Shanmugam P. Elangovan
发明人： Keiji Itabashi , Tatsuya Okubo , Yoshihiro Kamimura , Shanmugam P. Elangovan
IPC分类号： C01B39/46 , C01B39/36 , C01B39/02 , C01B39/26 , C01B39/38 , C01B39/42
CPC分类号： C01B39/46 , C01B39/02 , C01B39/026 , C01B39/26 , C01B39/36 , C01B39/365 , C01B39/38 , C01B39/42 , C30B5/00 , C30B29/34
摘要： Disclosed is a method for readily and inexpensively producing zeolite without using an organic structure-directing agent (organic SDA). Specifically disclosed is a method whereby a gel containing a silica source, an alumina source, an alkaline source and water is reacted with zeolite seed crystals, to produce a zeolite with the same kind of skeletal structure as the zeolite. The gel used is a gel of a composition whereby, when a zeolite is synthesized from this gel only, the synthesized zeolite comprises at least one of the kinds of composite building units of the target zeolite.

20. 发明授权

US09108187B2 Fe(II)-substituted beta type zeolite, gas adsorbent containing same and method for producing same, and method for removing nitrogen monoxide and hydrocarbon 有权
标题翻译： Fe（II）取代的β型沸石，含有它的气体吸附剂及其制备方法，以及除去一氧化氮和烃的方法
公开(公告)号：US09108187B2
公开(公告)日：2015-08-18
申请号：US13979670
申请日：2012-01-17
申请人： Masaru Ogura , Keiji Itabashi , Tatsuya Okubo , Shanmugam Palani Elangovan
发明人： Masaru Ogura , Keiji Itabashi , Tatsuya Okubo , Shanmugam Palani Elangovan
IPC分类号： C01B39/46 , F01N3/08 , B01J20/30 , B01J20/28 , C01B39/06 , B01D53/02
CPC分类号： B01J20/3085 , B01D53/02 , B01D2253/108 , B01D2253/1085 , B01D2253/306 , B01D2253/311 , B01D2257/404 , B01D2257/702 , B01D2258/01 , B01J20/28061 , B01J20/28071 , C01B39/065 , C01B39/46 , C01P2006/12 , C01P2006/14 , F01N3/0835 , F01N3/0842
摘要： To provide an Fe(II)-substituted beta type zeolite which has been ion-exchanged with Fe(II) ions and can effectively adsorb and remove nitrogen monoxide or hydrocarbon contained in gas to be cleaned, even if oxygen is present in the gas at a high concentration or the temperature of the gas is low. In the Fe(II)-substituted beta type zeolite, a ratio of SiO2/Al2O3 is preferably 10 to 18, a BET specific surface area is preferably 400 m2/g to 700 m2/g, a micropore specific surface area is preferably 290 m2/g to 500 m2/g, and a micropore volume is preferably 0.15 cm3/g to 0.25 cm3/g. The amount of Fe(II) supported is preferably 0.01% by mass to 6.5% by mass based on the Fe(II)-substituted beta type zeolite.
摘要翻译：为了提供与Fe（II）离子进行离子交换的Fe（II） - 取代的β型沸石，并且即使在气体中存在氧气也可以有效地吸附和去除待清洁的气体中所含的一氧化氮或烃。高浓度或气体的温度低。在Fe（II）取代的β型沸石中，SiO 2 / Al 2 O 3的比例优选为10〜18，BET比表面积优选为400m 2 / g〜700m 2 / g，微孔比表面积优选为290m 2 g〜500m 2 / g，微孔体积优选为0.15cm 3 / g〜0.25cm 3 / g。相对于Fe（II）取代的β型沸石，Fe（II）的量优选为0.01质量％〜6.5质量％。

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